{"id":21587,"date":"2018-12-28T11:01:58","date_gmt":"2018-12-28T08:01:58","guid":{"rendered":"http:\/\/ihcoedu.uobaghdad.edu.iq\/?p=21587"},"modified":"2018-12-31T10:44:21","modified_gmt":"2018-12-31T07:44:21","slug":"%d9%85%d9%86%d8%a7%d9%82%d8%b4%d8%a9-%d8%b1%d8%b3%d8%a7%d9%84%d8%a9-%d8%b7%d8%a7%d9%84%d8%a8-%d8%a7%d9%84%d9%85%d8%a7%d8%ac%d8%b3%d8%aa%d9%8a%d8%b1-%d8%ac%d8%a8%d8%b1%d9%8a%d9%84-%d8%b9%d8%a8","status":"publish","type":"post","link":"https:\/\/ihcoedu.uobaghdad.edu.iq\/?p=21587","title":{"rendered":"\u0645\u0646\u0627\u0642\u0634\u0629 \u0631\u0633\u0627\u0644\u0629 \u0637\u0627\u0644\u0628 \u0627\u0644\u0645\u0627\u062c\u0633\u062a\u064a\u0631 \u00a0\u062c\u0628\u0631\u064a\u0644 \u0639\u0628\u062f \u0627\u0644\u0633\u062a\u0627\u0631 \u062c\u0628\u0631 \u0645\u0646 \u0642\u0633\u0645 \u0639\u0644\u0648\u0645 \u0627\u0644\u0643\u064a\u0645\u064a\u0627\u0621\u00a0"},"content":{"rendered":"

<\/h4>\n

<\/h4>\n

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\u062a\u062d\u0636\u064a\u0631 (\u0645\u0648\u0646\u064a\u0645\u0631\u0627\u062a \u0648\u0628\u0648\u0644\u064a\u0645\u0631\u0627\u062a) \u062c\u062f\u064a\u062f\u0629 \u0648\u062a\u0642\u064a\u064a\u0645 \u0627\u0644\u0641\u0639\u0627\u0644\u064a\u0629 \u0627\u0644\u0628\u064a\u0648\u0644\u0648\u062c\u064a\u0629 \u0644\u0644\u0628\u0639\u0636 \u0645\u0646\u0647\u0627<\/span><\/h4>\n

\"\"<\/h4>\n

\u062d\u064a\u062b \u062a\u0623\u0644\u0641\u062a \u0644\u062c\u0646\u0629 \u0627\u0644\u0645\u0646\u0627\u0642\u0634\u0629 \u0645\u0646 \u0627\u0644\u062a\u062f\u0631\u064a\u0633\u064a\u064a\u0646 \u0627\u0644\u0623\u0641\u0627\u0636\u0644 :<\/span><\/h4>\n

\u0623.\u062f \u063a\u0632\u0648\u0627\u0646 \u062d\u0633\u0646 \u0639\u0628\u062f \u0627\u0644\u0648\u0647\u0627\u0628 \u0627\u0644\u0635\u0645\u064a\u062f\u0639\u064a\u00a0\u00a0\u00a0 \u00a0(\u0631\u0626\u064a\u0633\u0627)\u00a0\u00a0\u00a0<\/span><\/h4>\n

\u0623.\u0645.\u062f \u0627\u0645\u064a\u0646\u0629 \u0639\u0628\u062f\u0627\u0644\u0631\u062d\u0645\u0646 \u0641\u064a\u0627\u0636 \u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0(\u0639\u0636\u0648\u0627)\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0<\/span><\/h4>\n

\u0623.\u0645.\u062f \u0645\u0646\u0649 \u0633\u0645\u064a\u0631 \u0633\u0639\u064a\u062f\u00a0 \u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0(\u0639\u0636\u0648\u0627)\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0<\/span><\/h4>\n

\u0623.\u062f \u0627\u0628\u062a\u0633\u0627\u0645 \u062e\u0644\u064a\u0641\u0629 \u062c\u0627\u0633\u0645\u00a0\u00a0\u00a0\u00a0 \u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0(\u0639\u0636\u0648\u0627 \u0648\u0645\u0634\u0631\u0641\u0627)\u00a0\u00a0\u00a0\u00a0<\/span><\/h4>\n

<\/h4>\n

\"\"<\/h4>\n

\u062a\u0636\u0645\u0646 \u0645\u0648\u0636\u0648\u0639 \u0627\u0644\u0628\u062d\u062b \u062a\u062d\u0636\u064a\u0631 \u0645\u0631\u0643\u0628\u0627\u062a \u062d\u0644\u0642\u064a\u0629 \u063a\u064a\u0631 \u0645\u062a\u062c\u0627\u0646\u0633\u0629 \u062e\u0645\u0627\u0633\u064a\u0629 (\u062b\u0627\u064a\u0627\u062f\u064a\u0627\u0632\u0648\u0644 , \u0627\u0648\u0643\u0633\u0627\u062f\u0627\u064a\u0627\u0632\u0648\u0644) \u0643\u0645\u0648\u0646\u064a\u0645\u0631\u0627\u062a \u0648\u0627\u0633\u062a\u062e\u062f\u0645\u062a \u0644\u062a\u062d\u0636\u064a\u0631 \u0627\u0644\u0639\u062f\u064a\u062f \u0645\u0646 \u0627\u0644\u0628\u0648\u0644\u064a\u0645\u0631\u0627\u062a \u0644\u0623\u0633\u062a\u062e\u062f\u0627\u0645\u0647\u0627 \u0641\u064a \u0627\u0644\u062a\u0637\u0628\u064a\u0642\u0627\u062a \u0627\u0644\u0635\u0646\u0627\u0639\u064a\u0629 \u0648\u064a\u0642\u0633\u0645 \u0627\u0644\u0639\u0645\u0644 \u0627\u0644\u0649 \u0627\u0631\u0628\u0639\u0629 \u0627\u062c\u0632\u0627\u0621 \u062d\u064a\u062b \u0644\u062e\u0635\u062a \u062e\u0637\u0648\u0627\u062a \u0627\u0644\u062a\u0641\u0627\u0639\u0644\u0627\u062a \u0644\u0643\u0644 \u062c\u0632\u0621 \u0643\u0645\u0627 \u0647\u0648 \u0645\u0648\u0636\u062d \u0627\u062f\u0646\u0627\u0647 :<\/span><\/h4>\n

\u0627\u0644\u062c\u0632\u0621 \u0627\u0644\u0627\u0648\u0644 :\u00a0\u062a\u0636\u0645\u0646 \u0647\u0630\u0627 \u0627\u0644\u062c\u0632\u0621 \u062a\u062d\u0636\u064a\u0631 \u0627\u0644\u0645\u0631\u0643\u0628 \u0627\u0644\u0630\u064a \u064a\u062d\u062a\u0648\u064a \u0639\u0644\u0649 4,3,1- \u0627\u0648\u0643\u0633\u0627\u062f\u064a\u0627\u0632\u0648\u0644 \u0627\u0644\u0645\u0634\u062a\u0642 \u0645\u0646 \u0628\u0627\u0631\u0627 \u0647\u064a\u062f\u0631\u0648\u0643\u0633\u064a \u0628\u0646\u0632\u0644\u062f\u064a\u0647\u0627\u064a\u062f \u0645\u0639 \u0643\u0644\u064a\u062a\u0631\u0648\u0644 \u0643\u0644\u0648\u0631\u0627\u064a\u062f \u0648\u0627\u0644\u0630\u064a \u062a\u0645\u062a \u0628\u0644\u0645\u0631\u062a\u0647 \u0628\u062a\u0641\u0627\u0639\u0644\u0647 \u0645\u0639 \u0643\u0644\u0648\u0631\u064a\u062f\u0627\u062a \u0627\u0644\u062d\u0648\u0627\u0645\u0636 \u0644\u0644\u062d\u0635\u0648\u0644 \u0639\u0644\u0649 \u0628\u0648\u0644\u064a\u0645\u0631\u0627\u062a \u062a\u062d\u062a\u0648\u064a \u0639\u0644\u0649 \u0631\u0648\u0627\u0628\u0637 \u0622\u0645\u0627\u064a\u062f\u064a\u0629 \u0648 \u0623\u064a\u0645\u064a\u0646\u064a\u0629 \u0648 \u0623\u0633\u062a\u0631\u064a\u0629 .<\/span><\/h4>\n

\u0627\u0644\u062c\u0632\u0621 \u0627\u0644\u062b\u0627\u0646\u064a :\u00a0\u062a\u0636\u0645\u0646 \u0647\u0630\u0627 \u0627\u0644\u062c\u0632\u0621 \u062a\u062d\u0636\u064a\u0631 \u0627\u0644\u0645\u0631\u0643\u0628 \u0627\u0644\u0630\u064a \u064a\u062d\u062a\u0648\u064a \u0639\u0644\u0649 4,3,1- \u062b\u0627\u064a\u0627\u062f\u064a\u0627\u0632\u0648\u0644 \u0627\u0644\u0645\u0634\u062a\u0642 \u0645\u0646 \u062d\u0627\u0645\u0636 \u0627\u0644\u0643\u0644\u0648\u062a\u0627\u0631\u064a\u0643 \u0645\u0639 \u0645\u0631\u0643\u0628\u0627\u062a \u0627\u0644\u062b\u0627\u064a\u0648\u0633\u064a\u0645\u064a \u0643\u0627\u0631\u0628\u0627\u0632\u0627\u064a\u062f \u0648\u0627\u0644\u0630\u064a \u062a\u0645\u062a \u0628\u0644\u0645\u0631\u062a\u0647 \u0628\u062a\u0641\u0627\u0639\u0644\u0647 \u0645\u0639 \u0643\u0644\u0648\u0631\u064a\u062f\u0627\u062a \u0627\u0644\u062d\u0648\u0627\u0645\u0636 \u0644\u0644\u062d\u0635\u0648\u0644 \u0639\u0644\u0649 \u0628\u0648\u0644\u064a\u0645\u0631\u0627\u062a \u062a\u062d\u062a\u0648\u064a \u0639\u0644\u0649 \u0631\u0648\u0627\u0628\u0637 \u0622\u0645\u0627\u064a\u062f\u064a\u0629 \u0648 \u0623\u064a\u0645\u064a\u0646\u064a\u0629 \u0648 \u0623\u0633\u062a\u0631\u064a\u0629.<\/span><\/h4>\n

\u0627\u0644\u062c\u0632\u0621 \u0627\u0644\u062b\u0627\u0644\u062b :\u00a0\u062a\u0636\u0645\u0646 \u0647\u0630\u0627 \u0627\u0644\u062c\u0632\u0621 \u062a\u062d\u0636\u064a\u0631 \u0627\u0644\u0645\u0631\u0643\u0628 \u0627\u0644\u0630\u064a \u064a\u062d\u062a\u0648\u064a \u0639\u0644\u0649 4,3,1- \u062b\u0627\u064a\u0627\u062f\u064a\u0627\u0632\u0648\u0644 \u0627\u0644\u0645\u0634\u062a\u0642 \u0645\u0646 \u0645\u0646 \u062d\u0627\u0645\u0636 \u0627\u0644\u0627\u062f\u064a\u0628\u0643 \u0645\u0639 \u0645\u0631\u0643\u0628\u0627\u062a \u0627\u0644\u062b\u0627\u064a\u0648\u0633\u064a\u0645\u064a \u0643\u0627\u0631\u0628\u0627\u0632\u0627\u064a\u062f \u0648\u0627\u0644\u0630\u064a \u062a\u0645\u062a \u0628\u0644\u0645\u0631\u062a\u0647 \u0628\u062a\u0641\u0627\u0639\u0644\u0647 \u0645\u0639 \u0643\u0644\u0648\u0631\u064a\u062f\u0627\u062a \u0627\u0644\u062d\u0648\u0627\u0645\u0636 \u0644\u0644\u062d\u0635\u0648\u0644 \u0639\u0644\u0649 \u0628\u0648\u0644\u064a\u0645\u0631\u0627\u062a \u062a\u062d\u062a\u0648\u064a \u0639\u0644\u0649 \u0631\u0648\u0627\u0628\u0637 \u0622\u0645\u0627\u064a\u062f\u064a\u0629 \u0648 \u0623\u064a\u0645\u064a\u0646\u064a\u0629 \u0648 \u0623\u0633\u062a\u0631\u064a\u0629 .<\/span><\/h4>\n

\u0627\u0644\u062c\u0632\u0621 \u0627\u0644\u0631\u0627\u0628\u0639\u00a0\u00a0: \u062a\u0636\u0645\u0646 \u0647\u0630\u0627 \u0627\u0644\u062c\u0632\u0621 \u062a\u062d\u0636\u064a\u0631 \u0627\u0644\u0645\u0631\u0643\u0628 \u0627\u0644\u0630\u064a \u064a\u062d\u062a\u0648\u064a \u0639\u0644\u0649 4,3,1- \u062b\u0627\u064a\u0627\u062f\u064a\u0627\u0632\u0648\u0644 \u0627\u0644\u0645\u0634\u062a\u0642 \u0645\u0646 \u0628\u0627\u0631\u0627 \u0647\u064a\u062f\u0631\u0648\u0643\u0633\u064a \u0628\u0646\u0632\u0648\u0643 \u0627\u0633\u062f \u0645\u0639 \u0627\u062f\u064a\u0628\u0648\u064a\u0644 \u0643\u0644\u0648\u0631\u0627\u064a\u062f \u0648\u0627\u0644\u0630\u064a \u062a\u0645\u062a \u0628\u0644\u0645\u0631\u062a\u0647 \u0628\u062a\u0641\u0627\u0639\u0644\u0647 \u0645\u0639 \u0643\u0644\u0648\u0631\u064a\u062f\u0627\u062a \u0627\u0644\u062d\u0648\u0627\u0645\u0636 \u0644\u0644\u062d\u0635\u0648\u0644 \u0639\u0644\u0649 \u0628\u0648\u0644\u064a\u0645\u0631\u0627\u062a \u062a\u062d\u062a\u0648\u064a \u0639\u0644\u0649 \u0631\u0648\u0627\u0628\u0637 \u0622\u0645\u0627\u064a\u062f\u064a\u0629 \u0648 \u0623\u064a\u0645\u064a\u0646\u064a\u0629 \u0648 \u0623\u0633\u062a\u0631\u064a\u0629 .<\/span><\/h4>\n

\u0627\u0644\u062c\u0632\u0621 \u0627\u0644\u062e\u0627\u0645\u0633 :\u00a0\u062a\u0636\u0645\u0646 \u0647\u0630\u0627 \u0627\u0644\u062c\u0632\u0621 \u062a\u0641\u0627\u0639\u0644 4,3,1,- \u062b\u0627\u064a\u0627\u062f\u0627\u064a\u0632\u0648\u0644 \u0645\u0639 \u0628\u0627\u0631\u0627 \u0647\u064a\u062f\u0631\u0648\u0643\u0633\u064a \u0628\u0646\u0632\u0644\u062f\u0647\u0627\u064a\u062f \u0627\u0648 \u0641\u0627\u0646\u064a\u0644\u0627 \u0627\u0648 \u062a\u0631\u0641\u062b\u0627\u0644\u062f\u064a\u0647\u0627\u064a\u062f \u0627\u0648\u0645\u0631\u0643\u0628 (1) \u0644\u062a\u062d\u0636\u064a\u0631 \u0642\u0648\u0627\u0639\u062f \u0634\u0641.<\/span><\/h4>\n

\u00a0\u0634\u062e\u0635\u062a (\u0627\u0644\u0645\u0648\u0646\u064a\u0645\u0631\u0627\u062a \u0648\u0627\u0644\u0628\u0648\u0644\u064a\u0645\u0631\u0627\u062a) \u0627\u0644\u0645\u062d\u0636\u0631\u0629 \u0628\u0623\u0633\u062a\u062e\u062f\u0627\u0645 \u0645\u0637\u064a\u0627\u0641\u064a\u0640\u0640\u0629 FT-IR \u0648 1HNMR \u0648 UV. ,\u062f\u0631\u0633\u0640\u0640\u062a \u0627\u0644\u0644\u0632\u0648\u062c\u0629 \u0648\u0627\u0644\u0635\u0641\u0640\u0640\u0627\u062a \u0627\u0644\u062d\u0631\u0627\u0631\u064a\u0640\u0640\u0629 (TGA,DSC) \u0648\u0645\u0642\u064a\u0640\u0640\u0627\u0633 X-Ray \u0644\u0628\u0639\u0636 \u0627\u0644\u0628\u0648\u0644\u064a\u0645\u0631\u0627\u062a \u0648\u0627\u0644\u0641\u0639\u0627\u0644\u064a\u0629 \u0627\u0644\u0628\u064a\u0644\u0648\u062c\u064a\u0629 \u0648\u0627\u0644\u062a\u0648\u0635\u064a\u0644\u064a\u0629 .<\/span><\/h4>\n

\"\"<\/h4>\n

\"\"<\/h4>\n
\n

The MSc .thesis Discussion of student (Jibreel AbdulSatar Jabur) from department of Chemistry<\/span><\/h3>\n

At the hall of the late prof.Dr.Fahad Ali Al-Juboori, The MSc .thesis Discussion of student (Jibreel AbdulSatar Jabur) from department of Chemistry \u00a0entited (Preparing of a new (monomers , polymers) and evaluating the biological activity for some of them)has been discussed<\/span><\/h3>\n

The discussion committee<\/span><\/h3>\n

Prof.Dr.Ghazwan Hassan Abdulwahab Al-Sumaiday\u00a0\u00a0 head<\/span><\/h3>\n

Asst.prof.Dr.Amena \u00a0abdulrahman Faidh \u00a0\u00a0member<\/span><\/h3>\n

Asst.prof.Dr.Muna Sameer Saeed\u00a0\u00a0 member<\/span><\/h3>\n

Prof.Dr.Ebtisam Khalifa Jasim\u00a0\u00a0 supervisor member<\/span><\/h3>\n

The Abstract<\/span><\/h3>\n

\u00a0\u00a0\u00a0 \u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0This work involves synthesis of five member\u00a0 heterocyclics rings (Oxadiazole , Thiadiazole ) which were used as a monomer for preparing many different polymers that using in industrial applications this divided into four parts and the reaction steps for each part are summarized as shown below\u00a0<\/span><\/h3>\n

First part<\/span><\/h3>\n

\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0 This part includes the synthesis of 1,3,4-oxadiazol derived from p-hydroxy benzaldehyde and glutaryl chloride, which were polymerized by acid chloride .the compounds got to be polymers having ( amide , imine and ester) linkage as shown in scheme (1)<\/span><\/h3>\n

Second part<\/span><\/h3>\n

\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0 This part includes the synthesis of 1,3,4- Thiadiazole derived from glutaric acid and thiosemecarbazide,which polymerized with acid chloride, the compounds got to be polymers having ( amide , imine and ester) linkage as shown in scheme (2)<\/span><\/h3>\n

Third part<\/span><\/h3>\n

\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0 This part includes the synthesis of 1,3,4- Thiadiazole derived from adipic acid and thiosemecarbazide, which were polymerized with acid chloride,the compounds got to be polymers having ( amide, imine and ester) linkage as shown in scheme (3)<\/span><\/h3>\n

Fourth part<\/span><\/h3>\n

\u00a0\u00a0\u00a0\u00a0 \u00a0\u00a0\u00a0\u00a0This part includes the synthesis of 1,3,4- Thiadiazole derived from p-hydroxy benzoic acid and adipic chloride, which were polymerized with acid chloride .the compounds got to be polymers having ( amide , imine and ester) linkage as shown in scheme (4)<\/span><\/h3>\n

Fifth part<\/span><\/h3>\n

\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0 This part includes reacted of 1, 3, 4- Thiadiazole, with substituted p-hydroxy benzaladehyde or vanilla or terephthalaldehyde or bis(4-formylphenyl) glutarate to get Schiff ‘s base. as showed in scheme (5),scheme(6),scheme (7)<\/span><\/h3>\n

The new prepared derivatives monomers and polymers were characterized by (FT-IR, 1H-NMR ,UV, thermal analysis (TGA\u00a0 and DSC, X-Ray diffraction, Biological activity, viscosity and conductivity)<\/span><\/h3>\n

<\/h3>\n

<\/h3>\n

\u00a0<\/strong><\/span><\/h3>\n

<\/h3>\n","protected":false},"excerpt":{"rendered":"

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