{"id":47428,"date":"2022-12-27T09:47:57","date_gmt":"2022-12-27T06:47:57","guid":{"rendered":"https:\/\/ihcoedu.uobaghdad.edu.iq\/?p=47428"},"modified":"2023-06-28T01:00:14","modified_gmt":"2023-06-27T22:00:14","slug":"%d8%b1%d8%b3%d8%a7%d9%84%d8%a9-%d9%85%d8%a7%d8%ac%d8%b3%d8%aa%d9%8a%d8%b1-%d8%aa%d8%a8%d8%ad%d8%ab-%d8%aa%d8%ad%d8%b6%d9%8a%d8%b1%d8%b3%d8%b7%d8%ad-%d9%85%d9%86-%d8%ac%d8%b3%d9%8a%d9%85%d8%a7%d8%aa","status":"publish","type":"post","link":"https:\/\/ihcoedu.uobaghdad.edu.iq\/?p=47428","title":{"rendered":"\u0631\u0633\u0627\u0644\u0629 \u0645\u0627\u062c\u0633\u062a\u064a\u0631 \u062a\u0628\u062d\u062b \u062a\u062d\u0636\u064a\u0631\u0633\u0637\u062d \u0645\u0646 \u062c\u0633\u064a\u0645\u0627\u062a \u0623\u0648\u0643\u0633\u064a\u062f \u0627\u0644\u0646\u064a\u0643\u0644 \u0627\u0644\u0646\u0627\u0646\u0648\u064a\u0629 (NiONPs) \u0648\u062a\u0634\u062e\u064a\u0635\u0647 \u0628\u062a\u0642\u0646\u064a\u0627\u062a FTIR \u00a0\u0648 XRD \u00a0\u0648 SEM \u0648 EDS \u0648 AFM"},"content":{"rendered":"

\"\"\u00a0<\/strong><\/h4>\n

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    \n
  • \n

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  • \n

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  • \n

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  • \n

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    \u00a0<\/strong><\/h4>\n

    \"\"<\/strong><\/h4>\n

    \u0648\u064a\u0647\u062f\u0641 \u0627\u0644\u0628\u062d\u062b \u0627\u0644\u0649 :<\/strong><\/h4>\n
      \n
    • \n

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    • \n

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    • \n

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    • \n

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    • \n

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      <\/h4>\n

      \u0627\u062d\u062a\u0648\u062a \u0647\u0630\u0647 \u0627\u0644\u062f\u0631\u0627\u0633\u0629 \u062a\u062d\u0636\u064a\u0631 \u062c\u0633\u064a\u0645\u0627\u062a \u0646\u0627\u0646\u0648\u064a\u0629 \u0645\u062a\u0645\u062b\u0644\u0629 \u0628\u0623\u0648\u0643\u0633\u064a\u062f \u0627\u0644\u0646\u064a\u0643\u0644 \u0627\u0644\u0646\u0627\u0646\u0648\u064a NiONPs))\u0648\u0627\u0644\u0645\u062a\u0631\u0627\u0643\u0628 \u0646\u064a\u0643\u0644\/\u0627\u0648\u0643\u0633\u064a\u062f \u0627\u0644\u0646\u064a\u0643\u0644 \u0627\u0644\u0646\u0627\u0646\u0648\u064a (NiNPs\/NiONPs) \u0628\u0637\u0631\u064a\u0642\u0629 \u0627\u0644\u062a\u0631\u0633\u064a\u0628\u060c \u0644\u063a\u0631\u0636 \u0627\u0633\u062a\u062e\u062f\u0627\u0645\u0647\u0627 \u0643\u0633\u0637\u0648\u062d \u0645\u0627\u0632\u0629. \u0648\u0634\u062e\u0635\u062a \u0627\u0644\u062c\u0633\u064a\u0645\u0627\u062a \u0627\u0644\u0646\u0627\u0646\u0648\u064a\u0629 \u0627\u0644\u0645\u062d\u0636\u0631\u0629 \u062a\u0644\u0643 \u0628\u062a\u0642\u0646\u064a\u0629 \u062d\u064a\u0648\u062f \u0627\u0644\u0627\u0634\u0639\u0629 \u0627\u0644\u0633\u064a\u0646\u064a\u0629 \u00a0(XRD)\u0648\u0645\u0637\u064a\u0627\u0641\u064a\u0629 \u0627\u0644\u0627\u0634\u0639\u0629 \u062a\u062d\u062a \u0627\u0644\u062d\u0645\u0631\u0627\u0621 (FTIR) \u0648\u062a\u0634\u062a\u062a \u0627\u0644\u0637\u0627\u0642\u0629 \u0627\u0644\u0633\u064a\u0646\u064a\u0629 (EDS)\u0648\u062a\u062d\u0644\u064a\u0644 \u0645\u062c\u0647\u0631 \u0627\u0644\u0642\u0648\u0629 \u0627\u0644\u0630\u0631\u064a\u0629(AFM)\u060c \u0644\u062a\u062d\u062f\u064a\u062f \u062a\u0631\u0643\u064a\u0628\u0647\u0627 \u0648\u0634\u0643\u0644\u0647\u0627 \u0648\u0646\u0642\u0627\u0648\u062a\u0647\u0627. \u0643\u0645\u0627 \u062a\u0645\u062a \u062f\u0631\u0627\u0633\u0629 \u0627\u0644\u062e\u0635\u0627\u0626\u0635 \u0627\u0644\u0633\u0637\u062d\u064a\u0629\u00a0 \u0644\u0640 NiONPs \u0648 NiNPs\/NiONPs \u0627\u0644\u0645\u062d\u0636\u0631\u0629 \u0628\u062a\u0642\u0646\u064a\u0629\u00a0 \u0628\u0631\u0648\u0646\u0631- \u0627\u064a\u0645\u064a\u062a \u2013 \u062a\u064a\u0644\u0631 BET\u00a0 \u0648\u0628\u0627\u0631\u064a\u062a \u2013 \u062c\u0648\u064a\u0646\u0631 \u2013 \u0647\u0627\u0644\u0646\u062f\u0627\u060c\u00a0 \u0628\u0627\u0644\u0627\u0636\u0627\u0641\u0629 \u0627\u0644\u0649 \u0627\u0633\u062a\u062e\u062f\u0627\u0645 \u0627\u0644\u0645\u062c\u0647\u0631 \u0627\u0644\u0627\u0644\u0643\u062a\u0631\u0648\u0646\u064a \u0627\u0644\u0645\u0627\u0633\u062d SEM \u0644\u062a\u0623\u0643\u064a\u062f \u0634\u0643\u0644 \u0648\u0645\u0648\u0631\u0641\u0648\u0644\u0648\u062c\u064a\u0627 \u0627\u0644\u062f\u0642\u0627\u0626\u0642 \u0627\u0644\u0646\u0627\u0646\u0648\u064a\u0629.<\/h4>\n

      \u0631\u0643\u0632\u062a \u0647\u0630\u0647 \u0627\u0644\u062f\u0631\u0627\u0633\u0629 \u0628\u0634\u0643\u0644 \u0631\u0626\u064a\u0633\u064a \u0639\u0644\u0649 \u0627\u062e\u062a\u0628\u0627\u0631 \u0642\u0627\u0628\u0644\u064a\u0629 \u0633\u0637\u062d\u064a \u0627\u0644\u0627\u0645\u062a\u0632\u0627\u0632 \u0627\u0644\u0645\u062d\u0636\u0631\u064a\u0646 \u0644\u0627\u0632\u0627\u0644\u0629 \u0627\u0644\u0628\u0627\u0631\u0627 \u0643\u0644\u0648\u0631\u0648\u0641\u064a\u0646\u0648\u0644 \u0645\u0646 \u0645\u062d\u0644\u0648\u0644\u0647 \u0627\u0644\u0645\u0627\u0626\u064a \u0639\u0646\u062f \u0627\u0644\u062f\u0631\u062c\u0627\u062a \u0627\u0644\u062d\u0631\u0627\u0631\u064a\u0629K (323\u060c 313\u060c 303) \u0628\u0648\u062c\u0648\u062f \u0648\u0639\u062f\u0645 \u0648\u062c\u0648\u062f \u062a\u0623\u062b\u064a\u0631 \u0627\u0644\u0636\u0648\u0621. \u0648\u0642\u062f \u062a\u0645 \u062a\u062d\u062f\u064a\u062f \u0627\u0644\u0638\u0631\u0648\u0641 \u0627\u0644\u062a\u062c\u0631\u064a\u0628\u064a\u0629 \u0627\u0644\u0645\u062b\u0644\u0649 \u0644\u0644\u0627\u0645\u062a\u0632\u0627\u0632 \u0645\u0646 \u0648\u0632\u0646 \u0627\u0644\u0633\u0637\u062d \u0627\u0644\u0645\u0627\u0632 \u0648\u0632\u0645\u0646 \u0627\u0644\u0627\u062a\u0632\u0627\u0646 \u0648\u062a\u0631\u0643\u064a\u0632 \u0645\u062d\u0644\u0648\u0644 \u0627\u0644\u0641\u064a\u0646\u0648\u0644 \u0648\u062f\u0631\u062c\u0629 \u0627\u0644\u062d\u0631\u0627\u0631\u0629 \u0648\u0627\u0644\u0634\u062f\u0629 \u0627\u0644\u0627\u064a\u0648\u0646\u064a\u0629\u060c \u0641\u0648\u062c\u062f \u0627\u0646 \u0627\u0644\u0632\u0645\u0646 \u0627\u0644\u0644\u0627\u0632\u0645 \u0644\u062d\u062f\u0648\u062b \u0627\u0644\u0627\u062a\u0632\u0627\u0646 \u0647\u0648 (120) \u062f\u0642\u064a\u0642\u0629 . \u0648\u062a\u0645 \u062a\u0637\u0628\u064a\u0642 \u0627\u0644\u0628\u064a\u0627\u0646\u0627\u062a \u0627\u0644\u062a\u062c\u0631\u064a\u0628\u064a\u0629 \u0644\u0639\u0645\u0644\u064a\u0629 \u0627\u0644\u0627\u0645\u062a\u0632\u0627\u0632 \u0639\u0644\u0649 \u0646\u0645\u0627\u0630\u062c \u0641\u0631\u0646\u062f\u0644\u0634 (Freundlic) \u0648\u0644\u0627\u0646\u0643\u0645\u0627\u064a\u0631(Langmuir) \u0648\u062a\u064a\u0645\u0643\u0646((Temekn\u060c \u0648\u0627\u0643\u062f\u062a \u0627\u0644\u0646\u062a\u0627\u0626\u062c \u062a\u0648\u0627\u0641\u0642\u0647\u0627 \u0645\u0639 \u0627\u0646\u0645\u0648\u0630\u062c \u0641\u0631\u0646\u062f\u0644\u0634 \u0627\u0643\u062b\u0631 \u0645\u0645\u0627 \u0645\u0639 \u0627\u0646\u0645\u0648\u0630\u062c\u064a \u0644\u0627\u0646\u0643\u0645\u0627\u064a\u0631 \u0648\u062a\u064a\u0645\u0643\u0646. \u0643\u0645\u0627 \u062a\u0645 \u0627\u062d\u062a\u0633\u0627\u0628 \u0627\u0644\u062f\u0648\u0627\u0644 \u0627\u0644\u062b\u0631\u0645\u0648\u062f\u064a\u0646\u0627\u0645\u064a\u0643\u064a\u0629 \u0644\u0646\u0638\u0627\u0645\u064a \u0627\u0644\u0627\u0645\u062a\u0632\u0627\u0632 (\u062f\u0627\u0644\u0629 \u0643\u064a\u0628\u0633 \u00a0\u0648\u0627\u0644\u0627\u0646\u062a\u0631\u0648\u0628\u064a \u00a0\u0648\u0627\u0644\u0627\u0646\u062b\u0627\u0644\u0628\u064a )\u060c \u0648\u0648\u062c\u062f \u0645\u0646 \u0627\u0644\u0642\u064a\u0645\u0629 \u0627\u0644\u0645\u0648\u062c\u0628\u0629 \u0644\u0644\u0627\u0646\u062b\u0627\u0644\u0628\u064a\u00a0 \u0627\u0646 \u0627\u0644\u0639\u0645\u0644\u064a\u0629 \u0628\u0637\u0628\u064a\u0639\u062a\u0647\u0627 \u0645\u0627\u0635\u0629 \u0644\u0644\u062d\u0631\u0627\u0631\u0629 Endothermic)). \u0628\u064a\u0646\u0645\u0627 \u0627\u0643\u062f\u062a \u0627\u0644\u0642\u064a\u0645\u0629 \u0627\u0644\u0633\u0627\u0644\u0628\u0629 \u0644\u062f\u0627\u0644\u0629 \u0643\u064a\u0628\u0633 \u0627\u0644\u062d\u0631\u0629 \u0639\u0644\u0649 \u062a\u0644\u0642\u0627\u0626\u064a\u0629 \u0639\u0645\u0644\u064a\u0629 \u0627\u0644\u0627\u0645\u062a\u0632\u0627\u0632\u060c \u0643\u0645\u0627 \u062f\u0644\u062a \u0627\u0644\u0642\u064a\u0645\u0629 \u0627\u0644\u0645\u0648\u062c\u0628\u0629 \u0644\u0644\u0627\u0646\u062a\u0631\u0648\u0628\u064a \u0639\u0644\u0649 \u0646\u0642\u0635\u0627\u0646 \u0627\u0646\u062a\u0638\u0627\u0645 \u062a\u0631\u062a\u064a\u0628 \u062c\u0632\u064a\u0626\u0627\u062a \u0627\u0644\u0641\u064a\u0646\u0648\u0644 \u0639\u0644\u0649 \u0633\u0637\u062d\u064a \u0627\u0644\u0627\u0645\u062a\u0632\u0627\u0632.<\/h4>\n

      <\/h4>\n

      \u0648\u062a\u0645\u0643\u0646\u062a \u0627\u0644\u0628\u0627\u062d\u062b\u0629 \u0645\u0646 \u0627\u0642\u062a\u0631\u0627\u062d \u0628\u0639\u0636 \u0627\u0644\u062a\u0648\u0635\u064a\u0627\u062a \u0627\u0644\u062a\u0627\u0644\u064a\u0629 \u060c\u0627\u0633\u062a\u0646\u0627\u062f\u0627\u064b \u0639\u0644\u0649 \u0645\u0627 \u062a\u0642\u062f\u0645 \u0645\u0646 \u0647\u0630\u0647 \u0627\u0644\u062f\u0631\u0627\u0633\u0629\u00a0 :-<\/h4>\n
        \n
      1. \n

        \u062a\u0648\u0638\u064a\u0641 \u062c\u0633\u064a\u0645\u0627\u062a \u0627\u0648\u0643\u0633\u064a\u062f \u0627\u0644\u0646\u064a\u0643\u0644 \u0627\u0644\u0646\u0627\u0646\u0648\u064a\u0629 (NiONPs) \u0648\u0627\u0644\u0645\u062a\u0631\u0627\u0643\u0628\u00a0 (NiNPs\/NiONPs) \u0627\u0644\u0645\u062d\u0636\u0631\u064a\u0646 \u0641\u064a \u0647\u0630\u0647 \u0627\u0644\u062f\u0631\u0627\u0633\u0629 \u0644\u0627\u0645\u062a\u0632\u0627\u0632\u0627\u0644\u0641\u064a\u0646\u0648\u0644\u0627\u062a \u0648\u0648\u0645\u0644\u0648\u062b\u0627\u062a \u0627\u062e\u0631\u0649.<\/h4>\n<\/li>\n
      2. \n

        \u062f\u0631\u0627\u0633\u0629 \u062d\u0631\u0643\u064a\u0629 \u0644\u0627\u0645\u062a\u0632\u0627\u0632 \u0627\u0644\u0628\u0627\u0631\u0627\u0643\u0644\u0648\u0631\u0648\u0641\u064a\u0646\u0648\u0644 \u0639\u0644\u0649 \u062c\u0633\u064a\u0645\u0627\u062a \u0627\u0648\u0643\u0633\u064a\u062f \u0627\u0644\u0646\u064a\u0643\u0644 \u0627\u0644\u0646\u0627\u0646\u0648\u064a\u0629 NiONPs)) \u0648\u0627\u0644\u0645\u062a\u0631\u0627\u0643\u0628\u00a0 (NiNPs\/NiONPs) \u0627\u0644\u0645\u062d\u0636\u0631\u064a\u0646.<\/h4>\n<\/li>\n
      3. \n

        \u062a\u0634\u0648\u064a\u0628 \u0627\u0644\u0633\u0637\u062d \u0627\u0644\u0627\u0648\u0644 (NiONPs)\u0628\u062a\u0631\u0627\u0643\u064a\u0632 \u0645\u062e\u062a\u0644\u0641\u0629 \u0627\u062e\u0631\u0649 \u0645\u0646 \u0627\u0644\u0645\u0648\u0627\u062f \u0627\u0644\u0646\u0627\u0646\u0648\u064a\u0629 \u0648\u062f\u0631\u0627\u0633\u0629 \u062a\u0623\u062b\u064a\u0631\u0647\u0627 \u0639\u0644\u0649 \u0643\u0641\u0627\u0621\u0629 \u0627\u0644\u0627\u0645\u062a\u0632\u0627\u0632.<\/h4>\n<\/li>\n
      4. \n

        \u062a\u0634\u0648\u064a\u0628 \u0627\u0644\u0633\u0637\u062d \u0627\u0644\u062b\u0627\u0646\u064a(NiONPs\/NiNPs) \u0628\u0645\u0648\u0627\u062f \u0627\u062e\u0631\u0649 \u0648\u0627\u062e\u062a\u0628\u0627\u0631 \u0641\u0627\u0639\u0644\u064a\u062a\u0647\u0627 \u0641\u064a \u0627\u0644\u0627\u0645\u062a\u0632\u0627\u0632.<\/h4>\n<\/li>\n
      5. \n

        \u062f\u0631\u0627\u0633\u0629 \u0627\u0644\u062e\u0648\u0627\u0635 \u0627\u0644\u0645\u064a\u0643\u0627\u0646\u064a\u0643\u064a\u0629 \u0648\u0627\u0644\u0643\u0647\u0631\u0628\u0627\u0626\u064a\u0629 \u0644\u0640 NiONPs \u0648\u0627\u0644\u0645\u062a\u0631\u0627\u0643\u0628(NiNPs\/NiONPs).<\/h4>\n<\/li>\n<\/ol>\n

        \u062f\u0631\u0627\u0633\u0629 \u0627\u0644\u0641\u0639\u0627\u0644\u064a\u0629 \u0627\u0644\u0628\u0643\u062a\u064a\u0631\u064a\u0629 \u0648\u0627\u0644\u0641\u0637\u0631\u064a\u0629 \u0644\u0640 NiONPs \u0648\u0627\u0644\u0645\u062a\u0631\u0627\u0643\u0628 (NiNPs\/NiONPs).<\/h4>\n
        \n

        Adsorption and photo catalysis of parachloro phenol on nickel oxide nanoparticles in aqueous solution<\/span><\/h3>\n

        By Suaad Edan Hussian<\/span><\/h3>\n

        Supervised by Prof Dr. Juman \u00a0Ahmed Naser<\/span><\/h3>\n

        Aim of the Research<\/span><\/h3>\n

        \u00a0The aim of the research is to identify the Effect of Hands-On Strategy on<\/span><\/h3>\n

        -Preparing a surface of nickel oxide nanoparticles (NONPs) and diagnosing it with FTIR, XRD, SEM, EDS and AFM<\/span><\/h3>\n

        . Preparing a nanopound of nickel oxide nanoparticles and nickel nanoparticles (NiONPs\/NiNPs), for a comparative study after being diagnosed with the same techniques mentioned earlier<\/span><\/h3>\n

        . Use the nanosurfaces (NiONPs) and NiONPs\/NiNPs as adsorbing surfaces to adsorb parachlorophenol from its aqueous solution at different temperatures<\/span><\/h3>\n

        -Apply the experimental data of studied adsorption systems to Gels isothermats and Frendelch and Lenchmeier models and can, in addition to calculating the thermodynamic functions of the adsorption process<\/span><\/h3>\n

        -Conduct adsorption experiments with the presence and absence of light to test the susceptibility of prepared nanoparticles (NiONPs) and overlays (NiONPs\/NiNPs) to photocatalysis<\/span><\/h3>\n

        <\/h3>\n

        <\/h3>\n

        Abstract: This study included the preparation of nanoparticles represented by nickel oxide nanoparticles (NiONPs) and the compound nickel\/nickel oxide nanoparticles (NiNPs\/NiONPs) by deposition method, for the purpose of using them as adsorbent surfaces. The prepared nanoparticles were characterized by X-ray diffraction (XRD), infrared spectroscopy (FTIR) and X-ray energy scattering (EDS),(AFM)Atomic force microscope to determine their structure, shape and purity. The surface properties of NiONPs and NiNPs\/NiONPs prepared by BET-Bruner-Emmet-Teller and Barrett-Joyner-Halenda technique were studied, in addition to using SEM scanning electron microscopy to confirm the shape and morphology of the nanoparticles.<\/span><\/h3>\n

        This study focused mainly on testing the adsorption capacity of the prepared surfactants to remove para-chlorophenol from its aqueous solution at temperatures K (323, 313, and 303) with and without the influence of light. The optimal experimental conditions for adsorption were determined from the weight of the adsorbing surface, the equilibrium time, the concentration of the phenol solution, the temperature and the ionic intensity. It was found that the time required for equilibrium to occur was (120) minutes. The experimental data of the adsorption process were applied to the Freundlic, Langmuir and Timekn models, and the results confirmed their agreement with the Freundlich model more than with the Langmuir and Temekn models. The thermodynamic functions of the adsorption systems (Keeps function \u2206G, entropy \u2206S and enthalpy) were also calculated. (\u2206H), and it was found from the positive value of the enthalpy that the process is endothermic in nature. While the negative value of the free Kibs function confirmed the spontaneity of the adsorption process, and the positive value of the entropy indicated the irregularity of the arrangement of phenol molecules on the two adsorption surfaces.<\/span><\/h3>\n

        Recommendation:\u00a0 The following recommendations can be suggested, based on the above of this study:<\/span><\/h3>\n

        <\/h3>\n

        – Employing nickel oxide nanoparticles (NiONPs) and overlays (NiNPs\/NiONPs) prepared in this study to adsorb phenols and other contaminants.<\/span><\/h3>\n

        <\/h3>\n

        . A kinetic study of parachlorophenol adsorption on nickel oxide nanoparticles (NiONPs) and overlays (NiONPs\/NiNPs) prepared.<\/span><\/h3>\n

        – The first surface deformation (NiONPs) with various other concentrations of nanomaterials and studying their effect on adsorption efficiency.<\/span><\/h3>\n

        – Surface II (NiONPs\/NiNPs) with other materials and test their adsorption effectiveness.<\/span><\/h3>\n

        – Studying the mechanical and electrical properties of NiONPs and overlays (NiONPs\/NiNPs).<\/span><\/h3>\n

        <\/h3>\n

        – Studying the bacterial and fungal efficacy of NiONPs and overlays (NiNPs<\/span><\/h3>\n

         <\/p>\n","protected":false},"excerpt":{"rendered":"

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