{"id":24055,"date":"2019-02-26T20:53:48","date_gmt":"2019-02-26T17:53:48","guid":{"rendered":"http:\/\/ihcoedu.uobaghdad.edu.iq\/?p=24055"},"modified":"2019-02-27T23:03:10","modified_gmt":"2019-02-27T20:03:10","slug":"%d8%b1%d8%b3%d8%a7%d9%84%d8%a9-%d9%85%d8%a7%d8%ac%d8%b3%d8%aa%d9%8a%d8%b1-%d8%aa%d8%a8%d8%ad%d8%ab-%d9%81%d9%8a-%d8%aa%d8%ad%d8%b6%d9%8a%d8%b1-%d9%88-%d8%aa%d8%b4%d8%ae%d9%8a%d8%b5-%d8%a7%d9%84%d9%85","status":"publish","type":"post","link":"https:\/\/ihcoedu.uobaghdad.edu.iq\/?p=24055","title":{"rendered":"\u0631\u0633\u0627\u0644\u0629 \u0645\u0627\u062c\u0633\u062a\u064a\u0631 \u062a\u0628\u062d\u062b \u0641\u064a \u062a\u062d\u0636\u064a\u0631 \u0648 \u062a\u0634\u062e\u064a\u0635 \u0627\u0644\u0645\u0631\u0643\u0628\u0627\u062a \u0627\u0644\u062d\u0644\u0642\u064a\u0629 \u063a\u064a\u0631 \u0627\u0644\u0645\u062a\u062c\u0627\u0646\u0633\u0629 \u0627\u0644\u062c\u062f\u064a\u062f\u0629 \u0648\u062f\u0631\u0627\u0633\u0629 \u0646\u0634\u0627\u0637\u0647\u0627 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https:\/\/ihcoedu.uobaghdad.edu.iq\/wp-content\/uploads\/sites\/27\/2019\/02\/DSC_2029-768x512.jpg 768w\" sizes=\"auto, (max-width: 800px) 100vw, 800px\" \/><\/span><\/h4>\n<h4><\/h4>\n<h4 style=\"text-align: justify\"><span style=\"color: #000080\">\u0648\u064a\u0647\u062f\u0641 \u0627\u0644\u0628\u062d\u062b \u0627\u0644\u0649\u00a0<strong>\u062a\u062d\u0636\u064a\u0631 \u0628\u0639\u0636 \u0627\u0644\u0645\u0634\u062a\u0642\u0627\u062a \u0627\u0644\u062c\u062f\u064a\u062f\u0629 \u0644\u0640\u0645\u0631\u0643\u0628\u0627\u062a : \u0642\u0648\u0627\u0639\u062f \u0634\u064a\u0641 \u060c 3\u060c1- \u0623\u0648\u0643\u0632\u0627\u0632\u064a\u0628\u064a\u0646 \u060c \u0643\u0648\u0627\u064a\u0646\u0627\u0632\u0648\u0644\u064a\u0646 \u060c \u0623\u0648\u0643\u0632\u0627\u0632\u064a\u0646 \u060c \u062a\u062a\u0631\u0627\u0632\u0648\u0644 \u00a0\u0648 \u00a0\u062b\u0627\u064a\u0627\u0632\u0648\u0644\u064a\u062f\u064a\u0646\u00a0 \u0627\u0644\u0645\u0634\u062a\u0642\u0629 \u0645\u0646 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\u0639\u0646 \u0637\u0631\u064a\u0642 \u062a\u0641\u0627\u0639\u0644 \u063a\u0644\u0642 \u062d\u0644\u0642\u0629 \u0639\u0646\u062f \u062a\u0641\u0627\u0639\u0644 \u0642\u0648\u0627\u0639\u062f \u0634\u064a\u0641 \u00a0\u0645\u0639 2- \u0647\u064a\u062f\u0631\u0648\u0643\u0633\u064a \u062d\u0627\u0645\u0636 \u0627\u0644\u0628\u0646\u0632\u0648\u064a\u0643 \u0641\u064a \u0645\u0630\u064a\u0628 \u0627\u0644\u0628\u0646\u0632\u064a\u0646 \u0627\u0644\u062c\u0627\u0641 . \u00a0\u0623\u062e\u064a\u0631\u0627 \u060c \u0639\u0627\u0646\u062a \u0642\u0648\u0627\u0639\u062f \u0634\u064a\u0641 \u062a\u0641\u0627\u0639\u0644 \u062a\u0643\u0648\u064a\u0646 \u062d\u0644\u0642\u0629\u00a0 \u0645\u0639 2- \u0645\u0631\u0643\u0628\u062a\u0648 \u062d\u0627\u0645\u0636 \u0627\u0644\u062e\u0644\u064a\u0643 \u0627\u0648 \u0645\u0639 \u0623\u0632\u064a\u062f \u0627\u0644\u0635\u0648\u062f\u064a\u0648\u0645\u00a0 \u0641\u064a \u0645\u0630\u064a\u0628 \u0631\u0628\u0627\u0639\u064a \u0647\u064a\u062f\u0631\u0648\u0641\u064a\u0648\u0631\u0627\u0646(THF) \u00a0\u00a0\u0644\u062a\u0639\u0637\u064a \u0627\u0644\u0645\u0631\u0643\u0628\u0627\u062a \u0627\u0644\u0646\u0647\u0627\u0626\u064a\u0629.<\/span><\/h4>\n<p><img loading=\"lazy\" decoding=\"async\" class=\"aligncenter size-full wp-image-24058\" src=\"https:\/\/ihcoedu.uobaghdad.edu.iq\/wp-content\/uploads\/sites\/27\/2019\/02\/DSC_2030.jpg\" alt=\"\" width=\"800\" height=\"533\" srcset=\"https:\/\/ihcoedu.uobaghdad.edu.iq\/wp-content\/uploads\/sites\/27\/2019\/02\/DSC_2030.jpg 800w, https:\/\/ihcoedu.uobaghdad.edu.iq\/wp-content\/uploads\/sites\/27\/2019\/02\/DSC_2030-300x200.jpg 300w, https:\/\/ihcoedu.uobaghdad.edu.iq\/wp-content\/uploads\/sites\/27\/2019\/02\/DSC_2030-768x512.jpg 768w\" sizes=\"auto, (max-width: 800px) 100vw, 800px\" \/><\/p>\n<p>&nbsp;<\/p>\n<h4><span style=\"color: #000080\">\u0648\u062e\u0644\u0635\u062a \u0627\u0644\u0637\u0627\u0644\u0628\u0629 \u0641\u064a \u062e\u0627\u062a\u0645\u0629 \u0628\u062d\u062b\u0647\u0627 \u0627\u0644\u0649 \u0627\u0644\u062a\u0648\u0635\u064a\u0627\u062a \u0627\u0644\u062a\u0627\u0644\u064a\u0629 :<\/span><\/h4>\n<ol>\n<li>\n<h4><span style=\"color: #000080\"><strong>\u062f\u0631\u0627\u0633\u0629 \u0627\u0644\u062a\u0623\u062b\u064a\u0631\u0627\u062a \u0627\u0644\u062c\u0627\u0646\u0628\u064a\u0629 \u0648\u0627\u0644\u0633\u0645\u064a\u0651\u0629 \u0644\u0644\u0645\u0631\u0643\u0628\u0627\u062a \u0627\u0644\u0645\u062d\u0636\u0631\u0629 \u0644\u064a\u062a\u0645 \u062a\u062d\u0648\u064a\u0644\u0647\u0627\u00a0<\/strong><strong>\ufe87\u0644\u0649 \u0639\u0642\u0627\u0631 \u0641\u064a \u0627\u0644\u0645\u0633\u062a\u0642\u0628\u0644. <\/strong><\/span><\/h4>\n<\/li>\n<li>\n<h4><span style=\"color: #000080\"><strong>\u00a0<\/strong><strong>\u062f\u0631\u0627\u0633\u0629 \u062a\u0623\u062b\u064a\u0631 \u0627\u0644\u0645\u0631\u0643\u0628\u0627\u062a \u0627\u0644\u0645\u062d\u0636\u0631\u0629\u00a0 \u0636\u062f \u062e\u0644\u0627\u064a\u0627 \u0627\u0644\u0633\u0631\u0637\u0627\u0646.<\/strong><\/span><\/h4>\n<\/li>\n<li>\n<h4><span style=\"color: #000080\"><strong>\u00a0<\/strong><strong>\u062a\u062d\u0636\u064a\u0631 \u0645\u0634\u062a\u0642\u0627\u062a \u062c\u062f\u064a\u062f\u0629 \u0645\u0646 \u0642\u0648\u0627\u0639\u062f \u0634\u064a\u0641 \u0645\u062b\u0644 \u0627\u0644\u0623\u0632\u064a\u062a\u064a\u062f\u064a\u0646 \u060c \u0648 \u062f\u0631\u0627\u0633\u0629\u00a0<\/strong><strong>\u0627\u0644\u0641\u0639\u0627\u0644\u064a\u0629 \u0627\u0644\u0628\u064a\u0648\u0644\u0648\u062c\u064a\u0629 \u0644\u0647\u0627.<\/strong><\/span><\/h4>\n<\/li>\n<li>\n<h4><span style=\"color: #000080\"><strong>\u00a0<\/strong><strong>\u062f\u0631\u0627\u0633\u0629 \u0627\u0644\u062e\u0635\u0627\u0626\u0635 \u0627\u0644\u0628\u0644\u0648\u0631\u064a\u0629 \u0627\u0644\u0633\u0627\u0626\u0644\u0629 \u0644\u0647\u0630\u0647 \u0627\u0644\u0645\u0634\u062a\u0642\u0627\u062a.<\/strong><\/span><\/h4>\n<\/li>\n<\/ol>\n<p>&nbsp;<\/p>\n<h4><span style=\"color: #000080\">\u0648\u062d\u0635\u0644\u062a \u0627\u0644\u0637\u0627\u0644\u0628\u0629 \u0639\u0644\u0649 \u062a\u0642\u062f\u064a\u0631 (\u0627\u0645\u062a\u064a\u0627\u0632) \u0644\u062f\u0649 \u0645\u0646\u0627\u0642\u0634\u0629 \u0645\u062d\u062a\u0648\u064a\u0627\u062a \u0631\u0633\u0627\u0644\u062a\u0647\u0627 \u0648 \u0628\u062d\u062b\u0647\u0627 \u0645\u0646 \u0642\u0628\u0644 \u0627\u0639\u0636\u0627\u0621 \u0644\u062c\u0646\u0629 \u0627\u0644\u0645\u0646\u0627\u0642\u0634\u0629 \u0627\u0644\u0645\u062f\u0631\u062c\u0629 \u0627\u0633\u0645\u0627\u0626\u0647\u0645 \u0641\u064a\u0645\u0627 \u064a\u0644\u064a\u00a0 :<\/span><\/h4>\n<ol>\n<li>\n<h4><span style=\"color: #000080\">\u0623.\u062f. \u0627\u0633\u0627\u0645\u0629 \u0633\u0644\u0645\u0627\u0646 \u0639\u0628\u062f \u0627\u0644\u0631\u0632\u0627\u0642 ( \u0631\u0626\u064a\u0633\u0627)<\/span><\/h4>\n<\/li>\n<li>\n<h4><span style=\"color: #000080\">\u0623.\u062f. \u0631\u0633\u0645\u064a\u0629 \u0645\u062d\u0645\u0648\u062f \u0631\u0645\u064a\u0632 (\u0639\u0636\u0648\u0627)<\/span><\/h4>\n<\/li>\n<li>\n<h4><span style=\"color: #000080\">\u0623.\u0645.\u062f. \u0632\u064a\u0646\u0628 \u0639\u0628\u062f \u0627\u0644\u0631\u0632\u0627\u0642 \u062c\u0628\u0627\u0631\u0629 (\u0639\u0636\u0648\u0627)<\/span><\/h4>\n<\/li>\n<li>\n<h4><span style=\"color: #000080\">\u0623.\u0645.\u062f. \u0645\u064a\u0633\u0648\u0646 \u0637\u0627\u0631\u0642 \u062a\u0648\u0641\u064a\u0642 (\u0639\u0636\u0648\u0627 \u0648\u0645\u0634\u0631\u0641\u0627\u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0<\/span><\/h4>\n<\/li>\n<li style=\"text-align: left\">\n<hr \/>\n<h3><span style=\"color: #993366\">The department of Chemistry discussed MSc.thesis on Synthesis, Characterization of New Heterocyclic Compounds With Study Some of Their Biological Activity by Ranin Hashim Ridha supervised by Asst.prof.Dr.Maysoon Tariq Tawfeeq\u00a0<\/span><\/h3>\n<h3><span style=\"color: #993366\">The discussion committee<\/span><\/h3>\n<h3><span style=\"color: #993366\">Prof.Dr.Osama Salman AbdulRazak\u00a0\u00a0\u00a0 head<\/span><\/h3>\n<h3><span style=\"color: #993366\">Prof.Dr.Rasmia Mahmood Rameez \u00a0member<\/span><\/h3>\n<h3><span style=\"color: #993366\">Asst.prof.Dr. Zainab Abdulrazak Jibara\u00a0\u00a0 member<\/span><\/h3>\n<h3><span style=\"color: #993366\">Asst.prof.Dr.Maysoon Tariq Tawfeeq\u00a0\u00a0\u00a0 supervisor member<\/span><\/h3>\n<h3><span style=\"color: #993366\">The Abstract<\/span><\/h3>\n<h3 style=\"text-align: center\"><span style=\"color: #993366\">In this work a preliminary step was synthesis the oxadiazole derivative of 5- (3-nitrophenyl)-1,3,4-oxadiazole-2-thiol [3]\u00a0 by varied\u00a0 steps:\u00a0\u00a0 3-Nitrobenzoic acid\u00a0\u00a0 was successfully converted to ester [1] by reaction with thionyl chloride and thus to acid hydrazide [2] by reaction with hydrazine hydrate in absolute ethanol as a solvent. In addition, 5-(3-nitrophenyl)-1,3,4-oxadiazole-2-thiol [3] was produced when treated 3-nitrobenzoic acid hydrazide [2] with carbon disulphide (CS2) in an alcoholic potassium hydroxide solution , and reaction of compound [3] with chloroacetic acid in the base medium to give (thio substituted)-1,3,4-oxadiazole derivative [4], which was stirred with thiosemicarbazide and phosphoryl chloride (POCl3) in cyclization reaction to give the oxadiazole ring substituted with\u00a0 thiadiazole ring [5].\u00a0 Schiff\u2019s bases [6-11] were obtained via compound [5] intensification reaction with various aromatic aldehydes in absolute ethanol and some droplets of glacial acetic acid. In addition to synthesis of 1,3-oxazepein derivatives [12-25] from reaction of Schiff base derivatives[6-11] with succinic anhydride to give [12-14] or maleic anhydride to give [15-17] or phathlic anhydride to give [18-21] and 3-nitrophthalic anhydride to give [22-25]. On the other hand, Schiff&#8217;s bases were suffered cyclization reaction with 2-aminobenzoic acid in absolute ethanol to give compounds[26-30]. Also The derivatives of\u00a0 benzo[e][1,3]oxazine-4-one\u00a0 including 1,3,4-oxadiazole\u00a0 and\u00a0 1,3,4-thiadiazole\u00a0 rings [31-34]\u00a0 were prepared via\u00a0 ring-closure reaction of Schiff\u2019s bases [6-11] with 2-hydroxybenzoic\u00a0 acid in dry benzene\u00a0 solvent. Finally,the Schiff&#8217;s bases suffered from cyclization reactions with either 2-mercaptoacetic acid or sodium azide in THsolvent to give [35-37], and [38-42 respectively\u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0\u00a0<\/span><\/h3>\n<\/li>\n<\/ol>\n","protected":false},"excerpt":{"rendered":"<p>\u0646\u0627\u0642\u0634 \u0642\u0633\u0645 \u0627\u0644\u0643\u064a\u0645\u064a\u0627\u0621 \u0641\u064a \u0643\u0644\u064a\u0629 \u0627\u0644\u062a\u0631\u0628\u064a\u0629 \u0644\u0644\u0639\u0644\u0648\u0645 \u0627\u0644\u0635\u0631\u0641\u0629 (\u0627\u0628\u0646 \u0627\u0644\u0647\u064a\u062b\u0645) \u0631\u0633\u0627\u0644\u0629 \u0627\u0644\u0645\u0627\u062c\u0633\u062a\u064a\u0631 \u0627\u0644\u0645\u0648\u0633\u0648\u0645\u0629 ( \u062a\u062d\u0636\u064a\u0631, \u062a\u0634\u062e\u064a\u0635 \u0627\u0644\u0645\u0631\u0643\u0628\u0627\u062a \u0627\u0644\u062d\u0644\u0642\u064a\u0629 \u063a\u064a\u0631 \u0627\u0644\u0645\u062a\u062c\u0627\u0646\u0633\u0629&#8230;.<a class=\"cz_readmore\" href=\"https:\/\/ihcoedu.uobaghdad.edu.iq\/?p=24055\"><i class=\"fa fa-angle-left\" aria-hidden=\"true\"><\/i><span>\u0627\u0644\u0645\u0632\u064a\u062f<\/span><\/a><\/p>\n","protected":false},"author":25,"featured_media":24056,"comment_status":"closed","ping_status":"closed","sticky":false,"template":"","format":"standard","meta":{"_lmt_disableupdate":"","_lmt_disable":"","footnotes":""},"categories":[7,16],"tags":[23],"class_list":["post-24055","post","type-post","status-publish","format-standard","has-post-thumbnail","hentry","category-7","category-16","tag-ihcoedu"],"modified_by":"ihcoedu","_links":{"self":[{"href":"https:\/\/ihcoedu.uobaghdad.edu.iq\/index.php?rest_route=\/wp\/v2\/posts\/24055","targetHints":{"allow":["GET"]}}],"collection":[{"href":"https:\/\/ihcoedu.uobaghdad.edu.iq\/index.php?rest_route=\/wp\/v2\/posts"}],"about":[{"href":"https:\/\/ihcoedu.uobaghdad.edu.iq\/index.php?rest_route=\/wp\/v2\/types\/post"}],"author":[{"embeddable":true,"href":"https:\/\/ihcoedu.uobaghdad.edu.iq\/index.php?rest_route=\/wp\/v2\/users\/25"}],"replies":[{"embeddable":true,"href":"https:\/\/ihcoedu.uobaghdad.edu.iq\/index.php?rest_route=%2Fwp%2Fv2%2Fcomments&post=24055"}],"version-history":[{"count":0,"href":"https:\/\/ihcoedu.uobaghdad.edu.iq\/index.php?rest_route=\/wp\/v2\/posts\/24055\/revisions"}],"wp:featuredmedia":[{"embeddable":true,"href":"https:\/\/ihcoedu.uobaghdad.edu.iq\/index.php?rest_route=\/wp\/v2\/media\/24056"}],"wp:attachment":[{"href":"https:\/\/ihcoedu.uobaghdad.edu.iq\/index.php?rest_route=%2Fwp%2Fv2%2Fmedia&parent=24055"}],"wp:term":[{"taxonomy":"category","embeddable":true,"href":"https:\/\/ihcoedu.uobaghdad.edu.iq\/index.php?rest_route=%2Fwp%2Fv2%2Fcategories&post=24055"},{"taxonomy":"post_tag","embeddable":true,"href":"https:\/\/ihcoedu.uobaghdad.edu.iq\/index.php?rest_route=%2Fwp%2Fv2%2Ftags&post=24055"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}