{"id":28231,"date":"2019-11-13T09:44:58","date_gmt":"2019-11-13T06:44:58","guid":{"rendered":"http:\/\/ihcoedu.uobaghdad.edu.iq\/?p=28231"},"modified":"2019-11-16T08:47:19","modified_gmt":"2019-11-16T05:47:19","slug":"%d9%82%d8%b3%d9%85-%d8%a7%d9%84%d9%83%d9%8a%d9%85%d9%8a%d8%a7%d8%a1-%d9%8a%d9%86%d8%a7%d9%82%d8%b4-%d8%b1%d8%b3%d8%a7%d9%84%d8%a9-%d9%85%d8%a7%d8%ac%d8%b3%d8%aa%d9%8a%d8%b1-%d8%aa%d8%a8%d8%ad%d8%ab-5","status":"publish","type":"post","link":"https:\/\/ihcoedu.uobaghdad.edu.iq\/?p=28231","title":{"rendered":"\u0642\u0633\u0645 \u0627\u0644\u0643\u064a\u0645\u064a\u0627\u0621 \u064a\u0646\u0627\u0642\u0634 \u0631\u0633\u0627\u0644\u0629 \u0645\u0627\u062c\u0633\u062a\u064a\u0631 \u062a\u0628\u062d\u062b \u0627\u0644\u062e\u0635\u0627\u0626\u0635 \u0648\u0627\u0644\u0646\u0634\u0627\u0637 \u0627\u0644\u0628\u064a\u0648\u0644\u0648\u062c\u064a \u0644\u0644\u0645\u0639\u0642\u062f\u0627\u062a \u0627\u0644\u0645\u0634\u062a\u0642\u0629 \u0645\u0646 \u0644\u064a\u0643\u0627\u0646\u062f\u0627\u062a \u0645\u0639 \u0630\u0631\u0627\u062a(N\u060cO\u060cS)"},"content":{"rendered":"

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\"\"<\/p>\n

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\u062d\u064a\u062b\u00a0 :\u00a0\u00a0\u00a0<\/span><\/h4>\n

HL1=R)-2-((4-(dimethylamino)phenyl)((2-nitrophenyl)amino)methyl)-5,5-dimethylcyclohexane-1,3-dione<\/span><\/h4>\n

\u0627\u0645\u0627 \u0627\u0644\u064a\u0643\u0627\u0646\u062f \u0627\u0644\u062b\u0627\u0646\u064a \u0641\u0647\u0648 (\u0642\u0627\u0639\u062f\u0629 \u0634\u0641) \u0648\u062d\u0636\u0631 \u0645\u0646 \u062a\u0641\u0627\u0639\u0644 \u0627\u0644\u064a\u0643\u0627\u0646\u062f \u0627\u0644\u0627\u0648\u0644 \u0645\u0639 \u0645\u0627\u062f\u0629 \u0627\u0644\u062b\u0627\u064a\u0648 \u0633\u0645\u064a \u0643\u0627\u0631\u0628\u0627\u0632\u0627\u064a\u062f \u0648 \u0628\u0646\u0633\u0628 \u0645\u0648\u0644\u064a\u0629 \u0645\u0642\u062f\u0627\u0631\u0647\u0627\u00a0 1:1 .\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0 \u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0<\/span><\/h4>\n

\u062d\u064a\u062b\u00a0 :\u00a0\u00a0\u00a0<\/span><\/h4>\n

H2L2=(E)-2-(2-((S)-(4-(dimethylamino)phenyl)((2 nitrophenyl)amino)methyl)-5,5-dimethyl-3-oxocyclohexylidene)hydrazine-1-carbothioamide<\/span><\/h4>\n

H2L2\u0648 \u00a0\u00a0\u00a0HL1<\/span><\/h4>\n

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\u00a0( CoII, NiII, CuII, ZnII\u00a0 and\u00a0\u00a0\u00a0 CdII)\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0<\/span><\/h4>\n

\u00a0\u00a0 \u0648\u0633\u0637\u00a0 \u0644\u0644\u062a\u0641\u0627\u0639\u0644. DMF\u00a0\u00a0\u00a0\u00a0 \u0648\u0630\u0644\u0643 \u0628\u0645\u0632\u062c \u0646\u0633\u0628 \u0645\u0648\u0644\u064a\u0629 \u0645\u0642\u062f\u0627\u0631\u0647\u0627 2:1 (\u0641\u0644\u0632: \u0644\u064a\u0643\u0627\u0646\u062f) \u0628\u0627\u0633\u062a\u062e\u062f\u0627\u0645<\/span><\/h4>\n

.HL1\u0627\u0644\u0635\u064a\u063a\u0629 \u0627\u0644\u0639\u0627\u0645\u0629 \u0644\u0645\u0639\u0642\u062f\u0627\u062a \u0627\u0644\u064a\u0643\u0627\u0646\u062f \u0627\u0644\u0627\u0648\u0644 \u00a0<\/span><\/h4>\n

\u00a0[M(HL1)2] where M= Co(II), Ni(II), Cu(II), Zn(II)\u00a0 and\u00a0 Cd(II)<\/span><\/h4>\n

.H2L2\u0627\u0644\u0635\u064a\u063a\u0629 \u0627\u0644\u0639\u0627\u0645\u0629 \u0644\u0645\u0639\u0642\u062f\u0627\u062a \u0627\u0644\u064a\u0643\u0627\u0646\u062f \u0627\u0644\u062b\u0627\u0646\u064a \u00a0<\/span><\/h4>\n

[M(H2L2) Cl2]\u00a0 where M= Co(II), Cu(II) Zn(II)\u00a0 and\u00a0 Cd(II)<\/span><\/h4>\n

\u00a0[M(H2L2)]Cl2\u00a0 where M= Ni(II)<\/span><\/h4>\n

\"\"<\/h4>\n

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\u0648\u0627\u0639\u062a\u0645\u0627\u062f\u0627 \u0639\u0644\u0649 \u0627\u0644\u0645\u0639\u0637\u064a\u0627\u062a \u0627\u0644\u062a\u062d\u0644\u064a\u0644\u064a\u0629 \u0648\u0627\u0644\u0637\u064a\u0641\u064a\u0629 \u062a\u0645 \u0627\u0642\u062a\u0631\u0627\u062d \u0627\u0644\u0627\u0634\u0643\u0627\u0644 \u0627\u0644\u0627\u062a\u064a\u0629:<\/span><\/h4>\n

1- \u0627\u0634\u0643\u0627\u0644 \u062b\u0645\u0627\u0646\u064a\u0629 \u0627\u0644\u0633\u0637\u0648\u062d \u0645\u0634\u0648\u0647\u0647 \u0628\u0627\u0644\u0646\u0633\u0628\u0629 \u0644\u0645\u0639\u0642\u062f\u0627\u062a \u0627\u0644\u064a\u0643\u0627\u0646\u062f \u0627\u0644\u0627\u0648\u0644 \u0645\u0639 \u062c\u0645\u064a\u0639 \u0627\u0644\u0627\u064a\u0648\u0646\u0627\u062a Co(II), Ni(II), Cu(II), Zn(II)\u00a0 and Cd(II)<\/span><\/h4>\n

2- \u0627\u0634\u0643\u0627\u0644 \u062b\u0645\u0627\u0646\u064a\u0629 \u0627\u0644\u0633\u0637\u0648\u062d \u0645\u0634\u0648\u0647\u0647 \u0628\u0627\u0644\u0646\u0633\u0628\u0629 \u0644\u0645\u0639\u0642\u062f\u0627\u062a \u0627\u0644\u0644\u064a\u0643\u0627\u0646\u062f \u0627\u0644\u062b\u0627\u0646\u064a \u0645\u0639 \u0627\u064a\u0648\u0646\u0627\u062a \u0627\u0644\u0627\u064a\u0648\u0646\u0627\u062a. Co(II) , Cu(II)<\/span><\/h4>\n

3- \u0634\u0643\u0644 \u0645\u0631\u0628\u0639 \u0645\u0633\u062a\u0648\u064a \u0628\u0627\u0644\u0646\u0633\u0628\u0629 \u0644\u0645\u0639\u0642\u062f\u0627\u062a \u0627\u0644\u0644\u064a\u0643\u0627\u0646\u062f \u0627\u0644\u062b\u0627\u0646\u064a \u0645\u0639 \u0627\u064a\u0648\u0646. Ni(II)<\/span><\/h4>\n

4- \u0634\u0643\u0644 \u0631\u0628\u0627\u0639\u064a \u0627\u0644\u0633\u0637\u0648\u062d \u0628\u0627\u0644\u0646\u0633\u0628\u0629 \u0644\u0645\u0639\u0642\u062f\u0627\u062a \u0627\u0644\u0644\u064a\u0643\u0627\u0646\u062f \u0627\u0644\u062b\u0627\u0646\u064a \u0645\u0639 \u0627\u064a\u0648\u0646\u0627\u062a. Zn(II) , Cd(II)<\/span><\/h4>\n

\u062a\u0645 \u062a\u0634\u062e\u064a\u0635 \u0627\u0644\u0641\u0639\u0627\u0644\u064a\u0629 \u0627\u0644\u0628\u0627\u064a\u0648\u0644\u0648\u062c\u064a\u0629 \u0644\u0643\u0644\u0627 \u0627\u0644\u0644\u0643\u0646\u062f\u064a\u0646 \u0645\u0639 \u0645\u0639\u0642\u062f\u0627\u062a\u0647\u0627 \u0627\u0644\u0641\u0644\u0632\u064a\u0629 \u0628\u0627\u0644\u0646\u0633\u0628\u0629 \u0644\u0646\u0648\u0639\u064a\u0646 \u0645\u0646 \u0627\u0644\u0628\u0643\u062a\u0631\u064a\u0627 :<\/span><\/h4>\n

\u00a0\u0645\u0648\u062c\u0628\u0629\u00a0 \u0644\u0635\u0628\u063a\u0629 : (Staphylococcus aureus and Bacillus stubtilis)<\/span><\/h4>\n

\u0648\u0633\u0627\u0644\u0628\u0629 \u0644\u0635\u0628\u063a\u0629: (Escherichia coli and Pseudomonas aeruginosa)<\/span><\/h4>\n

\u0648\u0643\u0630\u0644\u0643 \u0634\u062e\u0635\u062a \u0627\u0644\u0641\u0639\u0627\u0644\u064a\u0629 \u0627\u062a\u062c\u0627\u0647 \u0646\u0648\u0639\u064a\u0646 \u0645\u0646 \u0627\u0644\u0641\u0637\u0631\u064a\u0627\u062a \u0648\u0647\u064a \u00a0(Candida and Trichomoniasis)<\/span><\/h4>\n
\n

Synthesis, Structural Characterization, Thermal properties and Biological Activity of New Complexes Derived from Ligands with N, O and S Donor Atoms<\/span><\/h3>\n

By Nihad Kadhum Hassan<\/span><\/h3>\n

Supervised by Asst.prof.Dr.Enaam Ismail Hassan<\/span><\/h3>\n

Abstract<\/span><\/h3>\n

This research involved the preparation and characterization of two types of\u00a0 ligands and their metal complexes. The first ligand (Mannich-base) was prepared using calcium chloride, HCl and EtOH, which \u00a0were used as a catalyst and reaction medium, by mixing three components:4-dimethylaminobenzaldehyde\u00a0 with\u00a0 2-nitroaniline and dime done and molar ratios of 1: 1: 1<\/span><\/h3>\n

HL1=R)-2-((4-(dimethylamino)phenyl)((2-nitrophenyl)amino)methyl)-5,5-dimethylcyclohexane-1,3-dione<\/span><\/h3>\n

While the second ligand (Schiff-base) was prepared from \u00a0the reaction of the first ligand\u00a0 with thiosemicarbazide at \u00a0molar ratios of<\/span><\/h3>\n

Where:<\/span><\/h3>\n

H2L2=(E)-2-(2-((S)-(4-(dimethylamino)phenyl) nitrophenyl)amino)methyl)-5,5-dimethyl-oxocyclohexylidene)hydrazine-1-carbothioamide<\/span><\/h3>\n

<\/h3>\n

<\/h4>\n

<\/h4>\n","protected":false},"excerpt":{"rendered":"

\u0646\u0627\u0642\u0634 \u0642\u0633\u0645 \u0644\u0643\u064a\u0645\u064a\u0627\u0621 \u0641\u064a \u0643\u0644\u064a\u0629 \u0627\u0644\u062a\u0631\u0628\u064a\u0629 \u0644\u0644\u0639\u0644\u0648\u0645 \u0627\u0644\u0635\u0631\u0641\u0629 (\u0627\u0628\u0646 \u0627\u0644\u0647\u064a\u062b\u0645) \u0631\u0633\u0627\u0644\u0629 \u0627\u0644\u0645\u0627\u062c\u0633\u062a\u064a\u0631 \u0627\u0644\u0645\u0648\u0633\u0648\u0645\u0629 (\u0627\u0644\u062a\u062d\u0636\u064a\u0631 \u060c \u0627\u0644\u062a\u0634\u062e\u064a\u0635 \u0627\u0644\u0647\u064a\u0643\u0644\u064a \u060c \u0627\u0644\u062e\u0635\u0627\u0626\u0635 \u0627\u0644\u062d\u0631\u0627\u0631\u064a\u0629….<\/i>\u0627\u0644\u0645\u0632\u064a\u062f<\/span><\/a><\/p>\n","protected":false},"author":25,"featured_media":28232,"comment_status":"closed","ping_status":"closed","sticky":false,"template":"","format":"standard","meta":{"_lmt_disableupdate":"no","_lmt_disable":"","footnotes":""},"categories":[7,16],"tags":[23],"class_list":["post-28231","post","type-post","status-publish","format-standard","has-post-thumbnail","hentry","category-7","category-16","tag-ihcoedu"],"modified_by":"ihcoedu","_links":{"self":[{"href":"https:\/\/ihcoedu.uobaghdad.edu.iq\/index.php?rest_route=\/wp\/v2\/posts\/28231","targetHints":{"allow":["GET"]}}],"collection":[{"href":"https:\/\/ihcoedu.uobaghdad.edu.iq\/index.php?rest_route=\/wp\/v2\/posts"}],"about":[{"href":"https:\/\/ihcoedu.uobaghdad.edu.iq\/index.php?rest_route=\/wp\/v2\/types\/post"}],"author":[{"embeddable":true,"href":"https:\/\/ihcoedu.uobaghdad.edu.iq\/index.php?rest_route=\/wp\/v2\/users\/25"}],"replies":[{"embeddable":true,"href":"https:\/\/ihcoedu.uobaghdad.edu.iq\/index.php?rest_route=%2Fwp%2Fv2%2Fcomments&post=28231"}],"version-history":[{"count":0,"href":"https:\/\/ihcoedu.uobaghdad.edu.iq\/index.php?rest_route=\/wp\/v2\/posts\/28231\/revisions"}],"wp:featuredmedia":[{"embeddable":true,"href":"https:\/\/ihcoedu.uobaghdad.edu.iq\/index.php?rest_route=\/wp\/v2\/media\/28232"}],"wp:attachment":[{"href":"https:\/\/ihcoedu.uobaghdad.edu.iq\/index.php?rest_route=%2Fwp%2Fv2%2Fmedia&parent=28231"}],"wp:term":[{"taxonomy":"category","embeddable":true,"href":"https:\/\/ihcoedu.uobaghdad.edu.iq\/index.php?rest_route=%2Fwp%2Fv2%2Fcategories&post=28231"},{"taxonomy":"post_tag","embeddable":true,"href":"https:\/\/ihcoedu.uobaghdad.edu.iq\/index.php?rest_route=%2Fwp%2Fv2%2Ftags&post=28231"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}