{"id":27148,"date":"2019-06-27T21:05:36","date_gmt":"2019-06-27T18:05:36","guid":{"rendered":"http:\/\/ihcoedu.uobaghdad.edu.iq\/?p=27148"},"modified":"2019-06-27T21:07:45","modified_gmt":"2019-06-27T18:07:45","slug":"%d9%82%d8%b3%d9%85-%d8%a7%d9%84%d9%81%d9%8a%d8%b2%d9%8a%d8%a7%d8%a1-%d9%8a%d9%86%d8%a7%d9%82%d8%b4-%d8%b1%d8%b3%d8%a7%d9%84%d8%a9-%d9%85%d8%a7%d8%ac%d8%b3%d8%aa%d9%8a%d8%b1-%d8%aa%d8%a8%d8%ad%d8%ab-2","status":"publish","type":"post","link":"https:\/\/ihcoedu.uobaghdad.edu.iq\/?p=27148","title":{"rendered":"\u0642\u0633\u0645 \u0627\u0644\u0641\u064a\u0632\u064a\u0627\u0621 \u064a\u0646\u0627\u0642\u0634 \u0631\u0633\u0627\u0644\u0629 \u0645\u0627\u062c\u0633\u062a\u064a\u0631 \u062a\u062f\u0631\u0633 \u0628\u0639\u0636 \u062e\u0635\u0627\u0626\u0635 \u0628\u0644\u0648\u0631\u0629 \u0643\u0628\u0631\u064a\u062a\u0627\u062a \u062b\u0644\u0627\u062b\u064a \u0627\u0644\u0643\u0644\u0627\u064a\u0633\u064a\u0646 \u0627\u0644\u0646\u0642\u064a\u0629"},"content":{"rendered":"

<\/h4>\n

\u0646\u0627\u0642\u0634 \u0642\u0633\u0645 \u0627\u0644\u0641\u064a\u0632\u064a\u0627\u0621 \u0641\u064a \u0643\u0644\u064a\u0629 \u0627\u0644\u062a\u0631\u0628\u064a\u0629 \u0644\u0644\u0639\u0644\u0648\u0645 \u0627\u0644\u0635\u0631\u0641\u0629 (\u0627\u0628\u0646 \u0627\u0644\u0647\u064a\u062b\u0645) \u0631\u0633\u0627\u0644\u0629 \u0627\u0644\u0645\u0627\u062c\u0633\u062a\u064a\u0631 \u0627\u0644\u0645\u0648\u0633\u0648\u0645\u0629 (\u0627\u0644\u0646\u0645\u0627\u0621 \u0627\u0644\u0628\u0644\u0648\u0631\u064a \u0648\u062f\u0631\u0627\u0633\u0629 \u0628\u0639\u0636 \u062e\u0635\u0627\u0626\u0635 \u0628\u0644\u0648\u0631\u0629 \u0643\u0628\u0631\u064a\u062a\u0627\u062a \u062b\u0644\u0627\u062b\u064a \u0627\u0644\u0643\u0644\u0627\u064a\u0633\u064a\u0646 \u0627\u0644\u0646\u0642\u064a\u0629 \u0648\u0627\u0644\u0645\u0637\u0639\u0645\u0629 \u0627\u0644\u0645\u0646\u0645\u0627\u0629 \u0628\u062a\u0642\u0646\u064a\u0629 \u0627\u0644\u062a\u0628\u062e\u0631 \u0627\u0644\u0628\u0637\u064a\u0621) \u0644\u0644\u0637\u0627\u0644\u0628 (\u0645\u0627\u0647\u0631 \u062c\u0628\u0627\u0631 \u0627\u0628\u0631\u0627\u0647\u064a\u0645) \u0648 \u0627\u0644\u062a\u064a \u0627\u0646\u062c\u0632\u0647\u0627 \u0628\u0627\u0634\u0631\u0627\u0641 \u0627\u0644\u062a\u062f\u0631\u064a\u0633\u064a\u0629 \u0641\u064a \u0627\u0644\u0642\u0633\u0645 (\u0623.\u0645.\u062f. \u062a\u063a\u0631\u064a\u062f \u0645\u0633\u0644\u0645 \u0645\u0631\u064a\u0648\u0634).<\/span><\/h4>\n

\"\"<\/strong><\/span><\/h4>\n

\u0648\u0646\u0648\u0642\u0634\u062a \u0627\u0644\u0631\u0633\u0627\u0644\u0629 \u0639\u0644\u0649 \u0642\u0627\u0639\u0629 \u0627\u0644\u0645\u0646\u0627\u0642\u0634\u0627\u062a \u0641\u064a \u0627\u0644\u0642\u0633\u0645 \u0645\u0646 \u0642\u0628\u0644 \u0644\u062c\u0646\u0629 \u0627\u0644\u0645\u0646\u0627\u0642\u0634\u0629 \u0627\u0644\u0645\u062f\u0631\u062c\u0629 \u0627\u0633\u0645\u0627\u0626\u0647\u0645 \u0641\u064a \u0645\u0627 \u064a\u0644\u064a:<\/span><\/h4>\n

– \u0623.\u062f. \u0639\u0645\u0627\u062f \u062e\u0636\u064a\u0631 \u0639\u0628\u0627\u0633\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0 \u0631\u0626\u064a\u0633\u0627.<\/span><\/h4>\n

– \u0623.\u062f. \u0648\u062f\u0627\u062f \u062d\u0645\u062f\u064a \u062c\u0627\u0633\u0645\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0 \u0639\u0636\u0648\u0627.<\/span><\/h4>\n

– \u0623.\u0645.\u062f. \u0633\u0639\u0627\u062f \u062d\u0627\u0645\u062f \u0644\u0639\u064a\u0628\u064a\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0 \u0639\u0636\u0648\u0627.<\/span><\/h4>\n

– \u0623.\u0645.\u062f. \u062a\u063a\u0631\u064a\u062f \u0645\u0633\u0644\u0645 \u0645\u0631\u064a\u0648\u0634\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0 \u0639\u0636\u0648\u0627 \u0648\u0645\u0634\u0631\u0641\u0627.<\/span><\/h4>\n

\u00a0\"\"<\/strong><\/span><\/h4>\n

\u0648\u064a\u0647\u062f\u0641 \u0627\u0644\u0628\u062d\u062b \u0627\u0644\u0649 :<\/strong><\/span><\/h4>\n
    \n
  1. \n

    \u062a\u062d\u0636\u064a\u0631 \ufedb\ufe92\ufeae\ufef3\ufe98\ufe8e\ufe95 \ufe9b\ufefc\ufe9b\ufef2 \u0627\u0644\u0643\u0644\u0627\u064a\u0633\u064a\u0646 \u0627\u0644\u0646\u0642\u064a\u0629 (TGS) \u0628\u062a\u0641\u0627\u0639\u0644 \u0627\u0644\u0643\u0644\u0627\u0633\u064a\u0646 \u0645\u0639 \u062d\u0627\u0645\u0636 \u0627\u0644\u0643\u0628\u0631\u064a\u062a\u064a\u0643 \u0627\u0644\u0645\u0631\u0643\u0632.<\/span><\/h4>\n<\/li>\n
  2. \n

    \u0646\u0645\u0627\u0621 \u0628\u0644\u0648\u0631\u0627\u062a \ufedb\ufe92\ufeae\ufef3\ufe98\ufe8e\ufe95 \ufe9b\ufefc\ufe9b\ufef2 \u0627\u0644\u0643\u0644\u0627\u064a\u0633\u064a\u0646 \u0627\u0644\u0646\u0642\u064a\u0629 (TGS) \u0628\u062a\u0631\u0627\u0643\u064a\u0632 \u0645\u0648\u0644\u0627\u0631\u064a\u0629 \u0645\u062e\u062a\u0644\u0641\u0629 \u0648\u0627\u062e\u062a\u064a\u0627\u0631 \u0627\u0644\u062a\u0631\u0643\u064a\u0632 \u0627\u0644\u0623\u0641\u0636\u0644.<\/span><\/h4>\n<\/li>\n
  3. \n

    \u0646\u0645\u0627\u0621 \u0628\u0644\u0648\u0631\u0627\u062a \ufedb\ufe92\ufeae\ufef3\ufe98\ufe8e\ufe95 \ufe9b\ufefc\ufe9b\ufef2 \u0627\u0644\u0643\u0644\u0627\u064a\u0633\u064a\u0646 \u0627\u0644\u0646\u0642\u064a\u0629 \u0628\u0623\u0648\u0633\u0627\u0637 \u0630\u0627\u062a \u062f\u0631\u062c\u0627\u062a \u062d\u0645\u0648\u0636\u0629 \u0645\u062e\u062a\u0644\u0641\u0629.<\/span><\/h4>\n<\/li>\n
  4. \n

    \u0646\u0645\u0627\u0621 \u0628\u0644\u0648\u0631\u0627\u062a \ufedb\ufe92\ufeae\ufef3\ufe98\ufe8e\ufe95 \ufe9b\ufefc\ufe9b\ufef2 \u0627\u0644\u0643\u0644\u0627\u064a\u0633\u064a\u0646 (TGS) \u0627\u0644\u0645\u0637\u0639\u0645\u0629 \u0628\u0623\u064a\u0648\u0646\u064a \u0627\u0644\u0645\u0646\u063a\u0646\u064a\u0632 \u0648\u0627\u0644\u0623\u0644\u0648\u0645\u0646\u064a\u0648\u0645 \u0643\u0644 \u0639\u0644\u0649 \u0627\u0646\u0641\u0631\u0627\u062f.<\/span><\/h4>\n<\/li>\n
  5. \n

    \u0625\u062c\u0631\u0627\u0621 \u0641\u062d\u0635 XRD \u0644\u0644\u0628\u0644\u0648\u0631\u0627\u062a \u0627\u0644\u0646\u0642\u064a\u0629 \u0648\u0627\u0644\u0645\u0637\u0639\u0645\u0629 \u0644\u062f\u0631\u0627\u0633\u0629 \u0627\u0644\u062e\u0635\u0627\u0626\u0635 \u0627\u0644\u062a\u0631\u0643\u064a\u0628\u064a\u0629 \u0648\u0627\u0644\u062a\u0639\u0631\u0641 \u0639\u0644\u0649 \u0645\u0639\u0644\u0645\u0627\u062a \u0627\u0644\u0634\u0628\u064a\u0643\u0629 \u0648\u0627\u0644\u062a\u0631\u0643\u064a\u0628 \u0627\u0644\u0628\u0644\u0648\u0631\u064a \u0644\u0647\u0630\u0647 \u0627\u0644\u0628\u0644\u0648\u0631\u0627\u062a.<\/span><\/h4>\n<\/li>\n
  6. \n

    \u062f\u0631\u0627\u0633\u0629 \u0627\u0644\u0623\u0646\u0645\u0627\u0637 \u0627\u0644\u0627\u0647\u062a\u0632\u0627\u0632\u064a\u0629 \u0639\u0646 \u0637\u0631\u064a\u0642 \u0625\u062c\u0631\u0627\u0621 \u0627\u0644\u0645\u0633\u062d \u0627\u0644\u0637\u064a\u0641\u064a \u0644\u0644\u0628\u0644\u0648\u0631\u0627\u062a \u0627\u0644\u0645\u0646\u0645\u0627\u0629 \u0628\u062a\u0642\u0646\u064a\u0629 \u0627\u0644\u0627\u0634\u0639\u0629 \u062a\u062d\u062a \u0627\u0644\u062d\u0645\u0631\u0627\u0621 \u0628\u0645\u062d\u0648\u0644 \u0641\u0648\u0631\u064a\u0631. (FTIR)<\/span><\/h4>\n<\/li>\n
  7. \n

    \u062f\u0631\u0627\u0633\u0629 \u0645\u0645\u064a\u0632\u0627\u062a \u0647\u0630\u0647 \u0627\u0644\u0628\u0644\u0648\u0631\u0627\u062a \u0627\u0644\u0645\u0637\u0639\u0645\u0629 \u0627\u0644\u0646\u0627\u062a\u062c\u0629 \u0645\u0646 \u0639\u0645\u0644\u064a\u0629 \u0627\u0644\u062a\u0637\u0639\u064a\u0645 \u0645\u0646 \u062d\u064a\u062b \u0627\u0644\u0646\u0645\u0627\u0621 \u0648\u0627\u0644\u0647\u064a\u0623\u0629 \u0648\u0627\u0644\u0623\u0628\u0639\u0627\u062f.<\/span><\/h4>\n<\/li>\n
  8. \n

    \u062f\u0631\u0627\u0633\u0629 \u0627\u0644\u062e\u0635\u0627\u0626\u0635 \u0627\u0644\u0628\u0635\u0631\u064a\u0629 \u0628\u0627\u0639\u062a\u0645\u0627\u062f \u062a\u0642\u0646\u064a\u0629 UV-Visible.<\/span><\/h4>\n<\/li>\n
  9. \n

    \u0645\u0646\u0627\u0642\u0634\u0629 \u0627\u0644\u0646\u062a\u0627\u0626\u062c \u0648\u0627\u062f\u0631\u0627\u062c \u0627\u0647\u0645 \u0627\u0644\u0627\u0633\u062a\u0646\u062a\u0627\u062c\u0627\u062a.<\/span><\/h4>\n<\/li>\n<\/ol>\n

    \u00a0<\/strong><\/span><\/h4>\n

    \u062a\u0645 \u0641\u064a \u0641\u064a \u0647\u0630\u0627 \u0627\u0644\u0628\u062d\u062b \u062a\u062d\u0636\u064a\u0631 \u0643\u0628\u0631\u064a\u062a\u0627\u062a \u062b\u0644\u0627\u062b\u064a \u0627\u0644\u0643\u0644\u0627\u064a\u0633\u064a\u0646 (Triglycine sulphate) \u0639\u0646 \u0637\u0631\u064a\u0642 \u0625\u0630\u0627\u0628\u0629 25.5g \u0645\u0646 glycine \u0641\u064a \u0645\u062d\u0644\u0648\u0644 mL 8.5 \u0645\u0646 H2<\/sub>SO4<\/sub> \u0641\u064a \u00a0mL50 \u0645\u0646 \u0627\u0644\u0645\u0627\u0621 \u0627\u0644\u0644\u0627\u0627\u064a\u0648\u0646\u064a \u0648\u062a\u0645 \u062a\u0633\u062e\u064a\u0646\u0647 \u0639\u0646\u062f \u062f\u0631\u062c\u0629 \u062d\u0631\u0627\u0631\u0629 C\u00b050 . \u0648\u0628\u0639\u062f \u0647\u0630\u0647 \u0627\u0644\u0639\u0645\u0644\u064a\u0629 \u062a\u0645 \u0627\u0644\u062d\u0635\u0648\u0644 \u0639\u0644\u0649 \u0628\u0644\u0648\u0631\u0627\u062a \u0644\u064a\u0633\u062a \u0634\u0641\u0627\u0641\u0629 \u0648\u063a\u064a\u0631 \u0646\u0627\u0645\u064a\u0629 \u0628\u0634\u0643\u0644 \u062c\u064a\u062f \u0645\u0646 \u0643\u0628\u0631\u064a\u062a\u0627\u062a \u062b\u0644\u0627\u062b\u064a \u0627\u0644\u0643\u0644\u0627\u064a\u0633\u064a\u0646 (TGS). \u062a\u0645 \u0627\u0633\u062a\u0639\u0645\u0627\u0644\u0647\u0627 \u0644\u0627\u062d\u0642\u0627 \u0644\u0646\u0645\u0627\u0621 \u0627\u0644\u0628\u0644\u0648\u0631\u0627\u062a \u0627\u0644\u0645\u0637\u0644\u0648\u0628\u0629.<\/span><\/h4>\n

    \u00a0\u062a\u0645 \u0646\u0645\u0627\u0621 \u0628\u0644\u0648\u0631\u0627\u062a \u0643\u0628\u0631\u064a\u062a\u0627\u062a \u062b\u0644\u0627\u062b\u064a \u0627\u0644\u0643\u0644\u0627\u064a\u0633\u064a\u0646 \u0641\u064a \u062b\u0644\u0627\u062b \u0645\u062c\u0645\u0648\u0639\u0627\u062a \u0645\u062e\u062a\u0644\u0641\u0629 \u0645\u0646 \u062e\u0644\u0627\u0644 \u062a\u0642\u0646\u064a\u0629 \u0627\u0644\u062a\u0628\u062e\u0631 \u0627\u0644\u0628\u0637\u064a\u0621 (Slow Evaporation Method) \u0628\u0627\u0633\u062a\u0639\u0645\u0627\u0644 \u0627\u0644\u0645\u0627\u0621 \u0627\u0644\u0644\u0627\u0627\u064a\u0648\u0646\u064a \u0643\u0645\u0630\u064a\u0628 \u0641\u064a \u062f\u0631\u062c\u0629 \u062d\u0631\u0627\u0631\u0629 \u0627\u0644\u063a\u0631\u0641\u0629. \u062a\u0636\u0645\u0646\u062a \u0627\u0644\u0645\u062c\u0645\u0648\u0639\u0629 \u0627\u0644\u0627\u0648\u0644\u0649 \u0627\u0646\u0645\u0627\u0621 \u0628\u0644\u0648\u0631\u0627\u062a TGS \u0627\u0644\u0646\u0642\u064a\u0629 \u0628\u062e\u0645\u0633\u0629 \u062a\u0631\u0627\u0643\u064a\u0632 \u0645\u0648\u0644\u0627\u0631\u064a\u0629 \u0645\u062e\u062a\u0644\u0641\u0629 \u0647\u064a M (0.5,1,1.25,1.5,2). \u0623\u0645\u0627 \u0627\u0644\u0645\u062c\u0645\u0648\u0639\u0629 \u0627\u0644\u062b\u0627\u0646\u064a\u0629 \u0641\u062a\u0636\u0645\u0646\u062a \u0627\u0646\u0645\u0627\u0621 \u0628\u0644\u0648\u0631\u0627\u062a TGS \u0627\u0644\u0646\u0642\u064a\u0629 \u0645\u0639 \u062a\u063a\u064a\u064a\u0631 \u0627\u0644\u0648\u0633\u0637 \u0627\u0644\u062d\u0627\u0645\u0636\u064a \u0644\u0644\u0645\u062d\u0644\u0648\u0644 \u0625\u0630 \u0643\u0627\u0646\u062a \u062f\u0627\u0644\u0629 \u0627\u0644\u062d\u0627\u0645\u0636\u064a\u0629 (6\u060c5\u060c4\u060c3= pH). \u0623\u0645\u0627 \u0627\u0644\u0645\u062c\u0645\u0648\u0639\u0629 \u0627\u0644\u062b\u0640\u0627\u0644\u062b\u0629 \u0641\u062a\u0636\u0640\u0645\u0646\u062a \u0627\u0646\u0645\u0627\u0621 \u0628\u0644\u0648\u0631\u0627\u062a \u0643\u0628\u0631\u064a\u062a\u0627\u062a \u062b\u0644\u0627\u062b\u064a \u0627\u0644\u0643\u0644\u0627\u064a\u0633\u064a\u0646 TGS \u0645\u0637\u0639\u0645\u0629 \u0628\u0623\u064a\u0648\u0646\u064a \u0627\u0644\u0645\u0646\u063a\u0646\u064a\u0632 \u0648\u0627\u0644\u0627\u0644\u0648\u0645\u0646\u064a\u0648\u0645 \u0628\u0646\u0633\u0628 \u062a\u0637\u0639\u064a\u0645 \u0645\u062e\u062a\u0644\u0641\u0629 \u0647\u064a M(0.001,0.003,0.005,0.007,0.01) \u0643\u0644 \u0639\u0644\u0649 \u0627\u0646\u0641\u0631\u0627\u062f\u060c \u0648\u0641\u064a \u0643\u0644 \u0627\u0644\u062d\u0627\u0644\u0627\u062a \u062a\u0645 \u0646\u0645\u0627\u0621 \u0628\u0644\u0648\u0631\u0627\u062a TGS \u0627\u0644\u0646\u0642\u064a\u0629 \u0648\u0627\u0644\u0645\u0646\u0645\u0627\u0629 \u0641\u064a \u0623\u0648\u0633\u0627\u0637 \u062d\u0627\u0645\u0636\u064a\u0629 \u0648\u0627\u0644\u0645\u0637\u0639\u0645\u0629 \u0628\u0646\u062c\u0627\u062d \u0648\u0643\u0627\u0646\u062a \u0639\u062f\u064a\u0645\u0629 \u0627\u0644\u0644\u0648\u0646 \u0634\u0641\u0627\u0641\u0629 \u0648\u0630\u0627\u062a \u0627\u0628\u0639\u0627\u062f \u062c\u064a\u062f\u0629. \u0648\u062a\u0645 \u0627\u0644\u062a\u062d\u0642\u0642 \u0645\u0646 \u0645\u0639\u062f\u0644 \u0627\u0644\u0646\u0645\u0627\u0621 \u0627\u0644\u0634\u0627\u0645\u0644 \u0644\u062c\u0645\u064a\u0639 \u0627\u0644\u0628\u0644\u0648\u0631\u0627\u062a \u0627\u0644\u0645\u0646\u0645\u0627\u0629\u060c \u0648\u0648\u062c\u062f \u0627\u0646 \u0647\u0646\u0627\u0643 \u0639\u0644\u0627\u0642\u0629 \u0628\u064a\u0646 \u0646\u0633\u0628\u0629 \u062a\u0631\u0643\u064a\u0632 \u0627\u0644\u0645\u0648\u0644\u0627\u0631\u064a\u0629 \u0648\u0645\u0639\u062f\u0644 \u0627\u0644\u0646\u0645\u0627\u0621\u060c \u0625\u0630 \u0644\u0648\u062d\u0638 \u0627\u0646 \u0645\u062f\u0629 \u0627\u0644\u0646\u0645\u0627\u0621 \u062a\u0642\u0644 \u0645\u0639 \u0632\u064a\u0627\u062f\u0629 \u0627\u0644\u062a\u0631\u0643\u064a\u0632 \u0627\u0644\u0645\u0648\u0644\u0627\u0631\u064a\u0629 \u0643\u0645\u0627 \u0644\u0648\u062d\u0638 \u0623\u064a\u0636\u0627 \u0648\u062c\u0648\u062f \u0639\u0644\u0627\u0642\u0629 \u0628\u064a\u0646 \u0645\u0639\u062f\u0644 \u0627\u0644\u0646\u0645\u0627\u0621 \u0648\u0646\u0633\u0628\u0629 \u0627\u0644\u062a\u0637\u0639\u064a\u0645 \u0625\u0630 \u064a\u0632\u062f\u0627\u062f \u0645\u0639\u062f\u0644 \u0627\u0644\u0646\u0645\u0627\u0621 \u0628\u0632\u064a\u0627\u062f\u0629 \u0646\u0633\u0628 \u0627\u0644\u062a\u0637\u0639\u064a\u0645 \u0627\u0645\u0627 \u0627\u0644\u0628\u0644\u0648\u0631\u0627\u062a \u0627\u0644\u0645\u0646\u0645\u0627\u0629 \u0641\u064a \u0648\u0633\u0637 \u062d\u0627\u0645\u0636\u064a \u0641\u0644\u0648\u062d\u0638 \u0627\u0646 \u0645\u0639\u062f\u0644 \u0627\u0644\u0646\u0645\u0627\u0621 \u0648\u062c\u0648\u062f\u0629 \u0627\u0644\u0628\u0644\u0648\u0631\u0627\u062a \u064a\u0639\u062a\u0645\u062f \u0628\u0635\u0648\u0631\u0629 \u0648\u0627\u0636\u062d\u0629 \u0639\u0644\u0649 \u0627\u0644\u0631\u0642\u0645 \u0627\u0644\u0647\u064a\u062f\u0631\u0648\u062c\u064a\u0646\u064a (pH).<\/span><\/h4>\n

    \u062a\u0645 \u0627\u0644\u062a\u0623\u0643\u062f \u0645\u0646 \u0627\u0644\u062a\u0631\u0643\u064a\u0628 \u0627\u0644\u0628\u0644\u0648\u0631\u064a \u0644\u0628\u0644\u0648\u0631\u0627\u062a (TGS) \u0627\u0639\u062a\u0645\u0627\u062f\u0627 \u0639\u0644\u0649 \u0623\u0646\u0645\u0627\u0637 \u062d\u064a\u0648\u062f \u0627\u0644\u0627\u0634\u0639\u0629 \u0627\u0644\u0633\u064a\u0646\u064a\u0629 \u0648\u0648\u062c\u062f \u0623\u0646 \u062c\u0645\u064a\u0639 \u0627\u0644\u0628\u0644\u0648\u0631\u0627\u062a \u0627\u0644\u0646\u0642\u064a\u0629 \u0648\u0627\u0644\u0645\u0646\u0645\u0627\u0629 \u0641\u064a \u0648\u0633\u0637 \u062d\u0627\u0645\u0636\u064a \u0648\u0627\u0644\u0645\u0637\u0639\u0645\u0629 \u062a\u0646\u062a\u0645\u064a \u0644\u0646\u0638\u0627\u0645 \u0627\u062d\u0627\u062f\u064a \u0627\u0644\u0645\u064a\u0644 (monoclinic) \u0648\u0627\u0646 \u0642\u064a\u0645 \u0645\u0639\u0644\u0645\u0627\u062a \u0627\u0644\u0634\u0628\u064a\u0643\u0629 \u0627\u0644\u0628\u0644\u0648\u0631\u064a\u0629 \u062a\u062a\u0641\u0642 \u0645\u0639 \u0628\u0637\u0627\u0642\u0629 JCPDS (15 \u2013 0947). \u0648\u0643\u0627\u0646 \u062d\u062c\u0645 \u0627\u0643\u0628\u0631 \u0628\u0644\u0648\u0631\u0627\u062a \u0643\u0628\u0631\u064a\u062a\u0627\u062a \u062b\u0644\u0627\u062b\u064a \u0627\u0644\u0643\u0644\u0627\u064a\u0633\u064a\u0646 \u0627\u0644\u0646\u0642\u064a\u0629 (32.37\u00d724\u00d75.11) mm3 <\/sup>\u0648\u0645\u0639\u0644\u0640\u0645\u0627\u062a \u0627\u0644\u0634\u0640\u0628\u064a\u0643\u0629 \u0644\u0640\u0640\u0640\u0640\u0647\u0627 ( \u00c5, c=5.728\u00c512.652 =b (a=9.167\u00c5, \u00a0\u00a0.\u0627\u0645\u0627 \u0628\u0644\u0648\u0631\u0627\u062a TGS \u00a0\u0627\u0644\u0645\u0637\u0639\u0645\u0629 \u0628\u0623\u064a\u0648\u0646 \u0627\u0644\u0645\u0646\u063a\u0646\u064a\u0632 \u0641\u0643\u0627\u0646 \u062d\u062c\u0645 \u0627\u0643\u0628\u0631 \u0627\u0644\u0628\u0644\u0648\u0631\u0627\u062a \u0647\u0648 (31.80\u00d723.33\u00d73.91)mm3<\/sup> \u0648\u0645\u0639\u0644\u0645\u0627\u062a \u0627\u0644\u0634\u0628\u064a\u0643\u0629 \u0644\u0647\u0627 (a=9.161\u00c5, b=12.664\u00c5, c=5.759\u00c5). \u0627\u0645\u0627 \u0628\u0644\u0648\u0631\u0627\u062a TGS \u0627\u0644\u0645\u0637\u0639\u0645\u0629 \u0628\u0623\u064a\u0648\u0646 \u0627\u0644\u0627\u0644\u0648\u0645\u0646\u064a\u0648\u0645 \u0641\u0642\u062f \u0643\u0627\u0646 \u062d\u062c\u0645 \u0627\u0643\u0628\u0631 \u0627\u0644\u0628\u0644\u0648\u0631\u0627\u062a \u0647\u0648 (30.87\u00d712.47\u00d75.89) mm3<\/sup> \u0648\u0645\u0639\u0644\u0645\u0627\u062a \u0627\u0644\u0634\u0628\u064a\u0643\u0629 \u0644\u0647\u0627 (a=9.168\u00c5,b=12.757\u00c5, c=5.742\u00c5) \u0627\u0645\u0627 \u0628\u0644\u0648\u0631\u0627\u062a \u0643\u0628\u0631\u064a\u062a\u0627\u062a \u062b\u0644\u0627\u062b\u064a \u0627\u0644\u0643\u0644\u0627\u064a\u0633\u064a\u0646 \u0627\u0644\u0645\u0646\u0645\u0627\u0629 \u0641\u064a \u0648\u0633\u0637 \u062d\u0627\u0645\u0636\u064a \u0641\u0643\u0627\u0646 \u062d\u062c\u0645 \u0627\u0643\u0628\u0631 \u0627\u0644\u0628\u0644\u0648\u0631\u0627\u062a \u0647\u0648 (39.32\u00d722.49\u00d75.14) mm3<\/sup> \u0648\u0643\u0627\u0646\u062a \u0645\u0639\u0644\u0645\u0627\u062a \u0627\u0644\u0634\u0628\u064a\u0643\u0629 \u0644\u0647\u0627 (a=9.234\u00c5, b=12.624\u00c5, c=5.726\u00c5)\u060c \u0625\u0630 \u0644\u0648\u062d\u0638 \u0628\u0627\u0646 \u062d\u062c\u0645 \u062e\u0644\u064a\u0629 \u0627\u0644\u0648\u062d\u062f\u0629 \u0642\u062f \u0627\u0632\u062f\u0627\u062f \u0628\u0632\u064a\u0627\u062f\u0629 \u0646\u0633\u0628\u0629 \u0627\u0644\u062a\u0637\u0639\u064a\u0645.<\/span><\/h4>\n

    \u062a\u0645\u062a \u062f\u0631\u0627\u0633\u0629 \u0627\u0644\u062e\u0648\u0627\u0635 \u0627\u0644\u0628\u0635\u0631\u064a\u0629 \u0628\u0627\u0639\u062a\u0645\u0627\u062f \u062a\u062d\u0644\u064a\u0644 (UV-Vis) \u0648\u0623\u0638\u0647\u0631\u062a \u0627\u0644\u0646\u062a\u0627\u0626\u062c \u0627\u0646 \u0632\u064a\u0627\u062f\u0629 \u0627\u0644\u062a\u0631\u0643\u064a\u0632 \u0627\u0644\u0645\u0648\u0644\u0627\u0631\u064a \u0642\u062f \u0627\u062f\u062a \u0627\u0644\u0649 \u0632\u064a\u0627\u062f\u0629 \u0627\u0644\u0646\u0641\u0627\u0630\u064a\u0629 \u0644\u0644\u0628\u0644\u0648\u0631\u0627\u062a \u0627\u0644\u0646\u0642\u064a\u0629\u060c \u0627\u0645\u0627 \u0627\u0644\u0628\u0644\u0648\u0631\u0627\u062a \u0627\u0644\u0646\u0627\u0645\u064a\u0629 \u0641\u064a \u0648\u0633\u0637 \u062d\u0627\u0645\u0636\u064a \u0641\u0644\u0648\u062d\u0638 \u0632\u064a\u0627\u062f\u0629 \u0627\u0644\u0646\u0641\u0627\u0630\u064a\u0629 \u0628\u0646\u0642\u0635\u0627\u0646 \u0627\u0644\u0631\u0642\u0645 \u0627\u0644\u0647\u064a\u062f\u0631\u0648\u062c\u064a\u0646\u064a\u060c \u0627\u0645\u0627 \u0627\u0644\u0628\u0644\u0648\u0631\u0627\u062a \u0627\u0644\u0645\u0637\u0639\u0645\u0629 \u0641\u0642\u062f \u0648\u062c\u062f \u0627\u0646 \u0642\u064a\u0645 \u0627\u0644\u0627\u0645\u062a\u0635\u0627\u0635\u064a\u0629 \u0627\u0632\u062f\u0627\u062f\u062a \u0639\u0646\u062f \u0632\u064a\u0627\u062f\u0629 \u0646\u0633\u0628 \u0627\u0644\u062a\u0637\u0639\u064a\u0645\u060c \u0648\u0642\u062f \u0623\u0638\u0647\u0631\u062a \u062c\u0645\u064a\u0639 \u0627\u0644\u0628\u0644\u0648\u0631\u0627\u062a \u0627\u0645\u062a\u0635\u0627\u0635\u064a\u0629 \u0644\u0644\u0623\u0634\u0639\u0629 \u062a\u062d\u062a \u0627\u0644\u062d\u0645\u0631\u0627\u0621 \u0648\u0634\u0641\u0627\u0641\u064a\u0629 \u0639\u0627\u0644\u064a\u0629 \u0639\u0644\u0649 \u0637\u0648\u0644 \u0627\u0644\u0645\u0646\u0637\u0642\u0629 \u0627\u0644\u0645\u0631\u0626\u064a\u0629. \u0648\u062a\u0645\u062a \u062f\u0631\u0627\u0633\u0629 \u0627\u0644\u0623\u0646\u0645\u0627\u0637 \u0627\u0644\u0627\u0647\u062a\u0632\u0627\u0632\u064a\u0629 \u0644\u0644\u0628\u0644\u0648\u0631\u0627\u062a \u0627\u0644\u0645\u0646\u0645\u0627\u0629 \u0628\u062a\u0642\u0646\u064a\u0629 FTIR \u0648\u062a\u0645 \u0627\u0644\u0643\u0634\u0641 \u0639\u0646 \u0642\u0645\u0645 \u062a\u0639\u0648\u062f \u0644\u0623\u0648\u0627\u0635\u0631 (Mn+2<\/sup>) \u0643\u0645\u0627 \u0648\u062c\u062f \u0623\u0646 \u0623\u0637\u064a\u0627\u0641 \u0627\u0644\u0623\u0634\u0639\u0629 \u062a\u062d\u062a \u0627\u0644\u062d\u0645\u0631\u0627\u0621 \u0644\u0628\u0644\u0648\u0631\u0627\u062a TGS \u0627\u0644\u0645\u0637\u0639\u0645\u0629 \u062a\u0634\u0628\u0647 \u062a\u0644\u0643 \u0644\u0644\u0628\u0644\u0648\u0631\u0627\u062a \u063a\u064a\u0631 \u0627\u0644\u0645\u0637\u0639\u0645\u0629 \u0645\u0639 \u062d\u062f\u0648\u062b \u062a\u062d\u0648\u0644 \u0637\u0641\u064a\u0641 (shift) \u0645\u0645\u0627 \u064a\u0634\u064a\u0631 \u0625\u0644\u0649 \u0623\u0646\u0647\u0627 \u062a\u062a\u0634\u0627\u0628\u0647 \u0641\u064a \u0627\u0644\u062a\u0631\u0643\u064a\u0628 \u0627\u0644\u0628\u0644\u0648\u0631\u064a.<\/span><\/h4>\n

    \u0648\u062e\u0644\u0635 \u0627\u0644\u0628\u062d\u062b \u0627\u0644\u0649 \u0627\u0642\u062a\u0631\u0627\u062d \u0627\u0644\u0637\u0627\u0644\u0628 \u0645\u0627 \u064a\u0623\u062a\u064a :<\/strong><\/span><\/h4>\n
      \n
    1. \n

      \u0627\u0646\u0645\u0627\u0621 \u0628\u0644\u0648\u0631\u0627\u062a TGS \u0645\u0646 \u062e\u0644\u0627\u0644 \u062a\u0642\u0646\u064a\u0629 Sankaranarayanan\u2013Ramasamy (SR) method \u0648\u062f\u0631\u0627\u0633\u0629 \u0627\u0644\u062a\u063a\u064a\u0631\u0627\u062a.<\/span><\/h4>\n<\/li>\n
    2. \n

      \u0627\u0644\u062a\u0637\u0639\u064a\u0645 \u0628\u0623\u064a\u0648\u0646\u0627\u062a \u0627\u062e\u0631\u0649 \u0644\u0627\u0633\u062a\u0639\u0645\u0627\u0644\u0647\u0627 \u062d\u0633\u0628 \u0627\u0644\u0645\u0648\u0627\u0635\u0641\u0627\u062a \u0627\u0644\u062c\u064a\u062f\u0629.<\/span><\/h4>\n<\/li>\n
    3. \n

      \u0625\u062e\u0636\u0627\u0639 \u0628\u0644\u0648\u0631\u0627\u062a TGS \u0644\u0641\u062d\u0648\u0635\u0627\u062a \u0623\u062e\u0631\u0649 \u0645\u062b\u0644 \u0625\u062c\u0631\u0627\u0621 \u062a\u062d\u0644\u064a\u0644 TG \/ DTA \u0648 DSC \u0644\u062a\u062d\u0644\u064a\u0644 \u0627\u0644\u0627\u0633\u062a\u0642\u0631\u0627\u0631 \u0627\u0644\u062d\u0631\u0627\u0631\u064a<\/span><\/h4>\n<\/li>\n
    4. \n

      \u0646\u0645\u0627\u0621 \u0647\u0630\u0647 \u0627\u0644\u0628\u0644\u0648\u0631\u0627\u062a \u0628\u062a\u0631\u0627\u0643\u064a\u0632 \u0645\u0648\u0644\u0627\u0631\u064a\u0629 \u0648\u0627\u0648\u0633\u0627\u0637 \u062d\u0627\u0645\u0636\u064a\u0629 \u0623\u062e\u0631\u0649.<\/span><\/h4>\n<\/li>\n
    5. \n

      \u0627\u0646\u0645\u0627\u0621 \u0627\u0644\u0628\u0644\u0648\u0631\u0627\u062a \u0641\u064a \u0648\u0633\u0637 \u062f\u0631\u062c\u0629 \u062d\u0631\u0627\u0631\u062a\u0647 \u0627\u0648\u0637\u0623 \u0645\u0646 \u062f\u0631\u062c\u0629 \u062d\u0631\u0627\u0631\u0629 \u0627\u0644\u063a\u0631\u0641\u0629.<\/span><\/h4>\n<\/li>\n
    6. \n

      \u0627\u0646\u0645\u0627\u0621 \u0627\u0644\u0628\u0644\u0648\u0631\u0627\u062a \u0641\u064a \u0648\u0633\u0637 \u062f\u0631\u062c\u0629 \u062d\u0631\u0627\u0631\u062a\u0647 \u0627\u0639\u0644\u0649 \u0645\u0646 \u062f\u0631\u062c\u0629 \u062d\u0631\u0627\u0631\u0629 \u0643\u0648\u0631\u064a \u0644\u0628\u0644\u0648\u0631\u0629 TGS.<\/span><\/h4>\n<\/li>\n<\/ol>\n

      \"\"<\/span><\/h4>\n
      \n
      \n

      \u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0<\/span><\/h4>\n

      <\/h4>\n

      Crystal Growth and Study Some Properties of Pure and Doped Triglycine Sulphate Crystal Grown by Slow Evaporation Technique<\/span><\/h4>\n

      Assist. Prof. Dr. Tagreed Muslim Marush<\/span><\/h4>\n

      <\/h4>\n

      Initially, triglycine sulphate (TGS) was prepared by dissolving 25.5g of glycine in 8.5 ml of H2<\/sub>SO4<\/sub> in 50mL of De-ionized water and heated at 50\u00b0C. After this process, we got crystals that were not grown well from (TGS) and later used to grow the required crystals.<\/span><\/h4>\n

      Triglycine sulphate crystals were grown in three different groups through Slow Evaporation Method using De-ionized water as a solvent at room temperature. The first group included the crystals which grown of pure TGS crystals with five different molarity concentrations of (0.5, 1, 1.25, 1.5, 2) M. The second group included the crystals which grown of pure TGS crystals with a change in the acidic medium of the solution where the hydrogen exponent was (pH= 6\u060c5\u060c4\u060c3). The third group included those that grown of (TGS) crystals doped with manganese ions and aluminum ions with different doped ratio are of (0.001, 0.003, 0.005, 0.007, 0.01) M singly. In all cases, the pure TGS crystals that grown in deionized water and in acidic medium, and the doped crystals were grown successfully and was colorless, transparent and of proper dimensions. The overall growth rate of all growing crystals was verified and found there was a relationship between molar concentration and growth rate. It was observed that the growth time decreases with the increase of molar concentration.\u00a0 Also, It was noted that there is a relationship between the rate of growth and the ratio of doped. The rate of growth increases with the increase of the ratio of doped. For the crystals in the acidic medium, it was noted that the growth rate and the quality of the crystals depend clearly on the pH.<\/span><\/h4>\n

      The crystalline structure of the TGS crystals was confirmed by X-ray diffraction patterns, all pure crystals and that grew in the acidic medium were found to belong to the monoclinic system, and the values of the lattice parameters corresponding to the card JCPDS file No (15 \u2013 0947). The largest Size of pure (TGS) crystals was (31.80\u00d723.33\u00d73.91) mm3<\/sup>, and the parameters of the lattice (a=9.161\u00c5, b=12.664\u00c5, c=5.759\u00c5). As for TGS crystals doped with Manganese ions, the size of the largest crystals was (31.80\u00d723.33\u00d73.91) mm3<\/sup>, and the parameters of the lattice (a=9.161\u00c5, b=12.664\u00c5, c=5.759\u00c5). As for TGS crystals doped with Aluminum ions, the size of the largest crystals was (30.87\u00d712.47\u00d75.89) mm3<\/sup> and the parameters of the lattice (a=9.168\u00c5, b=12.757\u00c5, c=5.742\u00c5). It was observed that the size of the unit cell was increased by increasing the ratio of doped.<\/span><\/h4>\n

      The optical properties were studied using the UV-Vis analysis. The results showed that the increase of molar concentration resulted to increase transmittance of the pure crystals, and it is the same for the crystals which grew in acidic medium, the increase in transmittance by decreasing the hydrogen exponent (pH), as for the doped crystals, it was found that the values of absorption increased when the ratio of doped increased, all crystals have been shown absorption of infrared radiation and high transmittance along the visible region. The spectral patterns of the crystals grown were studied using FTIR technology and Mn ions peaks were detected, the infrared spectra of the TGS crystals were found to be similar to those of the un-doped crystals with a slight shift indicating that they were similar in crystalline structure.<\/span><\/h4>\n

      <\/h4>\n

      <\/h4>\n

      <\/h4>\n

      <\/h4>\n","protected":false},"excerpt":{"rendered":"

      \u0646\u0627\u0642\u0634 \u0642\u0633\u0645 \u0627\u0644\u0641\u064a\u0632\u064a\u0627\u0621 \u0641\u064a \u0643\u0644\u064a\u0629 \u0627\u0644\u062a\u0631\u0628\u064a\u0629 \u0644\u0644\u0639\u0644\u0648\u0645 \u0627\u0644\u0635\u0631\u0641\u0629 (\u0627\u0628\u0646 \u0627\u0644\u0647\u064a\u062b\u0645) \u0631\u0633\u0627\u0644\u0629 \u0627\u0644\u0645\u0627\u062c\u0633\u062a\u064a\u0631 \u0627\u0644\u0645\u0648\u0633\u0648\u0645\u0629 (\u0627\u0644\u0646\u0645\u0627\u0621 \u0627\u0644\u0628\u0644\u0648\u0631\u064a \u0648\u062f\u0631\u0627\u0633\u0629 \u0628\u0639\u0636 \u062e\u0635\u0627\u0626\u0635 \u0628\u0644\u0648\u0631\u0629 \u0643\u0628\u0631\u064a\u062a\u0627\u062a….<\/i>\u0627\u0644\u0645\u0632\u064a\u062f<\/span><\/a><\/p>\n","protected":false},"author":25,"featured_media":27151,"comment_status":"closed","ping_status":"closed","sticky":false,"template":"","format":"standard","meta":{"_lmt_disableupdate":"","_lmt_disable":"","footnotes":""},"categories":[7,16],"tags":[23],"class_list":["post-27148","post","type-post","status-publish","format-standard","has-post-thumbnail","hentry","category-7","category-16","tag-ihcoedu"],"modified_by":"ihcoedu","_links":{"self":[{"href":"https:\/\/ihcoedu.uobaghdad.edu.iq\/index.php?rest_route=\/wp\/v2\/posts\/27148","targetHints":{"allow":["GET"]}}],"collection":[{"href":"https:\/\/ihcoedu.uobaghdad.edu.iq\/index.php?rest_route=\/wp\/v2\/posts"}],"about":[{"href":"https:\/\/ihcoedu.uobaghdad.edu.iq\/index.php?rest_route=\/wp\/v2\/types\/post"}],"author":[{"embeddable":true,"href":"https:\/\/ihcoedu.uobaghdad.edu.iq\/index.php?rest_route=\/wp\/v2\/users\/25"}],"replies":[{"embeddable":true,"href":"https:\/\/ihcoedu.uobaghdad.edu.iq\/index.php?rest_route=%2Fwp%2Fv2%2Fcomments&post=27148"}],"version-history":[{"count":0,"href":"https:\/\/ihcoedu.uobaghdad.edu.iq\/index.php?rest_route=\/wp\/v2\/posts\/27148\/revisions"}],"wp:featuredmedia":[{"embeddable":true,"href":"https:\/\/ihcoedu.uobaghdad.edu.iq\/index.php?rest_route=\/wp\/v2\/media\/27151"}],"wp:attachment":[{"href":"https:\/\/ihcoedu.uobaghdad.edu.iq\/index.php?rest_route=%2Fwp%2Fv2%2Fmedia&parent=27148"}],"wp:term":[{"taxonomy":"category","embeddable":true,"href":"https:\/\/ihcoedu.uobaghdad.edu.iq\/index.php?rest_route=%2Fwp%2Fv2%2Fcategories&post=27148"},{"taxonomy":"post_tag","embeddable":true,"href":"https:\/\/ihcoedu.uobaghdad.edu.iq\/index.php?rest_route=%2Fwp%2Fv2%2Ftags&post=27148"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}