{"id":32684,"date":"2020-06-27T00:54:14","date_gmt":"2020-06-26T21:54:14","guid":{"rendered":"http:\/\/ihcoedu.uobaghdad.edu.iq\/?p=32684"},"modified":"2020-09-23T10:19:21","modified_gmt":"2020-09-23T07:19:21","slug":"%d9%82%d8%b3%d9%85-%d8%a7%d9%84%d9%83%d9%8a%d9%85%d9%8a%d8%a7%d8%a1-%d9%8a%d9%86%d8%a7%d9%82%d8%b4-%d8%b1%d8%b3%d8%a7%d9%84%d8%a9-%d9%85%d8%a7%d8%ac%d8%b3%d8%aa%d9%8a%d8%b1-%d8%aa%d8%a8%d8%ad%d8%ab-17","status":"publish","type":"post","link":"https:\/\/ihcoedu.uobaghdad.edu.iq\/?p=32684","title":{"rendered":"\u0642\u0633\u0645 \u0627\u0644\u0643\u064a\u0645\u064a\u0627\u0621 \u064a\u0646\u0627\u0642\u0634 \u0631\u0633\u0627\u0644\u0629 \u0645\u0627\u062c\u0633\u062a\u064a\u0631 \u062a\u0628\u062d\u062b \u0641\u064a \u0627\u0644\u062a\u0642\u062f\u064a\u0631 \u0627\u0644\u0637\u064a\u0641\u064a \u0644\u0639\u0642\u0627\u0631\u064a \u0627\u0644\u0645\u064a\u062a\u0648\u0643\u0644\u0648\u0628\u0631\u0627\u0645\u0627\u064a\u062f 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https:\/\/ihcoedu.uobaghdad.edu.iq\/wp-content\/uploads\/sites\/27\/2020\/06\/DSC_0134-768x512.jpg 768w\" sizes=\"auto, (max-width: 800px) 100vw, 800px\" \/><\/h4>\n<h4 style=\"text-align: justify\"><span style=\"color: #000080\">\u0646\u0627\u0642\u0634 \u0642\u0633\u0645 \u0627\u0644\u0643\u064a\u0645\u064a\u0627\u0621 \u0641\u064a \u0643\u0644\u064a\u0629 \u0627\u0644\u062a\u0631\u0628\u064a\u0629 \u0644\u0644\u0639\u0644\u0648\u0645 \u0627\u0644\u0635\u0631\u0641\u0629 (\u0627\u0628\u0646 \u0627\u0644\u0647\u064a\u062b\u0645) \u0631\u0633\u0627\u0644\u0629 \u0627\u0644\u0645\u0627\u062c\u0633\u062a\u064a\u0631 \u0627\u0644\u0645\u0648\u0633\u0648\u0645\u0629 (\u062f\u0631\u0627\u0633\u0629 \u0637\u064a\u0641\u064a\u0629 \u0644\u062a\u0642\u062f\u064a\u0631 \u0639\u0642\u0627\u0631\u064a \u0627\u0644\u0645\u064a\u062a\u0648\u0643\u0644\u0648\u0628\u0631\u0627\u0645\u0627\u064a\u062f \u0647\u064a\u062f\u0631\u0648\u0643\u0644\u0648\u0631\u0627\u064a\u062f 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\u0647\u064a\u062f\u0631\u0648\u0643\u0644\u0648\u0631\u0627\u064a\u062f \u0648520.50 \u0646\u0627\u0646\u0648\u0645\u064a\u062a\u0631 \u0644\u0644\u0643\u0627\u0631 \u0641\u064a\u062f\u0648\u0644 \u0647\u064a\u062f\u0631\u0648\u0643\u0644\u0648\u0631\u0627\u064a\u062f \u0645\u0642\u0627\u0628\u0644 \u0645\u062d\u0627\u0644\u064a\u0644\u0647\u0627 \u0627\u0644\u0635\u0648\u0631\u064a\u0629.<\/span><\/h4>\n<h4 style=\"text-align: justify\"><span style=\"color: #000080\">\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0 \u062f\u0631\u0633\u062a \u00a0\u0627\u0644\u0639\u062f\u064a\u062f \u0645\u0646\u00a0 \u0627\u0644\u0639\u0648\u0627\u0645\u0644 \u0627\u0644\u062a\u064a \u062a\u0624\u062b\u0631 \u0639\u0644\u0649 \u0627\u062a\u0645\u0627\u0645 \u0627\u0644\u062a\u0641\u0627\u0639\u0644 \u0628\u0639\u0646\u0627\u064a\u0629\u00a0 \u0644\u0644\u062d\u0635\u0648\u0644 \u0639\u0644\u0649 \u0627\u0644\u0638\u0631\u0648\u0641 \u0627\u0644\u0641\u0636\u0644\u0649 \u0644\u0644\u062a\u0641\u0627\u0639\u0644\u0627\u062a \u062f\u0644\u062a \u0627\u0644\u0646\u062a\u0627\u0626\u062c \u0648\u0627\u0644\u0628\u064a\u0627\u0646\u0627\u062a \u0627\u0644\u0627\u062d\u0635\u0627\u0626\u064a\u0629 \u0639\u0644\u0649 \u0627\u0646 \u0627\u0644\u062e\u0635\u0627\u0626\u0635 \u0627\u0644\u0637\u064a\u0641\u064a\u0629 \u0644\u0645\u0646\u062d\u0646\u064a\u0627\u062a \u0627\u0644\u0645\u0639\u0627\u064a\u0631\u0629 \u0643\u0627\u0646\u062a \u0627\u0641\u0636\u0644 \u0639\u0646\u062f \u0627\u062a\u0628\u0627\u0639 \u0627\u0644\u0638\u0631\u0648\u0641 \u0627\u0644\u0645\u062b\u0644\u0649 \u0627\u0644\u062a\u064a \u062a\u0645 \u0627\u0644\u062d\u0635\u0648\u0644 \u0639\u0644\u064a\u0647\u0627.<\/span><\/h4>\n<h4 style=\"text-align: justify\"><span style=\"color: #000080\">\u0648\u062c\u062f\u062a \u0637\u0631\u064a\u0642\u0629 \u0645\u0637\u0627\u0648\u0639\u0629 \u0644\u0642\u0627\u0646\u0648\u0646 \u0644\u0627 \u0645\u0628\u0631\u062a- \u0628\u064a\u0631 \u0639\u0644\u0649 \u0645\u062f\u0649 \u0645\u0646 \u0627\u0644\u062a\u0631\u0643\u064a\u0632 \u064a\u062a\u0631\u0627\u0648\u062d 0.2 &#8211; 25\u00a0\u00a0\u00a0 \u0645\u0627\u064a\u0643\u0631\u0648\u063a\u0631\u0627\u0645.\u0645\u0644-1 \u00a0\u0644\u0643\u0644\u0627 \u0627\u0644\u0639\u0642\u0627\u0631\u064a\u0646 \u0648\u0645\u0639\u0627\u0645\u0644 \u0627\u0644\u0627\u0645\u062a\u0635\u0627\u0635 \u0627\u0644\u0645\u0648\u0644\u0627\u0631\u064a2.313\u00d7310 \u0644\u062a\u0631.\u0645\u0648\u0644-1.\u0633\u0645-1 \u0644\u0639\u0642\u0627\u0631 \u0627\u0644\u0645\u064a\u062a\u0648\u0643\u0644\u0648\u0631\u0648\u0628\u0631\u0648\u0645\u0627\u064a\u062f \u0647\u064a\u062f\u0631\u0648\u0643\u0644\u0648\u0631\u0627\u064a\u062f \u0648 103\u00d72.516 \u0644\u0639\u0642\u0627\u0631 \u0627\u0644\u0643\u0627\u0631\u0641\u064a\u062f\u064a\u0644\u0648\u0644 \u0647\u064a\u062f\u0631\u0648\u0643\u0644\u0648\u0631\u0627\u064a\u062f \u062a\u0645 \u062a\u062d\u062f\u064a\u062f \u062d\u062f\u0648\u062f \u0627\u0644\u0643\u0634\u0641 \u0648\u0648\u062c\u062f \u0627\u0646 \u00a00.1820 \u0645\u0627\u064a\u0643\u0631\u0648\u063a\u0631\u0627\u0645.\u0645\u0644-1 \u0644\u0639\u0642\u0627\u0631 \u0627\u0644\u0645\u064a\u062a\u0648\u0643\u0644\u0648\u0631\u0648\u0628\u0631\u0648\u0645\u0627\u064a\u062f \u0647\u064a\u062f\u0631\u0648\u0643\u0644\u0648\u0631\u0627\u064a\u062f \u0648 0.1422 \u0645\u0627\u064a\u0643\u0631\u0648\u063a\u0631\u0627\u0645.\u0645\u0644-1 \u0644\u0639\u0642\u0627\u0631 \u0627\u0644\u0643\u0627\u0631 \u0641\u064a\u062f\u064a\u0644\u0648\u0644 \u0647\u064a\u062f\u0631\u0648\u0643\u0644\u0648\u0631\u0627\u064a\u062f.<\/span><\/h4>\n<h4 style=\"text-align: justify\"><span style=\"color: #000080\">\u00a0\u00a0\u00a0\u00a0\u00a0 \u0627\u0633\u062a\u062e\u062f\u0645\u062a \u0637\u0631\u064a\u0642\u0629 \u0627\u0644\u0645\u062a\u063a\u064a\u0631\u0627\u062a \u0627\u0644\u0645\u0633\u062a\u0645\u0631\u0629 \u0648\u0627\u0644\u0646\u0633\u0628 \u0627\u0644\u0645\u0648\u0644\u064a\u0629 \u0644\u0645\u0639\u0631\u0641\u0629 \u062a\u0643\u0627\u0641\u0624\u064a\u0629 \u0627\u0644\u0645\u0639\u0642\u062f\u0627\u062a \u0627\u0644\u0645\u062a\u0643\u0648\u0646\u0629 \u0648\u0648\u062c\u062f \u0627\u0646 \u0646\u0633\u0628\u0629 \u0627\u0644\u0643\u0627\u0634\u0641 \u0627\u0644\u0649 \u0627\u0644\u0639\u0642\u0627\u0631 \u0647\u064a 1:1 \u0644\u062c\u0645\u064a\u0639 \u0627\u0644\u062a\u0641\u0627\u0639\u0644\u0627\u062a .<\/span><\/h4>\n<h4 style=\"text-align: justify\"><span style=\"color: #000080\">\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0 \u00a0\u0627\u0638\u0647\u0631\u062a \u0627\u0644\u062f\u0631\u0627\u0633\u0629 \u0639\u062f\u0645 \u0648\u062c\u0648\u062f \u0627\u064a \u062a\u0623\u062b\u064a\u0631 \u0644\u0644\u0645\u062a\u062f\u0627\u062e\u0644\u0627\u062a \u0627\u0644\u0645\u062a\u0639\u0627\u0631\u0641 \u0639\u0644\u0649 \u0648\u062c\u0648\u062f\u0647\u0627 \u0641\u064a \u0627\u0644\u0645\u0633\u062a\u062d\u0636\u0631\u0627\u062a \u0627\u0644\u0635\u064a\u062f\u0644\u0627\u0646\u064a\u0629 \u0641\u064a \u062a\u0642\u062f\u064a\u0631 \u0627\u0644\u0639\u0642\u0627\u0631\u064a\u0646 \u0627\u0644\u0645\u0630\u0643\u0648\u0631\u0629 , \u0644\u0630\u0644\u0643 \u0637\u0628\u0642\u062a \u0627\u0644\u0637\u0631\u064a\u0642\u0629 \u0627\u0644\u0645\u0642\u062a\u0631\u062d\u0629 \u0628\u0646\u062c\u0627\u062d \u0641\u064a \u062a\u0642\u062f\u064a\u0631 \u0627\u0644\u0639\u0642\u0627\u0631\u064a \u0644\u0645\u0633\u062a\u062d\u0636\u0631\u0627\u062a\u0647\u0627 \u0627\u0644\u0635\u064a\u062f\u0644\u0627\u0646\u064a\u0629\u00a0\u00a0 .<\/span><\/h4>\n<h3 style=\"text-align: left\"><\/h3>\n<hr \/>\n<h3 style=\"text-align: left\"><span style=\"color: #993366\">Spectrophotometric study for\u00a0 the determination of metoclopramide hydrochloride\u00a0 and carvedilol hydrochloride drugs in pure and pharmaceutical preparation<\/span><\/h3>\n<h3 style=\"text-align: left\"><span style=\"color: #993366\">summary<\/span><\/h3>\n<h3 style=\"text-align: left\"><span style=\"color: #993366\">Two different\u00a0 spectrophotometric method in this study were used for the determination of metoclopramide hydrochloride and carvedilol hydrochloride drugs in their pure form and pharmaceutical preparations . The suggested methods is rapid ,simple, sensitive ,accurate and inexpensive.\u00a0 The study includes show as follows:<\/span><\/h3>\n<h3 style=\"text-align: left\"><span style=\"color: #993366\">Chapter one :\u00a0 This chapter include a brief\u00a0 for ultraviolet \u2013 Visible(Uv-Vis) absorption spectroscopy, antiemetic drugs and anti-Hypertensive drugs\u00a0 it also shows some information about the two drugs that determined in this study with their general properties and literature survey of both drugs\u00a0<\/span><\/h3>\n<h3 style=\"text-align: left\"><span style=\"color: #993366\">Chapter two : oxidative coupling reaction<\/span><\/h3>\n<h3 style=\"text-align: left\"><span style=\"color: #993366\">This chapter include reaction of the two studied drugs with reagent 2,4-dinitrophenyl hydrazine (2,4-DNPHz) in the presence of potassium periodate\u00a0 and sodium hydroxide\u00a0 to from colored products. The maximum absorption\u00a0 (\u028emax)\u00a0 was determined at 404 nm for metoclopramide hydrochloride complex and 487 nm for carvedilol hydrochloride complex against reagent\u00a0 blank. Different\u00a0 variables effecting\u00a0\u00a0 the a compliment of the reaction were carefully optimized by\u00a0 varying the parameters one at a time and controlling all other\u2019s fixed. The results show better optical characteristics for calibration\u00a0 curve and statistical analysis\u2019s\u00a0 under optimum conditions.<\/span><\/h3>\n<h3 style=\"text-align: left\"><span style=\"color: #993366\">The results of this study showed that two\u00a0 drugs were estimated and compliance to the law of beer \u2013lambert . The range of concentration of metoclopramide hydrochloride drug\u00a0 complex between (1-35) \u00b5g.mL-1 and the value of molar absorptivity 7.263\u00d7103\u00a0\u00a0 L.mol-1.cm-1 and detection<\/span><\/h3>\n<h3 style=\"text-align: left\"><span style=\"color: #993366\">limit 0.6430 \u00b5g.ml-1.As well the linear range\u00a0 of\u00a0 carvedilol hydrochloride drug complex\u00a0 concentration between (1-35) \u00b5g.ml-1 and the value of molar absorptivity was equal 6.556\u00d7103 L.mol-1.cm-1 and\u00a0 detection limit is equal to 0.2092 \u00b5g.ml-1.<\/span><\/h3>\n<h3 style=\"text-align: left\"><span style=\"color: #993366\">The stoichiometry of the formed complexes were examined adopting continuous variation (Job\u2019s) and mole ratio methods ,it was found to be 1:1 (drug: reagent) for all reaction.<\/span><\/h3>\n<h3 style=\"text-align: left\"><span style=\"color: #993366\">No interference of the studied excipients were observed in the estimation of the cited drugs. Therefore, the suggested\u00a0 method was applied successfully for the determination\u00a0\u00a0 of the two cited drugs in their pharmaceutical preparation.<\/span><\/h3>\n<h3 style=\"text-align: left\"><span style=\"color: #993366\">Chapter three: Diazotization coupling reaction<\/span><\/h3>\n<h3 style=\"text-align: left\"><span style=\"color: #993366\">It depended on the reaction of the studied drugs with the diazonium salt of \u03c1-nitroaniline (which attended by the reaction of \u03c1-nitroaniline with sodium nitrite in the presence of hydrochloric acid) in alkaline medium to form colored azo-dye products .The maximum\u00a0 absorption for the formed azo-dye compounds was measured at 515.50nm\u00a0 for metoclopramide hydrochloride and\u00a0 520.50 nm for carvedilol hydrochloride against\u00a0 reagent\u00a0 blank<\/span><\/h3>\n<h3 style=\"text-align: left\"><span style=\"color: #993366\">The optimum reaction and other analytical parameters were evaluated .The results show\u00a0 better optical characteristics\u00a0 for calibration curve\u00a0 and statistical data under optimum conditions<\/span><\/h3>\n<h3 style=\"text-align: left\"><span style=\"color: #993366\">Bear\u2019s \u2013 lambert law is obeyed in the concentration range of\u00a0\u00a0 (0.2- 25) \u00b5g.mL-1 for two drugs, with molar absorptivity 2.313\u00d7103 L.mol-1.cm-1 for metoclopramide hydrochloride drug and 2.516\u00d7103 L.mol-1.cm-1 for<\/span><\/h3>\n<h3 style=\"text-align: left\"><span style=\"color: #993366\">carvedilol hydrochloride drug .Detection limits were determined and found to be 0.1820 \u00b5g.mL-1 for metoclopramide hydrochloride\u00a0 drug and 0.1422 \u00b5g .mL-1\u00a0\u00a0 for carvedilol hydrochloride<\/span><\/h3>\n<h3 style=\"text-align: left\"><span style=\"color: #993366\">The stoichiometry of the formed complexes were studied by adopting mole ratio and continuous variation (Job\u2019s) methods and it was found to be 1: 1 (drug: reagent) for all reaction<\/span><\/h3>\n<h3 style=\"text-align: left\"><span style=\"color: #993366\">No interference of the studied excipients were found in the determination of these drugs, therefore, the proposed method was applied successfully for the determination of the two cited drugs in their pharmaceutical preparation<\/span><\/h3>\n<p>&nbsp;<\/p>\n","protected":false},"excerpt":{"rendered":"<p>\u0646\u0627\u0642\u0634 \u0642\u0633\u0645 \u0627\u0644\u0643\u064a\u0645\u064a\u0627\u0621 \u0641\u064a \u0643\u0644\u064a\u0629 \u0627\u0644\u062a\u0631\u0628\u064a\u0629 \u0644\u0644\u0639\u0644\u0648\u0645 \u0627\u0644\u0635\u0631\u0641\u0629 (\u0627\u0628\u0646 \u0627\u0644\u0647\u064a\u062b\u0645) \u0631\u0633\u0627\u0644\u0629 \u0627\u0644\u0645\u0627\u062c\u0633\u062a\u064a\u0631 \u0627\u0644\u0645\u0648\u0633\u0648\u0645\u0629 (\u062f\u0631\u0627\u0633\u0629 \u0637\u064a\u0641\u064a\u0629&#8230;.<a class=\"cz_readmore\" href=\"https:\/\/ihcoedu.uobaghdad.edu.iq\/?p=32684\"><i class=\"fa fa-angle-left\" aria-hidden=\"true\"><\/i><span>\u0627\u0644\u0645\u0632\u064a\u062f<\/span><\/a><\/p>\n","protected":false},"author":25,"featured_media":32687,"comment_status":"closed","ping_status":"closed","sticky":false,"template":"","format":"standard","meta":{"_lmt_disableupdate":"no","_lmt_disable":"","footnotes":""},"categories":[44,7,16],"tags":[23,47],"class_list":["post-32684","post","type-post","status-publish","format-standard","has-post-thumbnail","hentry","category-44","category-7","category-16","tag-ihcoedu","tag-chem"],"modified_by":"ihcoedu","_links":{"self":[{"href":"https:\/\/ihcoedu.uobaghdad.edu.iq\/index.php?rest_route=\/wp\/v2\/posts\/32684","targetHints":{"allow":["GET"]}}],"collection":[{"href":"https:\/\/ihcoedu.uobaghdad.edu.iq\/index.php?rest_route=\/wp\/v2\/posts"}],"about":[{"href":"https:\/\/ihcoedu.uobaghdad.edu.iq\/index.php?rest_route=\/wp\/v2\/types\/post"}],"author":[{"embeddable":true,"href":"https:\/\/ihcoedu.uobaghdad.edu.iq\/index.php?rest_route=\/wp\/v2\/users\/25"}],"replies":[{"embeddable":true,"href":"https:\/\/ihcoedu.uobaghdad.edu.iq\/index.php?rest_route=%2Fwp%2Fv2%2Fcomments&post=32684"}],"version-history":[{"count":0,"href":"https:\/\/ihcoedu.uobaghdad.edu.iq\/index.php?rest_route=\/wp\/v2\/posts\/32684\/revisions"}],"wp:featuredmedia":[{"embeddable":true,"href":"https:\/\/ihcoedu.uobaghdad.edu.iq\/index.php?rest_route=\/wp\/v2\/media\/32687"}],"wp:attachment":[{"href":"https:\/\/ihcoedu.uobaghdad.edu.iq\/index.php?rest_route=%2Fwp%2Fv2%2Fmedia&parent=32684"}],"wp:term":[{"taxonomy":"category","embeddable":true,"href":"https:\/\/ihcoedu.uobaghdad.edu.iq\/index.php?rest_route=%2Fwp%2Fv2%2Fcategories&post=32684"},{"taxonomy":"post_tag","embeddable":true,"href":"https:\/\/ihcoedu.uobaghdad.edu.iq\/index.php?rest_route=%2Fwp%2Fv2%2Ftags&post=32684"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}