{"id":44557,"date":"2022-06-26T09:34:37","date_gmt":"2022-06-26T06:34:37","guid":{"rendered":"https:\/\/ihcoedu.uobaghdad.edu.iq\/?p=44557"},"modified":"2023-06-28T18:28:58","modified_gmt":"2023-06-28T15:28:58","slug":"%d9%82%d8%b3%d9%85-%d8%a7%d9%84%d9%83%d9%8a%d9%85%d9%8a%d8%a7%d8%a1-%d9%8a%d9%86%d8%a7%d9%82%d8%b4-%d8%b1%d8%b3%d8%a7%d9%84%d8%a9-%d9%85%d8%a7%d8%ac%d8%b3%d8%aa%d9%8a%d8%b1-%d8%aa%d8%a8%d8%ad%d8%ab-36","status":"publish","type":"post","link":"https:\/\/ihcoedu.uobaghdad.edu.iq\/?p=44557","title":{"rendered":"\u0642\u0633\u0645 \u0627\u0644\u0643\u064a\u0645\u064a\u0627\u0621 \u064a\u0646\u0627\u0642\u0634 \u0631\u0633\u0627\u0644\u0629 \u0645\u0627\u062c\u0633\u062a\u064a\u0631 \u062a\u0628\u062d\u062b \u0641\u064a \u062a\u062d\u0636\u064a\u0631 \u0648 \u062a\u0634\u062e\u064a\u0635 \u0645\u0639 \u0627\u0644\u062a\u0642\u064a\u064a\u0645 \u0627\u0644\u0628\u064a\u0648\u0644\u0648\u062c\u064a \u0644\u0645\u0639\u0642\u062f\u0627\u062a \u0641\u0644\u0632\u064a\u0629 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https:\/\/ihcoedu.uobaghdad.edu.iq\/wp-content\/uploads\/sites\/27\/2022\/06\/\u0645\u0646\u0627\u0642\u0634\u0629-\u0647\u062f\u064a\u0644-\u062c\u0644\u0627\u0644-\u0639\u0628\u0627\u0633-\u0645\u0627\u062c\u0633\u062a\u064a\u0631-\u0643\u064a\u0645\u064a\u0627\u0621-1-300x200.jpg 300w, https:\/\/ihcoedu.uobaghdad.edu.iq\/wp-content\/uploads\/sites\/27\/2022\/06\/\u0645\u0646\u0627\u0642\u0634\u0629-\u0647\u062f\u064a\u0644-\u062c\u0644\u0627\u0644-\u0639\u0628\u0627\u0633-\u0645\u0627\u062c\u0633\u062a\u064a\u0631-\u0643\u064a\u0645\u064a\u0627\u0621-1-768x512.jpg 768w, https:\/\/ihcoedu.uobaghdad.edu.iq\/wp-content\/uploads\/sites\/27\/2022\/06\/\u0645\u0646\u0627\u0642\u0634\u0629-\u0647\u062f\u064a\u0644-\u062c\u0644\u0627\u0644-\u0639\u0628\u0627\u0633-\u0645\u0627\u062c\u0633\u062a\u064a\u0631-\u0643\u064a\u0645\u064a\u0627\u0621-1-600x400.jpg 600w\" sizes=\"auto, (max-width: 872px) 100vw, 872px\" \/>\u0646\u0627\u0642\u0634 \u0642\u0633\u0645 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\u0639\u0636\u0648\u0627<\/strong><\/span><\/h4>\n<\/li>\n<li>\n<h4><span style=\"color: #000080;\"><strong>\u0627.\u0645.\u062f. \u0628\u064a\u062f\u0627\u0621 \u0643\u0631\u064a\u0645 \u0633\u0644\u0645\u0627\u0646 &#8211; \u0639\u0636\u0648\u0627<\/strong><\/span><\/h4>\n<\/li>\n<li>\n<h4><span style=\"color: #000080;\">\u0623. \u062f. \u0645\u062d\u0645\u062f \u062c\u0627\u0628\u0631 \u0627\u0628\u0631\u0627\u0647\u064a\u0645 &#8211; \u0639\u0636\u0648\u0627 \u0648 \u0645\u0634\u0631\u0641\u0627<\/span><\/h4>\n<\/li>\n<\/ul>\n<h4><img loading=\"lazy\" decoding=\"async\" class=\"aligncenter size-full wp-image-44559\" src=\"https:\/\/ihcoedu.uobaghdad.edu.iq\/wp-content\/uploads\/sites\/27\/2022\/06\/\u0645\u0646\u0627\u0642\u0634\u0629-\u0647\u062f\u064a\u0644-\u062c\u0644\u0627\u0644-\u0639\u0628\u0627\u0633-\u0645\u0627\u062c\u0633\u062a\u064a\u0631-\u0643\u064a\u0645\u064a\u0627\u0621-1.jpeg\" alt=\"\" width=\"872\" height=\"581\" srcset=\"https:\/\/ihcoedu.uobaghdad.edu.iq\/wp-content\/uploads\/sites\/27\/2022\/06\/\u0645\u0646\u0627\u0642\u0634\u0629-\u0647\u062f\u064a\u0644-\u062c\u0644\u0627\u0644-\u0639\u0628\u0627\u0633-\u0645\u0627\u062c\u0633\u062a\u064a\u0631-\u0643\u064a\u0645\u064a\u0627\u0621-1.jpeg 872w, https:\/\/ihcoedu.uobaghdad.edu.iq\/wp-content\/uploads\/sites\/27\/2022\/06\/\u0645\u0646\u0627\u0642\u0634\u0629-\u0647\u062f\u064a\u0644-\u062c\u0644\u0627\u0644-\u0639\u0628\u0627\u0633-\u0645\u0627\u062c\u0633\u062a\u064a\u0631-\u0643\u064a\u0645\u064a\u0627\u0621-1-300x200.jpeg 300w, https:\/\/ihcoedu.uobaghdad.edu.iq\/wp-content\/uploads\/sites\/27\/2022\/06\/\u0645\u0646\u0627\u0642\u0634\u0629-\u0647\u062f\u064a\u0644-\u062c\u0644\u0627\u0644-\u0639\u0628\u0627\u0633-\u0645\u0627\u062c\u0633\u062a\u064a\u0631-\u0643\u064a\u0645\u064a\u0627\u0621-1-768x512.jpeg 768w, https:\/\/ihcoedu.uobaghdad.edu.iq\/wp-content\/uploads\/sites\/27\/2022\/06\/\u0645\u0646\u0627\u0642\u0634\u0629-\u0647\u062f\u064a\u0644-\u062c\u0644\u0627\u0644-\u0639\u0628\u0627\u0633-\u0645\u0627\u062c\u0633\u062a\u064a\u0631-\u0643\u064a\u0645\u064a\u0627\u0621-1-600x400.jpeg 600w\" sizes=\"auto, (max-width: 872px) 100vw, 872px\" \/><\/h4>\n<h4><span style=\"color: #000080;\">\u0648\u064a\u0647\u062f\u0641 \u0645\u0646 \u0627\u0644\u0639\u0645\u0644 \u0627\u0644\u0649:<\/span><\/h4>\n<ol>\n<li>\n<h4><span style=\"color: #000080;\">\u062a\u0648\u0644\u064a\u0641 \u062c\u062f\u064a\u062f \u0634\u0628\u0647 \u0648\u062b\u064a\u0648\u0633\u064a\u0645\u064a\u0643\u0627\u0631\u0628\u0627\u0632\u0648\u0646 \u0645\u0646 \u062e\u0644\u0637 \u0642\u0627\u0639\u062f\u0629 \u0645\u0627\u0646\u064a\u0634 \u0627\u0644\u062a\u064a \u062a\u0645 \u062a\u062d\u0636\u064a\u0631\u0647\u0627 \u0639\u0628\u0631 \u062a\u0641\u0627\u0639\u0644 \u062b\u0644\u0627\u062b\u064a \u0627\u0644\u0645\u0643\u0648\u0646\u0627\u062a (\u0633\u064a\u0643\u0644\u0648\u0647\u0643\u0633\u0627\u0646\u0648\u0646 \u060c \u0628\u0646\u0632\u0627\u0644\u062f\u064a\u0647\u0627\u064a\u062f \u0648\u0641\u064a\u0646\u064a\u0644 \u0647\u064a\u062f\u0631\u0627\u0632\u064a\u0646) \u0645\u0639 \u0643\u0627\u0634\u0641 \u0634\u0628\u0647 \u0648\u062b\u064a\u0648\u0633\u064a\u0645\u064a \u0643\u0631\u0628\u0627\u0632\u064a\u062f.<\/span><\/h4>\n<\/li>\n<li>\n<h4><span style=\"color: #000080;\">\u062a\u0643\u0648\u064a\u0646 \u0645\u0639\u0642\u062f\u0627\u062a \u0641\u0644\u0632\u064a\u0629 \u0645\u0646 \u062a\u0641\u0627\u0639\u0644 \u0643\u0644\u0627 \u0627\u0644\u062a\u0631\u0627\u0628\u0637\u064a\u0646 \u0645\u0639 \u0623\u064a\u0648\u0646\u0627\u062a Cr (III) \u0648 Mn (II) \u0648 Co (II) \u0648 Ni (II) \u0648 Cu (II) \u0648 Zn (II) \u0648 Cd (II).<\/span><\/h4>\n<\/li>\n<li>\n<h4><span style=\"color: #000080;\">\u062a\u0648\u0635\u064a\u0641 \u0627\u0644\u0645\u0631\u0643\u0628\u0627\u062a \u0627\u0644\u0645\u062d\u0636\u0631\u0629 \u0628\u0627\u0633\u062a\u062e\u062f\u0627\u0645 \u0639\u062f\u0629 \u062a\u0642\u0646\u064a\u0627\u062a \u0641\u064a\u0632\u064a\u0627\u0626\u064a\u0629 \u0643\u064a\u0645\u064a\u0627\u0626\u064a\u0629.<\/span><\/h4>\n<\/li>\n<li>\n<h4><span style=\"color: #000080;\">\u062f\u0631\u0627\u0633\u0629 \u0627\u0644\u062a\u0631\u062a\u064a\u0628 \u0627\u0644\u0647\u0646\u062f\u0633\u064a \u0648\u0627\u0644\u0646\u0634\u0627\u0637 \u0627\u0644\u0628\u064a\u0648\u0644\u0648\u062c\u064a \u0644\u0647\u0630\u0647 \u0627\u0644\u0645\u0631\u0643\u0628\u0627\u062a.<\/span><\/h4>\n<\/li>\n<\/ol>\n<h4><span style=\"color: #000080;\"><strong>\u00a0<\/strong><\/span><\/h4>\n<h4><span style=\"color: #000080;\">\u062a\u0636\u0645\u0646\u062a \u0647\u0630\u0647 \u0627\u0644\u062f\u0631\u0627\u0633\u0629 \u062a\u062d\u0636\u064a\u0631 \u0627\u0644\u0645\u0631\u0643\u0628\u00a0\u00a02-(phenyl(2-phenylhydra-zinyl)methyl)cyclohexan-1-one (M)<\/span><\/h4>\n<h4><span style=\"color: #000080;\">\u00a0\u0648\u0641\u0642\u0627 \u0644\u062a\u0641\u0627\u0639\u0644 \u0645\u0627\u0646\u062e \u0648\u0628\u0627\u0633\u062a\u062e\u062f\u0627\u0645 \u062d\u0627\u0645\u0636 \u0627\u0644\u0647\u064a\u062f\u0631\u0648\u0643\u0644\u0648\u0631\u064a\u0643 \u0648 \u0643\u0644\u0648\u0631\u064a\u062f \u0627\u0644\u0643\u0627\u0644\u0633\u064a\u0648\u0645 \u0643\u0645\u062d\u0641\u0632, \u0627\u0644\u062a\u0641\u0627\u0639\u0644 \u062a\u0645 \u0628\u0627\u0633\u062a\u062e\u062f\u0627\u0645 \u0627\u0644\u0643\u062d\u0648\u0644 \u0627\u0644\u0627\u062b\u064a\u0644\u064a \u0643\u0648\u0633\u0637 \u0644\u0644\u062a\u0641\u0627\u0639\u0644 \u0645\u0646 \u062e\u0644\u0627\u0644 \u0645\u0632\u062c \u062b\u0644\u0627\u062b \u0645\u0643\u0648\u0646\u0627\u062a \u0648\u0647\u064a \u0627\u0644\u0628\u0646\u0632\u0627\u0644\u062f\u064a\u0647\u0627\u064a\u062f\u060c \u0641\u0646\u064a\u0644 \u0647\u064a\u062f\u0631\u0627\u0632\u064a\u0646 \u0648 \u0627\u0644\u0633\u0627\u064a\u0643\u0644\u0648\u0647\u0643\u0633\u0627\u0646\u0648\u0646 \u0648\u0628\u0646\u0633\u0628 \u0645\u0648\u0644\u064a\u0629 1:1:1 \u0639\u0644\u0649 \u0627\u0644\u062a\u0648\u0627\u0644\u064a \u0628\u062a\u062d\u0631\u064a\u0643 \u0627\u0644\u0645\u0632\u064a\u062c \u0644\u0645\u062f\u0629 12 \u0633\u0627\u0639\u0629 \u0639\u0646\u062f \u062f\u0631\u062c\u0629 \u062d\u0631\u0627\u0631\u0629 \u0627\u0644\u063a\u0631\u0641\u0629\u00a0 \u0648\u062a\u0645 \u0627\u0644\u062d\u0635\u0648\u0644 \u0639\u0644\u0649 \u0627\u0644\u0646\u0627\u062a\u062c \u0627\u0644\u0645\u0637\u0644\u0648\u0628 \u0643\u0645\u0627\u062f\u0629 \u0635\u0644\u0628\u0629 \u0645\u0646 \u062e\u0644\u0627\u0644 \u062a\u0631\u0634\u064a\u062d\u0647\u0627 \u0648\u063a\u0633\u0644\u0647\u0627 \u0628\u0627\u0644\u0645\u0627\u0621 \u0627\u0644\u0645\u0642\u0637\u0631 \u0648\u0627\u0639\u0627\u062f\u0629 \u0628\u0644\u0648\u0631\u062a\u0647\u0627 \u0648\u062a\u062c\u0641\u064a\u0641\u0647\u0627\u00a0 .<\/span><\/h4>\n<h4><span style=\"color: #000080;\">\u0627\u0633\u062a\u062e\u062f\u0645 \u0627\u0644\u0645\u0631\u0643\u0628 \u0627\u0639\u0644\u0627\u0647 \u0644\u062a\u062d\u0636\u064a\u0631 \u0645\u062c\u0645\u0648\u0639\u062a\u064a\u0646 \u062c\u062f\u064a\u062f\u062a\u064a\u0646 \u0645\u0646 \u0644\u0642\u0648\u0627\u0639\u062f \u0634\u0641<\/span><\/h4>\n<ul>\n<li>\n<h4><span style=\"color: #000080;\">\u0627\u0644\u0644\u064a\u0643\u0627\u0646\u062f \u0627\u0644\u0627\u0648\u0644 \u064a\u0633\u0645\u0649 (E)-2-(2-(phenyl(2-phenylhy-drazinyl)methyl)cyclohexylidene)hydrazine-1-Acarboxamide[HL<sup>1<\/sup>] \u0648\u0642\u062f \u062a\u0645 \u062a\u062d\u0636\u064a\u0631\u0647 \u0645\u0646 \u0645\u0641\u0627\u0639\u0644\u0629 \u0627\u0644\u0633\u0645\u064a \u0643\u0627\u0631\u0628\u0632\u0627\u064a\u062f \u0645\u0639 \u0645\u0634\u062a\u0642 \u0645\u0627\u0646\u062e \u0627\u0644\u0645\u062d\u0636\u0631 \u0627\u0639\u0644\u0627\u0647 \u0648\u0628\u0646\u0633\u0628\u0629 1:1 \u0648\u0628\u0648\u062c\u0648\u062f \u0627\u0644\u0627\u064a\u062b\u0627\u0646\u0648\u0644 \u0643\u0648\u0633\u0637 \u0644\u0644\u062a\u0641\u0627\u0639\u0644 \u0628\u0637\u0631\u064a\u0642\u0629 \u0627\u0644\u062a\u0635\u0639\u064a\u062f \u0627\u0644\u0627\u0631\u062c\u0627\u0639\u064a \u0648\u0644\u0645\u062f\u0629 6\u0633\u0627\u0639\u0627\u062a \u0648\u062a\u0645 \u062a\u0631\u0634\u064a\u062d \u0627\u0644\u0646\u0627\u062a\u062c \u0627\u0644\u0635\u0644\u0628 \u0648\u063a\u0633\u0644\u0647 \u0648\u0628\u0627\u0633\u062a\u062e\u062f\u0627\u0645 \u0627\u0644\u0627\u064a\u062b\u0627\u0646\u0648\u0644 \u0648\u0627\u0644\u0627\u064a\u062b\u0631 .<\/span><\/h4>\n<\/li>\n<li>\n<h4><span style=\"color: #000080;\">\u0627\u0644\u0644\u064a\u0643\u0627\u0646\u062f \u0627\u0644\u062b\u0627\u0646\u064a \u064a\u0633\u0645\u0649 (E)-2-(2-(phenyl(2-phenylhy-drazinyl)methyl)cyclohexylidene)hydrazine-1-carbothioamide[HL<sup>2<\/sup>] \u0648\u0642\u062f \u062a\u0645 \u062a\u062d\u0636\u064a\u0631\u0647 \u0645\u0646 \u0645\u0641\u0627\u0639\u0644\u0629 \u0627\u0644\u062b\u0627\u064a\u0648\u0633\u0645\u064a \u0643\u0627\u0631\u0628\u0632\u0627\u064a\u062f \u0645\u0639 \u0645\u0634\u062a\u0642 \u0645\u0627\u0646\u062e \u0627\u0644\u0645\u062d\u0636\u0631 \u0627\u0639\u0644\u0627\u0647 \u0648\u0628\u0646\u0633\u0628\u0629 1:1 \u0648\u0628\u0648\u062c\u0648\u062f \u0627\u0644\u0627\u064a\u062b\u0627\u0646\u0648\u0644 \u0643\u0648\u0633\u0637 \u0644\u0644\u062a\u0641\u0627\u0639\u0644 \u0628\u0637\u0631\u064a\u0642\u0629 \u0627\u0644\u062a\u0635\u0639\u064a\u062f \u0627\u0644\u0627\u0631\u062c\u0627\u0639\u064a \u0648\u0644\u0645\u062f\u0629 4\u0633\u0627\u0639\u0627\u062a \u0648\u062a\u0645 \u062a\u0631\u0634\u064a\u062d \u0627\u0644\u0646\u0627\u062a\u062c \u0627\u0644\u0635\u0644\u0628 \u0648\u063a\u0633\u0644\u0647 \u0648\u0628\u0627\u0633\u062a\u062e\u062f\u0627\u0645 \u0627\u0644\u0627\u064a\u062b\u0627\u0646\u0648\u0644 \u0648\u0627\u0644\u0627\u064a\u062b\u0631 .<\/span><\/h4>\n<\/li>\n<\/ul>\n<h4><\/h4>\n<h4><span style=\"color: #000080;\">\u0648\u0642\u062f \u0634\u062e\u0635\u062a \u0627\u0644\u0644\u064a\u0643\u0627\u0646\u062f\u0627\u062a \u0627\u0644\u0645\u062d\u0636\u0631\u0629 (HL<sup>1<\/sup>) \u0648 (HL<sup>2<\/sup>) \u0645\u0646 \u062e\u0644\u0627\u0644 \u0627\u0637\u064a\u0627\u0641 \u0627\u0644\u0627\u0634\u0639\u0629 \u062a\u062d\u062a \u0627\u0644\u062d\u0645\u0631\u0627\u0621 (FT-IR) , \u0648\u0627\u0637\u064a\u0627\u0641 \u0627\u0644\u0627\u0634\u0639\u0629 \u0641\u0648\u0642 \u0627\u0644\u0628\u0646\u0641\u0633\u062c\u064a\u0629 \u2013 \u0627\u0644\u0645\u0631\u0626\u064a\u0629 (Uv-vis) , \u0648\u0627\u0637\u064a\u0627\u0641 \u0627\u0644\u0631\u0646\u064a\u0646 \u0627\u0644\u0646\u0648\u0648\u064a \u0627\u0644\u0645\u063a\u0646\u0627\u0637\u064a\u0633\u064a (<sup>13<\/sup>C,<sup>1<\/sup>HNMR) \u060c \u0648\u0645\u0637\u064a\u0627\u0641\u064a\u0629 \u0627\u0644\u0643\u062a\u0644\u0629 \u0648\u0627\u0644\u062a\u062d\u0644\u064a\u0644 \u0627\u0644\u062f\u0642\u064a\u0642 \u0644\u0644\u0639\u0646\u0627\u0635\u0631 (C.H.N.S) \u0627\u0644\u0630\u064a \u0627\u0638\u0647\u0631 \u0645\u0637\u0627\u0628\u0642\u0629 \u062f\u0642\u064a\u0642\u0629 \u0645\u0639 \u0627\u0644\u0635\u064a\u063a \u0627\u0644\u062c\u0632\u0626\u064a\u0629 \u0644\u0647\u0630\u0647 \u0627\u0644\u0645\u0634\u062a\u0642\u0627\u062a.<\/span><\/h4>\n<h4><span style=\"color: #000080;\">\u062d\u0636\u0631\u062a \u0628\u0639\u0636 \u0627\u0644\u0645\u0639\u0642\u062f\u0627\u062a \u0627\u0644\u0641\u0644\u0632\u064a\u0629 \u0644\u0643\u0644\u0627 \u0627\u0644\u0644\u064a\u0643\u0627\u0646\u062f\u064a\u0646 \u0627\u0644\u0645\u0634\u062a\u0642\u064a\u0646 \u0648\u0630\u0644\u0643 \u0628\u0645\u0641\u0627\u0639\u0644\u0629 \u0643\u0644 \u0645\u0646\u0647\u0645\u0627 \u0645\u0639 \u0627\u0644\u0627\u064a\u0648\u0646\u0627\u062a \u0627\u0644\u0641\u0644\u0632\u064a\u0629 (Mn<sup>(II)<\/sup>, Co<sup>(II)<\/sup>, Ni<sup>(II)<\/sup>, Cu<sup>(II)<\/sup>, Zn<sup>(II)<\/sup>\u00a0 and Cd<sup>(II)<\/sup> , Cr<sup>(III)<\/sup>) \u0628\u0639\u0645\u0644\u064a\u0629 \u0627\u0644\u062a\u0635\u0639\u064a\u062f \u0627\u0644\u0627\u0631\u062c\u0627\u0639\u064a \u0648\u0628\u0646\u0633\u0628\u0629 1:1 \u0644\u064a\u0643\u0627\u0646\u062f :\u0641\u0644\u0632 \u0648\u0642\u062f \u0627\u0639\u0637\u062a \u0645\u0639\u0642\u062f\u0627\u062a \u062f\u0627\u064a\u0645\u0631\u064a\u0629 \u0644\u0644\u0644\u064a\u0643\u0627\u0646\u062f \u0627\u0644\u0627\u0648\u0644 \u0648 \u0627\u0644\u0635\u064a\u063a\u0629 \u0627\u0644\u0639\u0627\u0645\u0629 \u0644\u0647\u0627 :[Cr(L)(Cl)<sub>2<\/sub>(H<sub>2<\/sub>O)]<sub>2<\/sub>, [M(L)Cl]<sub>2<\/sub> M= Mn(II), Co(II), Ni(II), Cu(II)), Zn(II) Cd(II)\u00a0 .<\/span><\/h4>\n<h4><span style=\"color: #000080;\">\u0641\u064a \u062d\u064a\u0646 \u0643\u0627\u0646\u062a \u0645\u0639\u0642\u062f\u0627\u062a \u0627\u0644\u0644\u064a\u0643\u0627\u0646\u062f \u0627\u0644\u062b\u0627\u0646\u064a \u0628\u0627\u0644\u0635\u064a\u063a\u0629 \u0627\u0644\u0639\u0627\u0645\u0629 \u00a0[Cr(L<sup>2<\/sup>)Cl<sub>2<\/sub>H<sub>2<\/sub>O], [M (L<sup>2<\/sup>)Cl] M= Mn(II), Co(II), Ni(II), Cu(II)), Zn(II) \u0648 Cd(II) ..<\/span><\/h4>\n<h4><span style=\"color: #000080;\">\u00a0 \u062f\u0631\u0633\u062a \u0648\u0634\u062e\u0635\u062a \u0627\u0644\u0645\u0639\u0642\u062f\u0627\u062a \u0627\u0644\u0645\u062d\u0636\u0631\u0629 \u0645\u0646 \u062e\u0644\u0627\u0644 \u0627\u0637\u064a\u0627\u0641 \u0627\u0644\u0627\u0634\u0639\u0629 \u062a\u062d\u062a \u0627\u0644\u062d\u0645\u0631\u0627\u0621 \u0627\u0644\u062a\u064a \u0627\u0638\u0647\u0631\u062a \u0627\u0646 \u0627\u0644\u0644\u064a\u0643\u0627\u0646\u062f\u0627\u062a \u062a\u0633\u0644\u0643 \u0633\u0644\u0648\u0643 \u0627\u064a\u0648\u0646\u064a (-1) \u0646\u062a\u064a\u062c\u0629 \u0641\u0642\u062f\u0627\u0646\u0647\u0627 \u0644\u0628\u0631\u0648\u062a\u0648\u0646 \u0645\u0646 \u062f\u0631\u0629 \u0627\u0644\u0646\u062a\u0631\u0648\u062c\u064a\u0646 2 N\u0639\u0646\u062f \u062a\u0646\u0627\u0633\u0642\u0647\u0627 \u0645\u0639 \u0627\u0644\u0641\u0644\u0632\u0627\u062a\u00a0 , \u0648\u0627\u0633\u062a\u062e\u062f\u0645\u062a \u062a\u0642\u0646\u064a\u0627\u062a \u0627\u0644\u0627\u0634\u0639\u0629 \u0641\u0648\u0642 \u0627\u0644\u0628\u0646\u0641\u0633\u062c\u064a\u0629 \u2013 \u0627\u0644\u0645\u0631\u0626\u064a\u0629\u00a0 , \u0648\u0642\u064a\u0627\u0633\u0627\u062a \u0627\u0644\u062a\u0648\u0635\u064a\u0644\u064a\u0629 \u0627\u0644\u0645\u0648\u0644\u0627\u0631\u064a\u0629 \u0648\u0627\u0644\u062d\u0633\u0627\u0633\u064a\u0629 \u0627\u0644\u0645\u063a\u0646\u0627\u0637\u064a\u0633\u064a\u0629 \u0648, \u0648\u0627\u0644\u062a\u062d\u0644\u064a\u0644 \u0627\u0644\u062f\u0642\u064a\u0642 \u0644\u0644\u0639\u0646\u0627\u0635\u0631 \u0644\u0628\u0639\u0636 \u0627\u0644\u0645\u0639\u0642\u062f\u0627\u062a \u0627\u0644\u0645\u062d\u0636\u0631\u0629 \u0648\u0627\u064a\u0636\u0627\u00a0 \u062a\u0639\u064a\u064a\u0646 \u0645\u062d\u062a\u0648\u0649 \u0627\u0644\u0641\u0644\u0632 \u0628\u0648\u0627\u0633\u0637\u0629 \u062a\u0642\u0646\u064a\u0629 \u0627\u0644\u0627\u0645\u062a\u0635\u0627\u0635 \u0627\u0644\u0630\u0631\u064a , \u0648\u0628\u0646\u0627\u0621 \u0639\u0644\u0649 \u0627\u0644\u0646\u062a\u0627\u0626\u062c \u0648\u0627\u0644\u062a\u0634\u062e\u064a\u0635\u0627\u062a \u0627\u0644\u0645\u0630\u0643\u0648\u0631\u0629 \u0627\u0639\u0644\u0627\u0647 \u0641\u0642\u062f \u0627\u0642\u062a\u0631\u062d \u0645\u0627 \u064a\u0644\u064a<\/span><\/h4>\n<ul>\n<li>\n<h4><span style=\"color: #000080;\">\u0627\u0646 \u0644\u0645\u0639\u0642\u062f\u0627\u062a \u0627\u0644\u0643\u0631\u0648\u0645 \u0627\u0644\u062b\u0644\u0627\u062b\u064a \u0644\u0643\u0644\u0627 \u0627\u0644\u0644\u064a\u0643\u0627\u0646\u062f\u064a\u0646 \u0627\u0644\u0645\u062d\u0636\u0631\u064a\u0646 \u0627\u0644\u0634\u0643\u0644 \u0627\u0644\u062b\u0645\u0627\u0646\u064a \u0627\u0644\u0633\u0637\u0648\u062d .<\/span><\/h4>\n<\/li>\n<li>\n<h4><span style=\"color: #000080;\">\u0627\u0642\u062a\u0631\u062d\u00a0 \u0627\u0644\u0634\u0643\u0644 \u0631\u0628\u0627\u0639\u064a \u0627\u0644\u0633\u0637\u0648\u062d \u0644\u0645\u0639\u0642\u062f\u0627\u062a \u0627\u064a\u0648\u0646 \u00a0\u0627\u0644\u0645\u0646\u063a\u0646\u064a\u0632(II), \u0627\u0644\u0643\u0648\u0628\u0644\u062a(II), \u0627\u0644\u0646\u064a\u0643\u0644 (II) , \u0627\u0644\u062e\u0627\u0631\u0635\u064a\u0646(II) \u0648\u0627\u0644\u0643\u0627\u062f\u0645\u064a\u0648\u0645 (II) \u0644\u0644\u064a\u0643\u0627\u0646\u062f\u0627\u062a \u0627\u0644\u0645\u062d\u0636\u0631\u0629.<\/span><\/h4>\n<\/li>\n<li>\n<h4><span style=\"color: #000080;\">\u0627\u0644\u0634\u0643\u0644 \u0627\u0644\u0645\u0631\u0628\u0639 \u0627\u0644\u0645\u0633\u062a\u0648\u064a \u0643\u0627\u0646 \u0647\u0648 \u0627\u0644\u0634\u0643\u0644 \u0627\u0644\u0641\u0631\u0627\u063a\u064a \u0627\u0644\u0645\u0642\u062a\u0631\u062d \u0644\u0645\u0639\u062f\u0627\u062a \u0627\u0644\u0646\u062d\u0627\u0633(II) \u0627\u0644\u0645\u062d\u0636\u0631\u0629 \u0645\u0646 \u0627\u0644\u0644\u064a\u0643\u0627\u0646\u062f\u0627\u062a.<\/span><\/h4>\n<\/li>\n<\/ul>\n<h4><span style=\"color: #000080;\">\u0643\u0645\u0627 \u062a\u0645\u062a \u062f\u0631\u0627\u0633\u0629 \u0627\u0644\u0641\u0639\u0627\u0644\u064a\u0629 \u0627\u0644\u062d\u064a\u0627\u062a\u064a\u0629 \u0644\u0644\u064a\u0643\u0627\u0646\u062f\u0627\u062a \u0648 \u0645\u0639\u0642\u062f\u0627\u062a\u0647\u0627 \u0627\u0644\u0645\u062d\u0636\u0631\u0629 \u0648 \u0636\u062f \u0627\u0631\u0628\u0639\u0629 \u0627\u0646\u0648\u0627\u0639\u00a0 \u0645\u0646 \u0627\u0644\u0628\u0643\u062a\u0631\u064a\u0627 (<em>Escherichia<\/em><em>\u00a0coli<\/em>, <em>Pseudomonas auroginosa<\/em>, <em>Staphylococcus aureus<\/em> \u0648\u00a0 <em>Bacillus subtilis<\/em>) \u0648\u062a\u0645 \u0627\u062e\u062a\u0628\u0627\u0631 \u0641\u0639\u0627\u0644\u064a\u0629 \u0627\u0644\u0645\u0631\u0643\u0628\u0627\u062a \u0627\u0644\u0645\u062d\u0636\u0631\u0629 \u0648\u0645\u0642\u0627\u0631\u0646\u062a\u0647\u0627 \u0628\u0627\u0644\u0645\u0636\u0627\u062f \u0627\u0644\u0628\u0643\u062a\u064a\u0631\u064a Cefotaxime \u0648\u0627\u0638\u0647\u0631\u062a \u0627\u0644\u0646\u062a\u0627\u0626\u062c \u0641\u0639\u0627\u0644\u064a\u0629 \u0645\u0642\u0627\u0631\u0628\u0629 \u0644\u0644\u0645\u0631\u0643\u0628\u0627\u062a \u0627\u0644\u0645\u062d\u0636\u0631\u0629 \u0645\u0639 \u0627\u0644\u0645\u0636\u0627\u062f \u0627\u0644\u0628\u0643\u062a\u064a\u0631\u064a \u0627\u0644\u0645\u0633\u062a\u062e\u062f\u0645.<\/span><\/h4>\n<h4><span style=\"color: #000080;\">\u00a0\u0648\u0627\u064a\u0636\u0627 \u062a\u0645 \u0627\u0633\u062a\u062e\u062f\u0627\u0645 \u0646\u0648\u0639\u064a\u0646 \u0645\u0646 \u0627\u0644\u0641\u0637\u0631(<em>Candida albicans<\/em> \u0648 <em>Rhizopus sporium<\/em>) \u0648\u0627\u0638\u0647\u0631\u062a \u0627\u0644\u0646\u062a\u0627\u0626\u062c \u0627\u0646 \u062c\u0645\u064a\u0639 \u0627\u0644\u0644\u064a\u0643\u0627\u0646\u062f\u0627\u062a \u0645\u0639 \u0645\u0639\u0642\u062f\u0627\u062a\u0647\u0627 \u0627\u0644\u0645\u062d\u0636\u0631\u0629 \u062a\u0645\u062a\u0644\u0643 \u0641\u0639\u0627\u0644\u064a\u0629 \u062c\u064a\u062f\u0629 \u0627\u062a\u062c\u0627\u0647 \u0627\u0644\u0641\u0637\u0631.<\/span><\/h4>\n<h4><span style=\"color: #000080;\">\u00a0 \u0648\u062e\u0644\u0635\u062a \u0627\u0644\u0637\u0627\u0644\u0628\u0629 \u0627\u0644\u0649 \u0627\u0644\u062a\u0648\u0635\u064a\u0627\u062a \u0627\u0644\u0627\u062a\u064a\u0629 :<\/span><\/h4>\n<ol>\n<li>\n<h4><span style=\"color: #000080;\">\u062a\u062d\u0636\u064a\u0631 \u0628\u0631\u0648\u0627\u0628\u0637 semicarbazone \u0627\u0644\u062c\u062f\u064a\u062f\u0629 \u0628\u0628\u062f\u0627\u0626\u0644 \u0645\u062e\u062a\u0644\u0641\u0629.<\/span><\/h4>\n<\/li>\n<li>\n<h4><span style=\"color: #000080;\">\u062a\u062d\u0636\u064a\u0631 \u0628\u0631\u0648\u0627\u0628\u0637 \u062b\u064a\u0648\u0633\u064a\u0645\u064a\u0643\u0627\u0631\u0628\u0632\u0648\u0646 \u062c\u062f\u064a\u062f\u0629 \u0645\u0639 \u0628\u062f\u0627\u0626\u0644 \u0645\u062e\u062a\u0644\u0641\u0629.<\/span><\/h4>\n<\/li>\n<li>\n<h4><span style=\"color: #000080;\">\u062a\u062d\u0636\u064a\u0631 \u0645\u0639\u0642\u062f\u0627\u062a \u0641\u0644\u0632\u064a\u0629 \u062c\u062f\u064a\u062f\u0629 \u0628\u0627\u0644\u0631\u0627\u0628\u0637 \u0623\u0639\u0644\u0627\u0647 \u0627\u0644\u0630\u064a \u064a\u0639\u062a\u0645\u062f \u0639\u0644\u0649 \u0627\u0644\u0633\u0644\u0633\u0644\u0629 \u0627\u0644\u062b\u0627\u0646\u064a\u0629 \u0648 \/ \u0623\u0648 \u0627\u0644\u062b\u0627\u0644\u062b\u0629 \u0645\u0646 \u0627\u0644\u0623\u064a\u0648\u0646\u0627\u062a \u0627\u0644\u0627\u0646\u062a\u0642\u0627\u0644\u064a\u0629.<\/span><\/h4>\n<\/li>\n<li>\n<h4><span style=\"color: #000080;\">\u0627\u0644\u0639\u0645\u0644 \u0639\u0644\u0649 \u0625\u0639\u0627\u062f\u0629 \u062a\u0628\u0644\u0648\u0631 \u0627\u0644\u0631\u0648\u0627\u0628\u0637 \u0648\u0645\u062c\u0645\u0639\u0627\u062a\u0647\u0627 \u0627\u0644\u0645\u0639\u062f\u0646\u064a\u0629 \u0644\u0639\u0632\u0644 \u0645\u0631\u0643\u0628 \u0645\u0646\u0627\u0633\u0628 \u0644\u0644\u0623\u0634\u0639\u0629 \u0627\u0644\u0633\u064a\u0646\u064a\u0629 \u0628\u0644\u0648\u0631\u0629 \u0645\u0641\u0631\u062f\u0629.<\/span><\/h4>\n<\/li>\n<li>\n<h4><span style=\"color: #000080;\">\u0627\u0644\u062a\u0648\u0633\u0639 \u0641\u064a \u062f\u0631\u0627\u0633\u0629 \u0627\u0644\u0646\u0634\u0627\u0637 \u0627\u0644\u0645\u064a\u0643\u0631\u0648\u0628\u064a\u0648\u0644\u0648\u062c\u064a \u0645\u0646 \u062e\u0644\u0627\u0644 \u0627\u062e\u062a\u0628\u0627\u0631 \u0627\u0644\u0631\u0648\u0627\u0628\u0637 \u0648\u0645\u0631\u0643\u0628\u0627\u062a\u0647\u0627 \u0627\u0644\u0645\u0639\u062f\u0646\u064a\u0629 \u0636\u062f \u0627\u0644\u0643\u0627\u0626\u0646\u0627\u062a \u0627\u0644\u062d\u064a\u0629 \u0627\u0644\u062f\u0642\u064a\u0642\u0629 \u0627\u0644\u0623\u062e\u0631\u0649.<\/span><\/h4>\n<\/li>\n<li>\n<h4 style=\"text-align: right;\"><span style=\"color: #000080;\">\u062f\u0631\u0627\u0633\u0629 \u0627\u0644\u0646\u0634\u0627\u0637 \u0627\u0644\u0645\u0636\u0627\u062f \u0644\u0644\u0633\u0631\u0637\u0627\u0646 \u0648\u0627\u0646\u0642\u0633\u0627\u0645 \u0627\u0644\u062d\u0645\u0636 \u0627\u0644\u0646\u0648\u0648\u064a \u0644\u0644\u0645\u0631\u0643\u0628\u0627\u062a \u0627\u0644\u0645\u062d\u0636\u0631\u0629<\/span><\/h4>\n<hr \/>\n<\/li>\n<\/ol>\n<ol>\n<li>\n<h4 style=\"text-align: left;\"><span style=\"color: #000080;\"><strong>\u00a0<\/strong><\/span><\/h4>\n<\/li>\n<\/ol>\n<h3 style=\"text-align: left;\"><span style=\"color: #993366;\">Formation, Characterization and Biological Evaluation of New Metal Complexes With Carbazones Ligands<\/span><\/h3>\n<h3 style=\"text-align: left;\"><span style=\"color: #993366;\">By Hadeel \u00a0J. Abbas<\/span><\/h3>\n<h3 style=\"text-align: left;\"><span style=\"color: #993366;\">Supervised by Mohammed J. Al-Juboori<\/span><\/h3>\n<h3 style=\"text-align: left;\"><span style=\"color: #993366;\">The chemistry of Mannich-bases and their semi- and thiosemicarbazone compounds including metal complexes played a great role in the organic, inorganic and coordination chemistry. This is related to their impact on bioinorganic, analytical, environmental and pharmaceutical chemistry. According to these facts the aim of the work could be summarized as<\/span><\/h3>\n<h3 style=\"text-align: left;\"><span style=\"color: #993366;\">Synthesis of novel semi- and thiosemicarbazone from mixing of a Mannich base that prepared via a three-component reaction (cyclohexanone, benzaldehyde and phenylhydrazine) with the semi- and thiosemicarbazide reagent<\/span><\/h3>\n<h3 style=\"text-align: left;\"><span style=\"color: #993366;\">Formation of metal complexes from the reaction of both ligands with Cr(III), Mn(II), Co(II),\u00a0 Ni(II),\u00a0 Cu(II),\u00a0 Zn(II) and\u00a0 Cd(II) ions.<\/span><\/h3>\n<h3 style=\"text-align: left;\"><span style=\"color: #993366;\">Characterization of the prepared compounds using several physicochemical techniques.<\/span><\/h3>\n<h3 style=\"text-align: left;\"><span style=\"color: #993366;\">Study the geometrical arrangement and biological activity of these compounds.<\/span><\/h3>\n<h3 style=\"text-align: left;\"><span style=\"color: #993366;\">\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0 Summary<\/span><\/h3>\n<h3 style=\"text-align: left;\"><span style=\"color: #993366;\">The preparation of 2-(phenyl(2-phenylhydrazinyl)methyl)- cyclohexan-1-one compound (M) derived from the Mannich approach in which CaCl2 was used as a catalyst.The reaction was achieved in EtOH by mixing three components; benzaldehyde, phenylhydrazine and cyclohexanone with a 1:1:1 mole ratio. The resulting mixture was stirred for 12 h at room temperature. The title product was obtained as a solid material that filtered off, washed with distilled water, recrystallized from EtOH and then dried in the air, see Scheme(1). Compound (M) was used to prepare two of new Schiff base ligands<\/span><\/h3>\n<h3 style=\"text-align: left;\"><span style=\"color: #993366;\">The first ligand (E)-2-(2-(phenyl(2-phenylhy- drazinyl)methyl)cyclohexylidene)hydrazine-1-carboxamide (HL1) was prepared from the reaction of semicarbazide with compound (M) in a mole ratio of 1:1 using EtOH and heated for 6h.The solid product was filtered off and then washed with ethanol and ether, Scheme (1).<\/span><\/h3>\n<h3 style=\"text-align: left;\"><span style=\"color: #993366;\">The second ligand (E)-2-(2-(phenyl(2-phenylhydrazinyl)- methyl)cyclohexylidene)hydrazine-1-carbothioamide (HL2) was prepared from the reaction of thiosemicarbazide with compound (M) in a mole ratio of 1:1 using EtOH and heated for 4h. The solid product was filtered<\/span><\/h3>\n<h3 style=\"text-align: left;\"><span style=\"color: #993366;\">The recommendations:-<\/span><\/h3>\n<h3 style=\"text-align: left;\"><span style=\"color: #993366;\">. Preparation of new semicarbazone ligands with different substituents.<\/span><\/h3>\n<h3 style=\"text-align: left;\"><span style=\"color: #993366;\">. Preparation of new thiosemicarbazone ligands with different substituents.<\/span><\/h3>\n<h3 style=\"text-align: left;\"><span style=\"color: #993366;\">. Preparation of new metal complexes with the above ligand that based on the second and\/or third series of transition ions.<\/span><\/h3>\n<h3 style=\"text-align: left;\"><span style=\"color: #993366;\">. Working on the recrystallisation of the ligands and their metal complexes to isolate compound suitable for X-ray single crystal.<\/span><\/h3>\n<h3 style=\"text-align: left;\"><span style=\"color: #993366;\">. Expanding the microbiological activity study by testing the ligands and their metal complexes against other microorganisms.<\/span><\/h3>\n<h3 style=\"text-align: left;\"><span style=\"color: #993366;\">. Studying the anti-cancer activity and DNA cleavage of the prepared compounds.<\/span><\/h3>\n<h3 style=\"text-align: left;\"><\/h3>\n<h4><\/h4>\n<h4><\/h4>\n","protected":false},"excerpt":{"rendered":"<p>\u0646\u0627\u0642\u0634 \u0642\u0633\u0645 \u0627\u0644\u0643\u064a\u0645\u064a\u0627\u0621 \u0641\u064a \u0643\u0644\u064a\u0629 \u0627\u0644\u062a\u0631\u0628\u064a\u0629 \u0644\u0644\u0639\u0644\u0648\u0645 \u0627\u0644\u0635\u0631\u0641\u0629 (\u0627\u0628\u0646 \u0627\u0644\u0647\u064a\u062b\u0645) \u0631\u0633\u0627\u0644\u0629 \u0627\u0644\u0645\u0627\u062c\u0633\u062a\u064a\u0631 \u0627\u0644\u0645\u0648\u0633\u0648\u0645\u0629 &#8221; \u062a\u062d\u0636\u064a\u0631 \u0648 \u062a\u0634\u062e\u064a\u0635 \u0645\u0639 \u0627\u0644\u062a\u0642\u064a\u064a\u0645 \u0627\u0644\u0628\u064a\u0648\u0644\u0648\u062c\u064a&#8230;.<a class=\"cz_readmore\" href=\"https:\/\/ihcoedu.uobaghdad.edu.iq\/?p=44557\"><i class=\"fa fa-angle-left\" aria-hidden=\"true\"><\/i><span>\u0627\u0644\u0645\u0632\u064a\u062f<\/span><\/a><\/p>\n","protected":false},"author":25,"featured_media":44561,"comment_status":"closed","ping_status":"closed","sticky":false,"template":"","format":"standard","meta":{"_lmt_disableupdate":"no","_lmt_disable":"","footnotes":""},"categories":[7,59,98,16],"tags":[23,61,47],"class_list":["post-44557","post","type-post","status-publish","format-standard","has-post-thumbnail","hentry","category-7","category-59","category-98","category-16","tag-ihcoedu","tag-61","tag-chem"],"modified_by":"ihcoedu","_links":{"self":[{"href":"https:\/\/ihcoedu.uobaghdad.edu.iq\/index.php?rest_route=\/wp\/v2\/posts\/44557","targetHints":{"allow":["GET"]}}],"collection":[{"href":"https:\/\/ihcoedu.uobaghdad.edu.iq\/index.php?rest_route=\/wp\/v2\/posts"}],"about":[{"href":"https:\/\/ihcoedu.uobaghdad.edu.iq\/index.php?rest_route=\/wp\/v2\/types\/post"}],"author":[{"embeddable":true,"href":"https:\/\/ihcoedu.uobaghdad.edu.iq\/index.php?rest_route=\/wp\/v2\/users\/25"}],"replies":[{"embeddable":true,"href":"https:\/\/ihcoedu.uobaghdad.edu.iq\/index.php?rest_route=%2Fwp%2Fv2%2Fcomments&post=44557"}],"version-history":[{"count":0,"href":"https:\/\/ihcoedu.uobaghdad.edu.iq\/index.php?rest_route=\/wp\/v2\/posts\/44557\/revisions"}],"wp:featuredmedia":[{"embeddable":true,"href":"https:\/\/ihcoedu.uobaghdad.edu.iq\/index.php?rest_route=\/wp\/v2\/media\/44561"}],"wp:attachment":[{"href":"https:\/\/ihcoedu.uobaghdad.edu.iq\/index.php?rest_route=%2Fwp%2Fv2%2Fmedia&parent=44557"}],"wp:term":[{"taxonomy":"category","embeddable":true,"href":"https:\/\/ihcoedu.uobaghdad.edu.iq\/index.php?rest_route=%2Fwp%2Fv2%2Fcategories&post=44557"},{"taxonomy":"post_tag","embeddable":true,"href":"https:\/\/ihcoedu.uobaghdad.edu.iq\/index.php?rest_route=%2Fwp%2Fv2%2Ftags&post=44557"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}