{"id":44472,"date":"2022-06-20T13:26:27","date_gmt":"2022-06-20T10:26:27","guid":{"rendered":"https:\/\/ihcoedu.uobaghdad.edu.iq\/?p=44472"},"modified":"2023-06-28T18:36:51","modified_gmt":"2023-06-28T15:36:51","slug":"%d9%82%d8%b3%d9%85-%d8%a7%d9%84%d9%83%d9%8a%d9%85%d9%8a%d8%a7%d8%a1-%d9%8a%d9%86%d8%a7%d9%82%d8%b4-%d8%b1%d8%b3%d8%a7%d9%84%d8%a9-%d9%85%d8%a7%d8%ac%d8%b3%d8%aa%d9%8a%d8%b1-%d8%aa%d8%ad%d8%b6%d8%b1-8","status":"publish","type":"post","link":"https:\/\/ihcoedu.uobaghdad.edu.iq\/?p=44472","title":{"rendered":"\u0642\u0633\u0645 \u0627\u0644\u0643\u064a\u0645\u064a\u0627\u0621 \u064a\u0646\u0627\u0642\u0634 \u0631\u0633\u0627\u0644\u0629 \u0645\u0627\u062c\u0633\u062a\u064a\u0631 \u062a\u062d\u0636\u0631 \u0645\u0639\u0642\u062f\u0627\u062a \u0641\u0644\u0632\u064a\u0629 \u062c\u062f\u064a\u062f\u0629 \u0645\u0634\u062a\u0642\u0629 \u0645\u0646 \u0644\u064a\u0643\u0646\u062f\u0627\u062a \u0644\u0642\u0648\u0627\u0639\u062f \u0634\u0641 \u063a\u064a\u0631 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srcset=\"https:\/\/ihcoedu.uobaghdad.edu.iq\/wp-content\/uploads\/sites\/27\/2022\/06\/\u0647\u0646\u062f-\u0627\u0628\u0631\u0627\u0647\u064a\u0645-\u062e\u0644\u064a\u0644-\u0645\u0627\u062c\u0633\u062a\u064a\u0631-\u0643\u064a\u0645\u064a\u0627\u0621-24-3-2022-7.jpeg 1280w, https:\/\/ihcoedu.uobaghdad.edu.iq\/wp-content\/uploads\/sites\/27\/2022\/06\/\u0647\u0646\u062f-\u0627\u0628\u0631\u0627\u0647\u064a\u0645-\u062e\u0644\u064a\u0644-\u0645\u0627\u062c\u0633\u062a\u064a\u0631-\u0643\u064a\u0645\u064a\u0627\u0621-24-3-2022-7-300x200.jpeg 300w, https:\/\/ihcoedu.uobaghdad.edu.iq\/wp-content\/uploads\/sites\/27\/2022\/06\/\u0647\u0646\u062f-\u0627\u0628\u0631\u0627\u0647\u064a\u0645-\u062e\u0644\u064a\u0644-\u0645\u0627\u062c\u0633\u062a\u064a\u0631-\u0643\u064a\u0645\u064a\u0627\u0621-24-3-2022-7-1024x682.jpeg 1024w, 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\u0628\u0639\u0636\u0647\u0627 \u063a\u064a\u0631 \u0645\u0648\u0635\u0644\u0629 . \u062a\u0645 \u0627\u0633\u062a\u062e\u062f\u0627\u0645 \u0627\u0644\u062f\u0631\u0627\u0633\u0627\u062a \u0627\u0644\u0646\u0638\u0631\u064a\u0629 \u0644\u0627\u062b\u0628\u0627\u062a \u0646\u0648\u0639 \u0627\u0644\u062a\u0646\u0627\u0633\u0642 \u0648\u0627\u0644\u062a\u0631\u062a\u064a\u0628 \u0627\u0644\u0647\u0646\u062f\u0633\u064a \u0627\u0644\u0645\u0641\u0636\u0644 \u062d\u0648\u0644 \u0627\u0644\u0630\u0631\u0629 \u0627\u0644\u0645\u0631\u0643\u0632\u064a\u0629. \u0645\u0646 \u0627\u0639\u0644\u0627\u0647 \u062a\u0645 \u0627\u0633\u062a\u0646\u062a\u0627\u062c \u0627\u0646 \u0646\u0648\u0639 \u0627\u0644\u0627\u0631\u062a\u0628\u0627\u0637 \u0648 \u0627\u0644\u0634\u0643\u0644 \u0627\u0644\u0647\u0646\u062f\u0633\u064a \u0627\u0644\u0645\u0642\u062a\u0631\u062d \u0644\u0644\u0645\u0639\u0642\u062f\u0627\u062a \u064a\u0643\u0648\u0646 \u0643\u0627\u0644\u0627\u062a\u064a :<\/span><\/h4>\n<h4 style=\"text-align: justify;\"><span style=\"color: #000080;\">\u0623\u0646 \u0645\u0639\u0642\u062f\u0627\u062a\u00a0 Cr (III), Mn (II) and Ni(II) \u0644\u0644\u064a\u0643\u0646\u062f\u0627\u062a ( (HL<sup>1<\/sup>\u0648 (HL<sup>2<\/sup>) \u062a\u0643\u0648\u0646 \u0633\u062f\u0627\u0633\u064a\u0629 \u0627\u0644\u062a\u0646\u0627\u0633\u0642 )\u0627\u0645\u0627 \u0645\u0639\u0642\u062f\u0627\u062a (Cu (II \u0648 (Zn (II \u0648 (Cd (II \u0641\u062a\u0641\u0636\u0644 \u0627\u0644\u062a\u0646\u0627\u0633\u0642 \u0627\u0644\u0631\u0628\u0627\u0639\u064a.<\/span><\/h4>\n<h4 style=\"text-align: justify;\"><span style=\"color: #000080;\">\u062a\u0645\u062a \u0645\u0646\u0627\u0642\u0634\u0629 \u0627\u0644\u062a\u0623\u062b\u064a\u0631\u0627\u062a \u0627\u0644\u0628\u064a\u0648\u0644\u0648\u062c\u064a\u0629 \u0644\u0644\u064a\u0643\u0627\u0646\u062f\u0627\u062a \u0648\u0645\u0639\u0642\u062f\u0627\u062a\u0647\u0627 \u0627\u0644\u0645\u0639\u062f\u0646\u064a\u0629 \u0636\u062f \u0623\u0631\u0628\u0639 \u0633\u0644\u0627\u0644\u0627\u062a \u0628\u0643\u062a\u064a\u0631\u064a\u0629 \u0641\u064a \u0627\u0644\u0641\u0635\u0644 \u0627\u0644\u0631\u0627\u0628\u0639<\/span><\/h4>\n<h4 style=\"text-align: justify;\"><span style=\"color: #000080;\">\u0623\u0638\u0647\u0631\u062a \u0627\u0644\u0644\u064a\u0643\u0627\u0646\u062f\u0627\u062a \u0648 \u0645\u0639\u0642\u062f\u0627\u062a\u0647\u0627\u00a0 ( (HL<sup>1<\/sup>\u0648 HL<sup>2<\/sup>)) \u0646\u0634\u0627\u0637\u064b\u0627 \u0645\u0636\u0627\u062f\u064b\u0627 \u0644\u0644\u0645\u064a\u0643\u0631\u0648\u0628\u0627\u062a \u0636\u062f (<em>Escherichia coli<\/em> \u00a0<em>Pseudomonas aeruginosa, Staphylococcus aureus, and Staphylococcus bacilli<\/em>).<\/span><\/h4>\n<h4 style=\"text-align: justify;\"><\/h4>\n<h4 style=\"text-align: justify;\"><span style=\"color: #000080;\">\u062a\u0645 \u0627\u0644\u0627\u0646\u062a\u0647\u0627\u0621 \u0645\u0646 \u0627\u0644\u0627\u0642\u062a\u0631\u0627\u062d \u0627\u0644\u062a\u0627\u0644\u064a \u0644\u0644\u0639\u0645\u0644 \u0627\u0644\u0645\u0633\u062a\u0642\u0628\u0644\u064a \u060c \u0648\u0627\u0644\u0630\u064a \u064a\u0639\u062a\u0645\u062f \u0639\u0644\u0649 \u0627\u0644\u0639\u0645\u0644 \u0627\u0644\u0645\u0630\u0643\u0648\u0631 \u0641\u064a \u0647\u0630\u0647 \u0627\u0644\u0631\u0633\u0627\u0644\u0629.<\/span><\/h4>\n<h4 style=\"text-align: justify;\"><span style=\"color: #000080;\">1- \u062a\u062d\u0636\u064a\u0631 \u0644\u064a\u0643\u0627\u0646\u062f\u0627\u062a \u062c\u062f\u064a\u062f\u0629 \u0628\u0645\u062e\u062a\u0644\u0641 \u0627\u0644\u0628\u062f\u0627\u0626\u0644. \u0647\u0630\u0627 \u0644\u0645\u0644\u0627\u062d\u0638\u0629 \u0627\u0644\u062a\u0623\u062b\u064a\u0631 \u0639\u0644\u0649 \u0648\u0636\u0639 \u0627\u0644\u062a\u0646\u0633\u064a\u0642 \u0644\u0644\u0623\u064a\u0648\u0646\u0627\u062a \u0627\u0644\u0645\u0639\u062f\u0646\u064a\u0629 \u0639\u0646\u062f \u0627\u0644\u062a\u0639\u0642\u064a\u062f.<\/span><\/h4>\n<h4 style=\"text-align: justify;\"><span style=\"color: #000080;\">2- \u0627\u0633\u062a\u0643\u0634\u0627\u0641 \u0625\u0645\u0643\u0627\u0646\u064a\u0629 \u0627\u0633\u062a\u062e\u062f\u0627\u0645 \u0627\u0644\u0644\u0643\u0627\u0646\u062f \u0627\u0644\u0645\u062d\u0636\u0631 \u0643\u0643\u0648\u0627\u0634\u0641 \u0641\u064a \u0627\u0644\u0643\u064a\u0645\u064a\u0627\u0621 \u0627\u0644\u062a\u062d\u0644\u064a\u0644\u064a\u0629.<\/span><\/h4>\n<h4 style=\"text-align: justify;\"><span style=\"color: #000080;\">3- \u062f\u0631\u0627\u0633\u0629 \u0643\u064a\u0645\u064a\u0627\u0621 \u0627\u0644\u062a\u0646\u0633\u064a\u0642 \u0644\u0644\u064a\u0643\u0627\u0646\u062f\u0627\u062a \u0627\u0644\u0645\u062d\u0636\u0631\u0629 \u0645\u0639 \u0623\u064a\u0648\u0646\u0627\u062a \u0641\u0644\u0632 \u0627\u0646\u062a\u0642\u0627\u0644\u064a\u0629 \u0623\u062e\u0631\u0649 \u062e\u0627\u0635\u0629 \u0645\u0646 \u0627\u0644\u0633\u0644\u0633\u0644\u0629 \u0627\u0644\u062b\u0627\u0646\u064a\u0629 \u0648 \/ \u0623\u0648 \u0627\u0644\u062b\u0627\u0644\u062b\u0629.<\/span><\/h4>\n<h4 style=\"text-align: justify;\"><span style=\"color: #000080;\">4- \u0627\u0644\u0639\u0645\u0644 \u0639\u0644\u0649 \u0625\u0639\u0627\u062f\u0629 \u0628\u0644\u0648\u0631\u0629 \u0627\u0644\u0645\u0631\u0643\u0628\u0627\u062a \u0627\u0644\u0645\u062d\u0636\u0631\u0629 (\u0627\u0644\u064a\u0643\u0627\u0646\u062f\u0627\u062a \u0648\u0627\u0644\u0645\u0639\u0642\u062f\u0627\u062a) \u0644\u0639\u0632\u0644 \u0627\u0644\u0628\u0644\u0648\u0631\u0627\u062a \u0627\u0644\u0645\u0646\u0627\u0633\u0628\u0629 \u0644\u0644\u0623\u0634\u0639\u0629 \u0627\u0644\u0633\u064a\u0646\u064a\u0629 \u0630\u0627\u062a \u0627\u0644\u062a\u0631\u0643\u064a\u0628 \u0627\u0644\u0628\u0644\u0648\u0631\u064a \u0627\u0644\u0623\u062d\u0627\u062f\u064a.<\/span><\/h4>\n<h4 style=\"text-align: justify;\"><span style=\"color: #000080;\">5- \u062f\u0631\u0627\u0633\u0629 \u0627\u0644\u0646\u0634\u0627\u0637 \u0627\u0644\u0628\u064a\u0648\u0644\u0648\u062c\u064a \u0644\u0644\u0645\u0631\u0643\u0628\u0627\u062a \u0627\u0644\u0645\u062d\u0636\u0631\u0629 \u0636\u062f \u0627\u0644\u0643\u0627\u0626\u0646\u0627\u062a \u0627\u0644\u062d\u064a\u0629 \u0627\u0644\u062f\u0642\u064a\u0642\u0629 \u0627\u0644\u0623\u062e\u0631\u0649.<\/span><\/h4>\n<h4 style=\"text-align: justify;\"><span style=\"color: #000080;\">6- \u0641\u062d\u0635 \u0627\u0633\u062a\u062e\u062f\u0627\u0645 \u0627\u0644\u0644\u064a\u0643\u0627\u0646\u062f\u0627\u062a \u0648\u0645\u0639\u0642\u062f\u0627\u062a\u0647\u0627 \u0641\u064a \u062a\u0642\u0646\u064a\u0629 \u0631\u0628\u0637 \u0627\u0644\u062d\u0645\u0636 \u0627\u0644\u0646\u0648\u0648\u064a.<\/span><\/h4>\n<hr \/>\n<h3 style=\"text-align: left;\"><span style=\"color: #993366;\">New Metal Complexes Derived From Heterocyclic Schiff-base Ligands; Preparation, Structural Investigation<\/span><\/h3>\n<h3 style=\"text-align: left;\"><span style=\"color: #993366;\">and Biological Activity<\/span><\/h3>\n<h3 style=\"text-align: left;\"><span style=\"color: #993366;\">By Hind Ibrahim Khaleel Safi<\/span><\/h3>\n<h3 style=\"text-align: left;\"><span style=\"color: #993366;\">Supervised by Assist. Prof. Baidaa Kareem Al-Rubaye<\/span><\/h3>\n<h3 style=\"text-align: left;\"><span style=\"color: #993366;\">Aim of the work<\/span><\/h3>\n<h3 style=\"text-align: left;\"><span style=\"color: #993366;\">The synthesis and structural characterization of two novel ligands with the N and O donor atoms and their metal complexes are included in this work. The biological activity of the ligands and their metal complexes against bacterial strains were also investigated. This work covers;<\/span><\/h3>\n<h3 style=\"text-align: left;\"><span style=\"color: #993366;\">\u00a0The preparation of a new precursor namely furan-2-carbohydrazide from the reaction of the hydrazine with furan-2-carbonyl chloride.<\/span><\/h3>\n<h3 style=\"text-align: left;\"><span style=\"color: #993366;\">The preparation of two Mannich bases that are used as precursors in the formation of ligands.<\/span><\/h3>\n<h3 style=\"text-align: left;\"><span style=\"color: #993366;\">Synthesis of two novel Schiff base ligands (HL1 and HL2) that were achieved from the reaction of furan-2-carbohydrazide the Mannich bases.<\/span><\/h3>\n<h3 style=\"text-align: left;\"><span style=\"color: #993366;\">Formation of a set of complexes that achieved from the interaction of both HL1 and HL2 with a range of d-block transition metals.<\/span><\/h3>\n<h3 style=\"text-align: left;\"><span style=\"color: #993366;\">Investigating the stereochemistry and possible structures of complexes.<\/span><\/h3>\n<h3 style=\"text-align: left;\"><span style=\"color: #993366;\">Exploring the anti-bacterial activity of HL1 and HL2 and their complexes towards G-positive and G-negative types of bacteria.<\/span><\/h3>\n<h3 style=\"text-align: left;\"><span style=\"color: #993366;\">The key aspects in synthetic chemistry are simplicity and efficiency, in the formation of new chemical compounds. These compounds may be used as reagents in medical chemistry and organic synthesis. The structural complexity of a molecule may require a multi-step synthetic process, which includes isolation and purification steps.<\/span><\/h3>\n<h3 style=\"text-align: left;\"><span style=\"color: #993366;\">This thesis contains four chapters:<\/span><\/h3>\n<h3 style=\"text-align: left;\"><span style=\"color: #993366;\">Chapter One: An overview of Mannich interactions and the evolution of metal complexes with N2O2 coordination cores.It also covers the literature review on the recent state of the art on the role of the cyclic and macro cyclic N2O2 ligands in metal complexes.In addition, the uses and applications of these systems and their metal complexes are also documented. It also contains the aim and objectives of this research.<\/span><\/h3>\n<h3 style=\"text-align: left;\"><span style=\"color: #993366;\">Chapter Two:In this chapter the experimental aspects are explained including the materials used in this research, physical measurements (spectroscopic techniques), chemical compositions of the generated bonds and their complexes, and procedures for the synthesis of bonds and their metal complexes.This chapter also describes the synthesis and characterization of a number of ligands including the N2O2 chelating system, as well as their metallic complexes.It resulted from the reaction of amine derivatives with furan-2 carbohydrazide to prepare the ligands. The first step involved treating the addition of benzaldehyde<\/span><\/h3>\n<h3 style=\"text-align: left;\"><\/h3>\n<h3 style=\"text-align: left;\"><span style=\"color: #993366;\">Prospective Research Work<\/span><\/h3>\n<h3 style=\"text-align: left;\"><span style=\"color: #993366;\">\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0 The following suggestion for futuristic work has been concluded, which is based on the work reported in this thesis.<\/span><\/h3>\n<h3 style=\"text-align: left;\"><span style=\"color: #993366;\">Preparation of novel ligands with various substituents. This is to observe the impact on the coordination mode of the metal ions upon complexation.<\/span><\/h3>\n<h3 style=\"text-align: left;\"><span style=\"color: #993366;\">Explore the possibility of using the prepared ligand as reagents in analytical chemistry.<\/span><\/h3>\n<h3 style=\"text-align: left;\"><span style=\"color: #993366;\">Studying the coordination chemistry of the prepared ligands with other transition metal ions in particular that from the second and\/or third series.<\/span><\/h3>\n<h3 style=\"text-align: left;\"><span style=\"color: #993366;\">Working on recrystallizing the prepared compounds (ligands and metal complexes) to isolate crystals appropriate for X-ray single-crystal structure.<\/span><\/h3>\n<h3 style=\"text-align: left;\"><span style=\"color: #993366;\">Studying the biological activity of the prepared compounds against other microorganisms.<\/span><\/h3>\n<h3 style=\"text-align: left;\"><span style=\"color: #993366;\">Examine the use of ligands and their complexes in the DNA binding technique.<\/span><\/h3>\n<p>&nbsp;<\/p>\n","protected":false},"excerpt":{"rendered":"<p>\u0646\u0627\u0642\u0634 \u0642\u0633\u0645 \u0627\u0644\u0643\u064a\u0645\u064a\u0627\u0621 \u0641\u064a \u0643\u0644\u064a\u0629 \u0627\u0644\u062a\u0631\u0628\u064a\u0629 \u0644\u0644\u0639\u0644\u0648\u0645 \u0627\u0644\u0635\u0631\u0641\u0629 (\u0627\u0628\u0646 \u0627\u0644\u0647\u064a\u062b\u0645) \u0631\u0633\u0627\u0644\u0629 \u0627\u0644\u0645\u0627\u062c\u0633\u062a\u064a\u0631 \u0627\u0644\u0645\u0648\u0633\u0648\u0645\u0629 &#8221; \u0645\u0639\u0642\u062f\u0627\u062a \u0641\u0644\u0632\u064a\u0629 \u062c\u062f\u064a\u062f\u0629 \u0645\u0634\u062a\u0642\u0629 \u0645\u0646 \u0644\u064a\u0643\u0646\u062f\u0627\u062a&#8230;.<a class=\"cz_readmore\" href=\"https:\/\/ihcoedu.uobaghdad.edu.iq\/?p=44472\"><i class=\"fa fa-angle-left\" aria-hidden=\"true\"><\/i><span>\u0627\u0644\u0645\u0632\u064a\u062f<\/span><\/a><\/p>\n","protected":false},"author":25,"featured_media":44480,"comment_status":"closed","ping_status":"closed","sticky":false,"template":"","format":"standard","meta":{"_lmt_disableupdate":"no","_lmt_disable":"","footnotes":""},"categories":[7,59,98,16],"tags":[23,47],"class_list":["post-44472","post","type-post","status-publish","format-standard","has-post-thumbnail","hentry","category-7","category-59","category-98","category-16","tag-ihcoedu","tag-chem"],"modified_by":"ihcoedu","_links":{"self":[{"href":"https:\/\/ihcoedu.uobaghdad.edu.iq\/index.php?rest_route=\/wp\/v2\/posts\/44472","targetHints":{"allow":["GET"]}}],"collection":[{"href":"https:\/\/ihcoedu.uobaghdad.edu.iq\/index.php?rest_route=\/wp\/v2\/posts"}],"about":[{"href":"https:\/\/ihcoedu.uobaghdad.edu.iq\/index.php?rest_route=\/wp\/v2\/types\/post"}],"author":[{"embeddable":true,"href":"https:\/\/ihcoedu.uobaghdad.edu.iq\/index.php?rest_route=\/wp\/v2\/users\/25"}],"replies":[{"embeddable":true,"href":"https:\/\/ihcoedu.uobaghdad.edu.iq\/index.php?rest_route=%2Fwp%2Fv2%2Fcomments&post=44472"}],"version-history":[{"count":0,"href":"https:\/\/ihcoedu.uobaghdad.edu.iq\/index.php?rest_route=\/wp\/v2\/posts\/44472\/revisions"}],"wp:featuredmedia":[{"embeddable":true,"href":"https:\/\/ihcoedu.uobaghdad.edu.iq\/index.php?rest_route=\/wp\/v2\/media\/44480"}],"wp:attachment":[{"href":"https:\/\/ihcoedu.uobaghdad.edu.iq\/index.php?rest_route=%2Fwp%2Fv2%2Fmedia&parent=44472"}],"wp:term":[{"taxonomy":"category","embeddable":true,"href":"https:\/\/ihcoedu.uobaghdad.edu.iq\/index.php?rest_route=%2Fwp%2Fv2%2Fcategories&post=44472"},{"taxonomy":"post_tag","embeddable":true,"href":"https:\/\/ihcoedu.uobaghdad.edu.iq\/index.php?rest_route=%2Fwp%2Fv2%2Ftags&post=44472"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}