{"id":28272,"date":"2019-11-16T08:26:51","date_gmt":"2019-11-16T05:26:51","guid":{"rendered":"http:\/\/ihcoedu.uobaghdad.edu.iq\/?p=28272"},"modified":"2019-11-17T12:16:16","modified_gmt":"2019-11-17T09:16:16","slug":"%d9%82%d8%b3%d9%85-%d8%a7%d9%84%d9%83%d9%8a%d9%85%d9%8a%d8%a7%d8%a1-%d9%8a%d9%86%d8%a7%d9%82%d8%b4-%d8%b1%d8%b3%d8%a7%d9%84%d8%a9-%d9%85%d8%a7%d8%ac%d8%b3%d8%aa%d9%8a%d8%b1-%d8%aa%d8%a8%d8%ad%d8%ab-7","status":"publish","type":"post","link":"https:\/\/ihcoedu.uobaghdad.edu.iq\/?p=28272","title":{"rendered":"\u0642\u0633\u0645 \u0627\u0644\u0643\u064a\u0645\u064a\u0627\u0621 \u064a\u0646\u0627\u0642\u0634 \u0631\u0633\u0627\u0644\u0629 \u0645\u0627\u062c\u0633\u062a\u064a\u0631 \u062a\u0628\u062d\u062b \u0641\u064a \u0627\u0644\u0641\u0639\u0627\u0644\u064a\u0629 \u0627\u0644\u0628\u0627\u064a\u0648\u0644\u0648\u062c\u064a\u0629 \u0644\u0642\u0648\u0627\u0639\u062f \u0634\u0641 \u062c\u062f\u064a\u062f\u0629 \u0648\u0645\u0639\u0642\u062f\u0627\u062a\u0647 \u0645\u0639 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https:\/\/ihcoedu.uobaghdad.edu.iq\/wp-content\/uploads\/sites\/27\/2019\/11\/DSC_4491-300x200.jpg 300w, https:\/\/ihcoedu.uobaghdad.edu.iq\/wp-content\/uploads\/sites\/27\/2019\/11\/DSC_4491-768x513.jpg 768w\" sizes=\"auto, (max-width: 800px) 100vw, 800px\" \/><\/p>\n<h4><span style=\"color: #000080\">\u0648\u0646\u0648\u0642\u0634\u062a \u0627\u0644\u0631\u0633\u0627\u0644\u0629 \u0645\u0646 \u0642\u0628\u0644 \u0627\u0644\u0630\u0648\u0627\u062a \u0627\u0639\u0636\u0627\u0621 \u0644\u062c\u0646\u0629 \u0627\u0644\u0645\u0646\u0627\u0642\u0634\u0629 \u0627\u0644\u0645\u062f\u0631\u062c\u0629 \u0627\u0633\u0645\u0627\u0626\u0647\u0645 \u0641\u064a\u0645\u0627 \u064a\u0644\u064a \u0639\u0644 \u0642\u0627\u0639\u0629 \u0627\u0644\u0645\u0631\u062d\u0648\u0645 (\u0623.\u062f. \u0641\u0647\u062f \u0627\u0644\u062c\u0628\u0648\u0631\u064a) :<\/span><\/h4>\n<ul>\n<li>\n<h4><span style=\"color: #000080\">\u0623.\u062f. \u0639\u0627\u0645\u0631 \u062c\u0628\u0627\u0631 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src=\"https:\/\/ihcoedu.uobaghdad.edu.iq\/wp-content\/uploads\/sites\/27\/2019\/11\/DSC_4481.jpg\" alt=\"\" width=\"800\" height=\"534\" srcset=\"https:\/\/ihcoedu.uobaghdad.edu.iq\/wp-content\/uploads\/sites\/27\/2019\/11\/DSC_4481.jpg 800w, https:\/\/ihcoedu.uobaghdad.edu.iq\/wp-content\/uploads\/sites\/27\/2019\/11\/DSC_4481-300x200.jpg 300w, https:\/\/ihcoedu.uobaghdad.edu.iq\/wp-content\/uploads\/sites\/27\/2019\/11\/DSC_4481-768x513.jpg 768w\" sizes=\"auto, (max-width: 800px) 100vw, 800px\" \/><\/p>\n<h4><span style=\"color: #000080\"><strong>\u0648\u064a\u0647\u062f\u0641 \u0627\u0644\u0628\u062d\u062b \u0627\u0644\u0649 :<\/strong><\/span><\/h4>\n<ul>\n<li>\n<h4><span style=\"color: #000080\">\u062a\u062d\u0636\u064a\u0631 \u0644\u064a\u0643\u0646\u062f\u064a\u0646 \u0642\u0648\u0627\u0639\u062f \u0634\u0641 \u0645\u0646 \u0645\u0641\u0627\u0639\u0644\u0629 \u0627\u0644\u0641\u0627\u0646\u0644\u064a\u0646 \u0645\u0639 3- \u0627\u0645\u064a\u0646\u0648 1- 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\u062a\u0634\u062e\u064a\u0635 \u0627\u0644\u0644\u064a\u0643\u0627\u0646\u062f\u064a\u0646 \u0628\u0648\u0627\u0633\u0637\u0629\u00a0 \u0627\u0644\u062a\u0642\u0646\u064a\u0627\u062a \u0627\u0644\u0637\u064a\u0641\u064a\u0629 \u0645\u062b\u0644 \u0627\u0637\u064a\u0627\u0641 \u0627\u0644\u0627\u0634\u0639\u0629\u00a0 \u062a\u062d\u062a \u0627\u0644\u062d\u0645\u0631\u0627\u0621 \u0648\u0641\u0648\u0642 \u0627\u0644\u0628\u0646\u0641\u0633\u062c\u064a\u0629 \u0648\u0627\u0644\u0645\u0631\u0626\u064a\u0629 \u0648\u00a0 \u0627\u0644\u0631\u0646\u064a\u0646 \u0627\u0644\u0646\u0648\u0648\u064a \u0627\u0644\u0645\u063a\u0646\u0627\u0637\u064a\u0633\u064a \u0644\u0644\u0628\u0631\u0648\u062a\u0648\u0646 \u0627\u0644\u062a\u062d\u0644\u064a\u0644 \u0627\u0644\u062f\u0642\u064a\u0642 \u0644\u0644\u0639\u0646\u0627\u0635\u0631 \u0648 \u0627\u0644\u0643\u062a\u0644\u0629 .<\/span><\/h4>\n<h4><span style=\"color: #000080\">\u0648 \u062a\u062a\u0623\u0644\u0641 \u0645\u0639\u0642\u062f\u0627\u062a \u0645\u062e\u062a\u0644\u0637\u0629 \u0627\u0644\u0644\u064a\u0643\u0627\u0646\u062f \u0645\u0646 \u0642\u0648\u0627\u0639\u062f \u0634\u0641 \u0648 \u062d\u0627\u0645\u0636 \u0627\u0644\u0627\u0646\u062b\u0631\u0627\u0646\u064a\u0644\u0643 \u0645\u0639 \u0623\u064a\u0648\u0646\u0627\u062a \u0628\u0639\u0636 \u0627\u0644\u0639\u0646\u0627\u0635\u0631 \u0645\u062b\u0644 M(II): Co \u0648Ni \u0648 Cu\u0648 Cd\u0648 Hg, \u0634\u062e\u0635\u062a \u0647\u0630\u0647 \u0627\u0644\u0645\u0639\u0642\u062f\u0627\u062a \u0628\u0648\u0627\u0633\u0637\u0629 \u0627\u0644\u062a\u062d\u0644\u064a\u0644 \u0627\u0644\u062f\u0642\u064a\u0642 \u0644\u0644\u0639\u0646\u0627\u0635\u0631 \u0648\u0627\u0644\u062a\u0648\u0635\u064a\u0644\u064a\u0629 \u0627\u0644\u0645\u0648\u0644\u0627\u0631\u064a\u0629 \u0648 \u0627\u0644\u0623\u0634\u0639\u0629 \u062a\u062d\u062a \u0627\u0644\u062d\u0645\u0631\u0627\u0621 \u0648\u0641\u0648\u0642 \u0627\u0644\u0628\u0646\u0641\u0633\u062c\u064a\u0629 \u0648\u0627\u0644\u0645\u0631\u0626\u064a\u0629 \u0648\u0627\u0644\u0627\u0645\u062a\u0635\u0627\u0635 \u0627\u0644\u0630\u0631\u064a \u0648\u0642\u064a\u0627\u0633 \u0627\u0644\u062d\u0633\u0627\u0633\u064a\u0629 \u0627\u0644\u0645\u063a\u0646\u0627\u0637\u064a\u0633\u064a\u0629 .<\/span><\/h4>\n<h4><span style=\"color: #000080\">\u0648\u0642\u062f \u0627\u0638\u0647\u0631\u062a \u0628\u064a\u0627\u0646\u0627\u062a \u0627\u0644\u0623\u0637\u064a\u0627\u0641 \u0628\u0627\u0646 \u0627\u0644\u0644\u064a\u0643\u0627\u0646\u062f\u064a\u0646 ( SB1\u0648 SB2) \u0645\u062a\u0639\u0627\u062f\u0644 \u062b\u0646\u0627\u0626\u064a \u0627\u0644\u0633\u0646 \u0648\u0645\u062a\u0646\u0627\u0633\u0642 \u0645\u0639 \u0627\u0644\u0627\u064a\u0648\u0646\u0627\u062a \u0627\u0644\u0641\u0644\u0632\u064a\u0629 \u0645\u0646 \u062e\u0644\u0627\u0644 \u0630\u0631\u0629 \u0627\u0644\u0646\u062a\u0631\u0648\u062c\u064a\u0646 \u0644\u0645\u062c\u0645\u0648\u0639\u0629 \u0627\u0644\u0627\u0632\u0648\u0645\u064a\u062b\u064a\u0646 \u0648\u0630\u0631\u0629 \u0627\u0644\u0646\u062a\u0631\u0648\u062c\u064a\u0646 \u0644\u062d\u0644\u0642\u0629 \u0627\u0644\u0628\u0627\u064a\u0631\u0632\u0648\u0644 \u0648\u0627\u0644\u0634\u0643\u0644 \u0627\u0644\u0645\u062a\u0648\u0642\u0639 \u0644\u0643\u0644 \u0627\u0644\u0645\u0639\u0642\u062f\u0627\u062a \u0647\u0648 \u0627\u0644\u062b\u0645\u0627\u0646\u064a \u0627\u0644\u0633\u0637\u0648\u062d .<\/span><\/h4>\n<h4><span style=\"color: #000080\">\u0648\u0623\u062e\u064a\u0631\u0627 \u062a\u0645 \u0627\u062e\u062a\u0628\u0627\u0631 \u0627\u0644\u0641\u0639\u0627\u0644\u064a\u0629 \u0627\u0644\u0628\u0627\u064a\u0648\u0644\u0648\u062c\u064a\u0629 \u0627\u0644\u0645\u0636\u0627\u062f\u0629 \u0644\u0644\u0628\u0643\u062a\u0631\u064a\u0627 \u062a\u062c\u0627\u0647 Staphylococcus aureus \u0648 Escherichia coli \u0644\u0644\u064a\u0643\u0627\u0646\u062f\u0627\u062a \u0648\u0645\u0639\u0642\u062f\u0627\u062a\u0647\u0627 \u0628\u062a\u0642\u0646\u064a\u0629 \u0642\u064a\u0627\u0633 \u0645\u0646\u0637\u0642\u0629 \u0627\u0644\u062a\u062b\u0628\u064a\u0637 (ZI)\u00a0\u00a0 ..<\/span><\/h4>\n<h4><\/h4>\n<h4><span style=\"color: #000080\">\u0648\u0641\u064a \u062e\u062a\u0627\u0645 \u0631\u0633\u0627\u0644\u062a\u0647 \u0627\u0648\u0635\u0649 \u0627\u0644\u0637\u0627\u0644\u0628 \u0628\u0627\u0644\u062a\u0648\u0635\u064a\u0627\u062a \u0627\u0644\u062a\u0627\u0644\u064a\u0629 :<\/span><\/h4>\n<ol>\n<li>\n<h4><span style=\"color: #000080\">\u062a\u062d\u0636\u064a\u0631 \u0645\u0639\u0642\u062f\u0627\u062a \u0628\u0627\u0633\u062a\u062e\u0627\u0645 \u0627\u0645\u0644\u0627\u062d \u0641\u0644\u0632\u064a\u0629 \u062c\u062f\u064a\u062f\u0629<\/span><\/h4>\n<\/li>\n<li>\n<h4><span style=\"color: #000080\">\u0627\u0633\u062a\u062e\u062f\u0627\u0645 \u0642\u0648\u0627\u0639\u062f \u0634\u0641 \u0641\u064a \u0627\u0644\u0643\u064a\u0645\u064a\u0627\u0621 \u0627\u0644\u062a\u062d\u0644\u064a\u0644\u064a\u0629 \u0648\u0641\u064a \u062a\u0642\u062f\u064a\u0631 \u0627\u064a\u0648\u0646\u0627\u062a \u0627\u0644\u0641\u0644\u0632\u064a\u0629<\/span><\/h4>\n<\/li>\n<li>\n<h4><span style=\"color: #000080\">\u062f\u0631\u0627\u0633\u0629 \u0627\u0644\u062a\u062d\u0644\u064a\u0644 \u0627\u0644\u062d\u0631\u0627\u0631\u064a \u0644\u0644\u064a\u0643\u0627\u0646\u062f\u0627\u062a \u0642\u0648\u0627\u0639\u062f \u0634\u0641 \u0648\u0645\u0639\u0642\u062f\u0627\u062a\u0647\u0627<\/span><\/h4>\n<\/li>\n<li>\n<h4><span style=\"color: #000080\">\u062f\u0631\u0627\u0633\u0629 \u0627\u0644\u0641\u0639\u0627\u0644\u064a\u0629 \u0627\u0644\u0628\u0643\u062a\u0631\u064a\u0629 \u0644\u0642\u0648\u0627\u0639\u062f \u0634\u0641 \u0648\u0645\u0639\u0642\u062f\u0627\u062a\u0647\u0627\u00a0 \u00a0\u00a0<\/span><\/h4>\n<hr \/>\n<\/li>\n<\/ol>\n<h4 style=\"direction: ltr\"><\/h4>\n<h4 style=\"direction: ltr\"><span style=\"color: #000080\">Synthesis, Characterization and Biological Activity Study of New Schiff Bases Ligands and Its Complexes with Some Metal Ions<\/span><\/h4>\n<h4 style=\"direction: ltr\"><span style=\"color: #000080\">salam kareem sahib ali<\/span><\/h4>\n<h4 style=\"direction: ltr\"><span style=\"color: #000080\"><strong>Supervisor:<\/strong> Dr. Lekaa Khalid Abdul Karem<\/span><\/h4>\n<h4 style=\"direction: ltr\"><span style=\"color: #000080\"><strong>Title<\/strong>: Assistant professor<\/span><\/h4>\n<h4 style=\"direction: ltr\"><span style=\"color: #000080\">\u00a0<strong>Aim of the work<\/strong><\/span><\/h4>\n<ul>\n<li>\n<h4 style=\"direction: ltr\"><span style=\"color: #000080\">Synthesize the Schiff base SB1 that is derived from vanillin with 3-Amino-1-phenyl-2-pyrazoline-5-one.<\/span><\/h4>\n<\/li>\n<li>\n<h4 style=\"direction: ltr\"><span style=\"color: #000080\">Synthesize the Schiff base SB2 that is derived from 4-(dimethyl amino) benzalaldehyde with 3-Amino-1-phenyl-2-pyrazoline-5-one.<\/span><\/h4>\n<\/li>\n<li>\n<h4 style=\"direction: ltr\"><span style=\"color: #000080\">Characterize the synthesized ligands SB1 and SB2 by the use of elemental micro analysis (C.H.N.), FT-IR, 1H-NMR, UV\u2013Vis, GC-MS and study they anti-bacterial activity that is tested against gram negative and gram-positive bacteria.<\/span><\/h4>\n<\/li>\n<li>\n<h4 style=\"direction: ltr\"><span style=\"color: #000080\">Preparing mixed ligand compounds of Co(II), Ni(II), Cu(II), Cd(II) and Hg(II) ions with Schiff bases SB1 and SB2 considered as the primary ligand and (A) considered as the secondary ligand.<\/span><\/h4>\n<\/li>\n<li>\n<h4 style=\"direction: ltr\"><span style=\"color: #000080\">Characterizing the prepared mixed ligands complexes by the use of elemental micro analysis (C.H.N.), UV\u2013Vis, FT-IR, magnetic measurements as well as studying the anti-bacterial activity, that is tested against gram negative and gram positive bacteria.<\/span><\/h4>\n<\/li>\n<\/ul>\n<h4 style=\"direction: ltr\"><span style=\"color: #000080\"><strong>Abstract<\/strong><\/span><\/h4>\n<h4 style=\"direction: ltr\"><span style=\"color: #000080\">\u00a0\u00a0 This study deals with Schiff base ligands derivative from (3-Amino-1-phenyl-2-pyrazoline-5-one) with 4-Hydroxy-3-methoxybenzaldehyde to create ligand (SB1) and 4-(Dimethylamino) benzaldehyde to create ligand (SB2).<\/span><\/h4>\n<h4 style=\"direction: ltr\"><span style=\"color: #000080\">\u00a0\u00a0 The two ligands were characterized by spectroscopic techniques such as infrared, ultraviolet, 1H NMR and element analysis, mass spectrometry.<\/span><\/h4>\n<h4 style=\"direction: ltr\"><span style=\"color: #000080\">Mixed ligands complexes were composed of Schiff bases and Anthranillic acid with some transition elements ions M (II) such as: Co, Ni, Cu, Cd and Hg. These complexes were identified by elemental micro-analysis, molar conductivity, infrared, ultraviolet-visible, atomic absorption, and magnetic susceptibility measurement.<\/span><\/h4>\n<h4 style=\"direction: ltr\"><\/h4>\n<h4 style=\"direction: ltr\"><span style=\"color: #000080\">The spectral data showed that the ligands SB1 and SB2 as a neutral bi dentate and consistent with metal ions through the N atom of the azomethine group and the N atom for pyrazole ring. The expected geometric shape is the octahedral for all complexes.<\/span><\/h4>\n<h4 style=\"direction: ltr\"><span style=\"color: #000080\">Finally, the biological antibacterial efficiency of the ligands and their complexes was tested from Staphylococcus aureus and Escherichia coli by the measurement of the inhibition zone (ZI).<\/span><\/h4>\n","protected":false},"excerpt":{"rendered":"<p>\u0646\u0627\u0642\u0634 \u0642\u0633\u0645 \u0627\u0644\u0643\u064a\u0645\u064a\u0627\u0621 \u0641\u064a \u0643\u0644\u064a\u0629 \u0627\u0644\u062a\u0631\u0628\u064a\u0629 \u0644\u0644\u0639\u0644\u0648\u0645 \u0627\u0644\u0635\u0631\u0641\u0629 (\u0627\u0628\u0646 \u0627\u0644\u0647\u064a\u062b\u0645) \u0631\u0633\u0627\u0644\u0629 \u0627\u0644\u0645\u0627\u062c\u0633\u062a\u064a\u0631 \u0627\u0644\u0645\u0648\u0633\u0648\u0645\u0629 (\u062a\u062d\u0636\u064a\u0631\u060c \u062a\u0634\u062e\u064a\u0635 \u0648\u062f\u0631\u0627\u0633\u0629 \u0627\u0644\u0641\u0639\u0627\u0644\u064a\u0629 \u0627\u0644\u0628\u064a\u0648\u0644\u0648\u062c\u064a\u0629 \u0644\u0644\u064a\u0643\u0627\u0646\u062f\u0627\u062a \u0642\u0648\u0627\u0639\u062f&#8230;.<a class=\"cz_readmore\" href=\"https:\/\/ihcoedu.uobaghdad.edu.iq\/?p=28272\"><i class=\"fa fa-angle-left\" aria-hidden=\"true\"><\/i><span>\u0627\u0644\u0645\u0632\u064a\u062f<\/span><\/a><\/p>\n","protected":false},"author":25,"featured_media":28274,"comment_status":"closed","ping_status":"closed","sticky":false,"template":"","format":"standard","meta":{"_lmt_disableupdate":"no","_lmt_disable":"","footnotes":""},"categories":[7,16],"tags":[23],"class_list":["post-28272","post","type-post","status-publish","format-standard","has-post-thumbnail","hentry","category-7","category-16","tag-ihcoedu"],"modified_by":"ihcoedu","_links":{"self":[{"href":"https:\/\/ihcoedu.uobaghdad.edu.iq\/index.php?rest_route=\/wp\/v2\/posts\/28272","targetHints":{"allow":["GET"]}}],"collection":[{"href":"https:\/\/ihcoedu.uobaghdad.edu.iq\/index.php?rest_route=\/wp\/v2\/posts"}],"about":[{"href":"https:\/\/ihcoedu.uobaghdad.edu.iq\/index.php?rest_route=\/wp\/v2\/types\/post"}],"author":[{"embeddable":true,"href":"https:\/\/ihcoedu.uobaghdad.edu.iq\/index.php?rest_route=\/wp\/v2\/users\/25"}],"replies":[{"embeddable":true,"href":"https:\/\/ihcoedu.uobaghdad.edu.iq\/index.php?rest_route=%2Fwp%2Fv2%2Fcomments&post=28272"}],"version-history":[{"count":0,"href":"https:\/\/ihcoedu.uobaghdad.edu.iq\/index.php?rest_route=\/wp\/v2\/posts\/28272\/revisions"}],"wp:featuredmedia":[{"embeddable":true,"href":"https:\/\/ihcoedu.uobaghdad.edu.iq\/index.php?rest_route=\/wp\/v2\/media\/28274"}],"wp:attachment":[{"href":"https:\/\/ihcoedu.uobaghdad.edu.iq\/index.php?rest_route=%2Fwp%2Fv2%2Fmedia&parent=28272"}],"wp:term":[{"taxonomy":"category","embeddable":true,"href":"https:\/\/ihcoedu.uobaghdad.edu.iq\/index.php?rest_route=%2Fwp%2Fv2%2Fcategories&post=28272"},{"taxonomy":"post_tag","embeddable":true,"href":"https:\/\/ihcoedu.uobaghdad.edu.iq\/index.php?rest_route=%2Fwp%2Fv2%2Ftags&post=28272"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}